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All the solutions in either the pure or the mixed solvents used in this work were kept in this narrow window of concentrations for the purpose of comparison.
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note
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The two solvents of THF and methanol are well-mixed by vigorous, shaking, and the solutions are allowed to take enough time to reach equilibriums. The images shown in Figures 2 and 3 are thus the final morphological structures formed by the well-equilibrated solutions at the specific solvent compositions.
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0041305677
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note
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Immediately deposited onto mica and imaged by AFM after admixing the added THF solvent with the methanol solution by quick and vigorous shaking.
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0 = 0.1 M and [cat.] = 1 mM. For details on the polymerization of 4-ethynylbenzolyl-L-leucine methyl ester, see ref 11.
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