Pulse error compensating symmetric magic-echo trains

Journal of Magnetic Resonance

Volumn 161, Issue 2, 2003, Pages 132-137

  Boutis, G S ^a   Cappellaro, P ^a   Cho, H ^a   Ramanathan, C ^a   Cory, D G ^a  

^a Massachusetts Institute of Technology Cambridge   (United States)

Author keywords

Dipolar coupling; Finite pulse errors; Line narrowing; Magic echo; Time reversal

Indexed keywords

CALCIUM COMPOUNDS; ERROR COMPENSATION; HAMILTONIANS; IMAGING TECHNIQUES; SINGLE CRYSTALS;

MAGIC-ECHO TRAINS;

ECHO SUPPRESSION;

EID: 0041993668     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1016/S1090-7807(03)00010-7     Document Type: Article

References (31)

1. Haeberlen U., Waugh J.S. Coherent averaging effects in magnetic resonance. Phys. Rev. 175:1968;453-467.
2. Mansfield P., Orchard M.J., Stalker D.C., Richards K.H.B. Symmetrized multipulse nuclear-magnetic-resonance experiments in solids: measurement of the chemical-shift shielding tensor in some compounds. Phys. Rev. B. 7:1973;90-105.
3. Rhim W.-K., Elleman D.D., Vaugan R.W. Enhanced resolution for solid-state NMR. J. Chem. Phys. 58:1973;1772-1773.
4. Waugh J.S., Huber L.M., Haeberlen U. Approach to high-resolution NMR in solids. Phys. Rev. Lett. 20:1968;180-182.
5. Takegoshi K., McDowell C.A. A magic echo pulse sequence for the high-resolution NMR spectra of abundant spins in solids. Chem. Phys. Lett. 116:1985;100-104.
6. Matsui S. Suppressing the zero-frequency artifact in magic-sandwich-echo proton images of solids. J. Magn. Reson. 98:1992;618-621.
7. Rhim W.-K., Pines A., Waugh J.S. Time-reversal experiments in dipolar-coupled spin systems. Phys. Rev. B. 3:1971;684-696.
8. Matsui S. Solid-state NMR imaging by magic sandwich echoes. Chem. Phys. Lett. 179:1991;187-190.
9. Haeberlen U. High Resolution NMR in Solids: Selective Averaging. 1976;Academic Press, New York.
10. Matti Maricq M. Application of average Hamiltonian theory to the NMR of solids. Phys. Rev. B. 25:1982;6622-6632.
11. Matsui S., Ogasawara Y., Inouye T. Proton images of elastomers by solid-state NMR imaging. J. Magn. Reson. A. 105:1993;215-218.
12. Matsui S., Uraoka A., Inouye T. Improved resolution in solid-state NMR imaging by self-phase encoding. J. Magn. Reson. A. 112:1995;130-133.
13. Matsui S., Uraoka A., Inouye T. Solid-state NMR imaging by tetrahedral-magic-echo time-suspension sequences. J. Magn. Reson. A. 120:1996;11-17.
14. Matsui S., Saito S. Symmetric echo acquisition for absolute-value display in solid-state NMR imaging. J. Magn. Reson. 149:2001;103-109.
15. Hepp M.A., Miller J.B. Mapping molecular-orientation by solid-state NMR imaging. J. Magn. Reson. A. 111:1994;62-69.
16. Zhang W., Cory D.G. First direct measurement of the spin diffusion rate in a homogenous solid. Phys. Rev. Lett. 80:1998;1324-1327.
17. Wang C.H., Ramshaw J.D. Decay of multiple spin echoes in dipolar solids. Phys. Rev. B. 6:1972;3253-3262.
18. Burum D.P., Rhim W.K. Analysis of multiple pulse NMR in solids. III. J. Chem. Phys. 71:1979;944-956.
19. Burum D.P., Linder M., Ernst R.R. A new "Tune-Up" NMR pulse cycle for minimizing and characterizing phase transients. J. Magn. Reson. 43:1981;463-471.
20. Gerstein B.C., Dybowski C.R. Transient Techniques in NMR of Solids. 1985;Academic Press, New York.
21. Idziak S., Haeberlen U. Design and construction of a high homogeneity RF coil for solid-state multiple-pulse NMR. J. Magn. Reson. 50:1982;281-288.
22. Levitt M., Freeman R., Frenkiel T. Supercycles for broad-band heteronuclear decoupling. J. Magn. Reson. 50:1982;157-160.
23. Shaka A.J., Keeler J., Freeman R. Evaluation of a new broad-band decoupling sequence - WALTZ-16. J. Magn. Reson. 53:1983;313-340.
24. Waugh J.S. Theory of broad-band spin decoupling. J. Magn. Reson. 50:1982;30-49.
25. Levitt M., Freeman R., Frenkiel T. Broad-band heteronuclear decoupling. J. Magn. Reson. 47:1982;328-330.
26. Waugh J.S. Systematic procedure for constructing broad-band decoupling sequences. J. Magn. Reson. 49:1982;517-521.
27. Matsui S., Muira H. H-1-C-13 cross-polarization using a modified magic echo sequence for H-1 spin locking. Chem. Phys. Lett. 242:1995;163-168.
28. Hohwy M., Nielson N.C. High-order truncation in multiple pulse NMR. J. Chem. Phys. 106:1997;7571-7586.
29. Conradi M.S., Garroway A.N., Cory D.G., Miller J.B. Generation of short, intense gradient pulses. J. Magn. Reson. 94:1991;370-375.
30. Cory D.G. Solid state NMR imaging. Ann. Rep. NMR Spect. 24:1992;87-180.
31. Pines A., Waugh J.S. Quantitative aspects of coherent averaging. simple treatment of resonance offset processes in multiple-pulse NMR. J. Magn. Reson. 8:1972;354-365.