Imide-siloxane block copolymer/silica hybrid membranes: Preparation, characterization and gas separation properties

Journal of Membrane Science

Volumn 220, Issue 1-2, 2003, Pages 59-73

  Park, Ho Bum ^a   Kim, Jang Ki ^a   Nam, Sang Yong ^b   Lee, Young Moo ^a  

^a Hanyang University   (South Korea)

^b Gyeongsang National University   (South Korea)

Author keywords

Gas separation; Membrane; Organic inorganic hybrid materials; Polydimethylsiloxane; Silica

Indexed keywords

BLOCK COPOLYMERS; CHEMICAL BONDS; INFRARED SPECTROSCOPY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SILICA; SOL-GELS;

GAS SELECTIVITY;

POLYMERIC MEMBRANES;

CARBON DIOXIDE; COPOLYMER; HELIUM; IMIDE; NITROGEN; OXYGEN; RUBBER; SILICON; SILICON DIOXIDE; SILOXANE;

COPOLYMER; FOURIER TRANSFORM; GAS SEPARATION; MEMBRANE; STRUCTURAL ANALYSIS; TEMPERATURE EFFECT;

ARTICLE; CHEMICAL COMPOSITION; CHEMICAL STRUCTURE; COVALENT BOND; GAS; GEL; INFRARED SPECTROSCOPY; MEMBRANE; NUCLEAR MAGNETIC RESONANCE; POLYMERIZATION; PRIORITY JOURNAL; REDUCTION; SEPARATION TECHNIQUE; SOLID; SYNTHESIS; TEMPERATURE DEPENDENCE; THERMOGRAVIMETRY;

EID: 0043169706     PISSN: 03767388     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0376-7388(03)00215-1     Document Type: Article

References (36)

1. Huang H.-H., Orler B., Wilkes G.L. Structure-property behavior of new hybrid materials incorporating oligomeric species into sol-gel glasses. Part 3. Effect of acid content, tetraethoxysilane content, and molecular weight of polydimethylsiloxane. Macromolecules. 20:1987;1322-1330.
2. Kohjiya S., Ochiai K., Yamashita S. Preparation of inorganic/organic hybrid gels by the sol-gel process. J. Non-Cryst. Solids. 119:1990;132-135.
3. Morikawa A., Iyoku Y., Kakimoto M., Imai Y. Preparation of a new class of polyimide-silica hybrid films by sol-gel process. Polym. J. 24(1):1992;107-113.
4. Mascia L., Kioul A. Polyimide-silica hybrid materials by sol-gel processing. J. Mater. Sci. Lett. 13:1994;641-643.
5. Kim J.H., Lee Y.M. Gas permeation properties of poly(amide-6-b-ethylene oxide)-silica hybrid membranes. J. Membr. Sci. 193:2001;209.
6. Yano S., Iwata K., Kurita K. Physical properties and structure of organic-inorganic hybrid materials produced by sol-gel process. Mater. Sci. Eng. C6:1998;75-90.
7. Xenopoulos C., Mascia L., Shaw S.J. Variables analysis in the gelation of alkoxysilane solutions for the production of polyimide-silica hybrids. Mater. Sci. Eng. C6:1998;99-114.
8. Morikawa A., Yamaguchi H., Kakimoto M., Imai Y. Formation of interconnected globular structure of silica phase in polyimide-silica hybrid films prepared by the sol-gel process. Chem. Mater. 6:1994;913-917.
9. Wang S., Ahmad Z., Mark J.E. Polyimide-silica hybrid materials modified by incorporation of an organically substituted alkoxysilane. Chem. Mater. 6:1994;943-946.
10. Mascia L., Kioul A. Influence of siloxane composition and morphology on properties of polyimide-silica hybrids. Polymer. 36(19):1995;3649-3659.
11. Mascia L., Zhang Z., Shaw S.J. Carbon fibre composites based on polyimide/silica creamers: aspects of structure-properties relationship. Composites Part A. 27A:1996;1211-1221.
12. Schrotter I.C., Smaihi M., Guizard C. Polyimide-siloxane hybrid materials: influence of coupling agents addition on microstructure and properties. J. Appl. Polym. Sci. 61:1996;2137-2149.
13. Furukawa N., Yuasa M., Kimura Y. Characterization of polysiloxane-block-polyimides with silicate group in the polysiloxane segments. Polymer. 40:1999;1853-1862.
14. Zhu Z.-K., Yang Y., Yin J., Qi Z.-N. Preparation and properties of organosoluble polyimide/silica hybrid materials by sol-gel process. J. Appl. Polym. Sci. 73:1999;2977-2984.
15. Wu K.H., Chang T.C., Wang Y.T., Chiu Y.S. Organic-inorganic hybrid materials. Part I. Characterization and degradation of poly(imide-silica) hybrids. J. Polym. Sci. Polym. Chem. 37:1999;2275-2284.
16. Hsiue G.-H., Chen J.-K., Liu Y.L. Synthesis and characterization of nanocomposite of polyimide-silica hybrid from nonaqueous sol-gel process. J. Appl. Polym. Sci. 76:2000;1609-1618.
17. Huang J.-C., Zhu Z.-K., Yin J., Zhang D.-M., Qian X.-F. Preparation and properties of rigid-rod polyimide/silica hybrid materials by sol-gel process. J. Appl. Polym. Sci. 79:2001;794-800.
18. Chen Y., Iroh J.O. Synthesis and characterization of polyimide/silica hybrid composites. Chem. Mater. 11:1999;1218-1222.
19. Joly C., Goizet S., Schrotter J.C., Sanchez J., Escoubes M. Sol-gel polyimide-silica composite membrane: gas transport properties. J. Membr. Sci. 130:1997;63-74.
20. Nunes S.P., Peinemann K.V., Ohlrogge K., Alpers A., Keller M., Pires A.T.N. Membrane of poly(ether imide) and nanodispersed silica. J. Membr. Sci. 157:1999;219-226.
21. 2 separation. J. Membr. Sci. 115:1996;65-75.
22. Smaihi M., Schrotter J.-C., Lesimple C., Prevost I., Guizard C. Gas separation properties of hybrid imide-siloxane copolymers with various silica contents. J. Membr. Sci. 161:1999;157-170.
23. Joly C., Smaihi M., Porcar L., Noble R.D. Polyimide-silica composite materials: how does silica influence their microstructure and gas permeation properties. Chem. Mater. 11:1999;2331-2338.
24. Zhong S.-H., Li C.-F., Xiao X.-F. Preparation and characterization of polyimide-silica hybrid membranes on kieselguhr-mullite supports. J. Membr. Sci. 199:2002;53-58.
25. Yeom S.-H., Chung Y.-S., Lee W.-T., Kim S.-I., Kim J.-H. Preparation and gas permeation properties of polyimide-silica hybrid membranes. Membr. J. (Korea). 11(3):2001;116-123.
26. Barrer R.M. Permeation, diffusion and solution of gases in organic polymers. Trans. Faraday Soc. 35:1939;628-643.
27. R.M. Felder, G.S. Huvard, Permeation, diffusion, and sorption of gases and vapors, in: L. Marton, C. Marton (Eds.), Methods of Experimental Physics, Academic Press, New York, 1980, pp. 315-378.
28. Park H.B., Kim C.K., Lee Y.M. Gas separation properties of polysiloxane/polyether mixed soft segment urethane urea membranes. J. Membr. Sci. 204:2002;257.
29. Park H.B., Ha S.Y., Lee Y.M. Percolation behavior of gas permeability in rigid-flexible block copolymer membranes. J. Membr. Sci. 177:2000;143.
30. Han H., Gryte C.C., Ree M. Water diffusion and sorption in films of high performance poly(4,4′-oxydiphenylene pyromellitimide): effects of humidity, imidization history and film thickness. Polymer. 36:1995;1663.
31. Ouyang M., Yuan C., Muisener R.J., Boulares A., Koberstein J.T. Conversion of some siloxane polymers to silicon oxide by UV/ozone photochemical processes. Chem. Mater. 12:2000;1591-1596.
32. Feng J., Weng L.-T., Chan C.-M., Xhie J., Li L. Imaging of sub-surface nano particles by tapping-mode atomic force microscopy. Polymer. 42:2001;2259-2262.
33. Zhao J., Rojstaczer S.R., Chen J., Xu M., Gardella J.A. Jr. Effect of siloxane segment length on the surface composition of poly(imidesiloxane) copolymers and its role in adhesion. Macromolecules. 32:1999;455-461.
34. Ha S.Y., Park H.B., Lee Y.M. Percolational effect of siloxane content in poly(amideimide siloxane) on the gas permeation behavior. Macromolecules. 32:1999;2394-2396.
35. Lee Y.B., Park H.B., Shim J.K., Lee Y.M. Synthesis and characterization of polyamideimide-branched siloxane and its gas-separation. J. Appl. Polym. Sci. 74:1999;965-973.
36. Ha S.Y., Oh B.K., Lee Y.M. Preparation of poly(amideimide siloxane) from trimellitic anhydride chloride. Polymer. 36(18):1995;3549-3553.