High-throughput screening of selectivity of melt polymerization catalysts using fluorescence spectroscopy and two-wavelength fluorescence imaging

Analytical Chemistry

Volumn 75, Issue 17, 2003, Pages 4676-4681

  Potyrailo, Radislav A ^a   Lemmon, John P ^a   Leib, Terry K ^a  

^a GENERAL ELECTRIC COMPANY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

FLUORESCENCE EMISSION;

CATALYSTS; CHARGE COUPLED DEVICES; IMAGING TECHNIQUES; MOLECULAR WEIGHT; PHENOLS;

POLARIZATION;

4,4' ISOPROPYLIDENEDIPHENOL; POLYCARBONATE; POLYMER; SOLVENT;

ARTICLE; CATALYST; CHEMICAL ANALYSIS; COMBINATORIAL CHEMISTRY; CROSS LINKING; FILTER; FLUORESCENCE SPECTROSCOPY; MELTING POINT; MOLECULAR WEIGHT; POLYMERIZATION; QUANTITATIVE ANALYSIS; SYNTHESIS;

EID: 0041837188     PISSN: 00032700     EISSN: None     Source Type: Journal    
DOI: 10.1021/ac034296d     Document Type: Article

References (48)

1. Malhotra, R., Ed. Combinatorial Approaches to Materials Development; American Chemical Society: Washington, DC, 2002.
2. Takeuchi, I., Newsam, J. M., Wille, L. T., Koinuma, H., Amis, E. J., Eds. Combinatorial and Arficial Intelligence Methods in Materials Science; Materials Research Society: Warrendale, PA, 2002.
3. Schlögl, R. Angew. Chem., Int. Ed. 1998, 37, 2333-2336.
4. Crabtree, R. H. Chem. Commun. 1999, 1611-1616.
5. Holzwarth, A.; Schmidt, H.-W.; Maier, W. Angew. Chem., Int. Ed. 1998, 37, 2644-2647.
6. Connolly, A. R.; Sutherland, J. D. Angew. Chem., Int. Ed. 2000, 39, 4268-4271.
7. Senkan, S. M. Nature 1998, 394, 350-353.
8. Su, H.; Yeung, E. S. J. Am. Chem. Soc. 2000, 122, 7422-7423.
9. Snively, C. M.; Oskarsdottir, G.; Lauterbach, J. Angew. Chem., Int. Ed. 2001, 40, 3028-3030.
10. Taylor, S. J.; Morken, J. P. Science 1998, 280, 267-270.
11. Reddington, E.; Sapienza, A.; Gurau, B.; Viswanathan, R.; Sarangapani, S.; Smotkin, E. S.; Mallouk, T. E. Science 1998, 280, 1735-1737.
12. Busch, O. M.; Hoffmann, C.; Johann, T. R. F.; Schmidt, H.-W.; Strehlau, W.; Schüth, F. J. Am. Chem. Soc. 2002, 124, 13527-13532.
13. Morris, N. D.; Mallouk, T. E. J. Am. Chem. Soc. 2002, 124, 11114-11121.
14. Brocchini, S.; James, K.; Tangpasuthadol, V.; Kohn, J. J. Am. Chem. Soc. 1997, 119, 4553-4554.
15. Boussie, T. R.; Coutard, C.; Turner, H.; Murphy, V.; Powers, T. S. Angew. Chem., Int. Ed. 1998, 37, 3272-3275.
16. Klaerner, G.; Safir, A. L.; Chang, H.-T.; Petro, M.; Nielsen, R. B. Polym. Prepr. 1999, 40, 469.
17. Bosman, A. W.; Heumann, A.; Klaerner, G.; Benoit, D.; Frechet, J. M. J.; Hawker, C. J. J. Am. Chem. Soc. 2001, 123, 6461-6462.
18. Komon, Z. J. A.; Diamond, G. M.; Leclerc, M. K.; Murphy, V.; Okazaki, M. ; Bazan, G. C. J. Am. Chem. Soc. 2002, 124, 15280-15285.
19. Pasch, H.; Kilz, P. Macromol. Rapid Commun. 2003, 24, 104-108.
20. Tian, J.; Coates, G. W. Angew. Chem., Int. Ed. 2000, 39, 3626-3629.
21. Stork, M.; Herrmann, A.; Nemnich, T.; Klapper, M.; Müllen, K. Angew. Chem., Int. Ed. 2000, 39, 4367-4369.
22. Belu, A. M.; Brocchini, S.; Kohn, J.; Ratner, B. D. Rapid Commun. Mass Spectrom. 2000, 14, 564-571.
23. Pijpers, T. F. J.; Mathot, V. B. F.; Goderis, B.; van der Vegte, E. Proc. NATAS Annu. Conf. Therm. Anal. Appl. 2000, 28.
24. Tuchbreiter, A.; Marquardt, J.; Zimmermann, J.; Walter, P.; Mülhaupt, R.; Kappler, B.; Faller, D.; Roths, T.; Honerkamp, J. J. Comb. Chem. 2001, 3, 598-603.
25. Gabriel, C.; Lilge, D.; Kristen, M. O. Macromol. Rapid Commun. 2002, 24, 109-112.
26. Potyrailo, R. A.; Wroczynski, R. J.; Lemmon, J. P.; Flanagan, W. P.; Siclovan, O. P. J. Comb. Chem. 2003, 5, 8-17.
27. Potyrailo, R. A. In Encyclopedia of Materials: Science and Technology; Buschow, K. H. J., Cahn, R. W., Flemings, M. C., Ilschner, B., Kramer, E. J., Mahajan, S., Eds.; Elsevier: Amsterdam, The Netherlands, 2001; Vol. 2, pp 1329-1343.
28. Gachkovskii, V. F. Vysokomol. Soedin. 1965, 7, 2199-2205 (English).
29. Morawetz, H. Science 1979, 203, 405-410.
30. Chipalkatti, M. H.; Laski, J. J. In Structure-Property Relations in Polymers. Spectroscopy and Performance; Urban, M. W., Craver, C. D., Eds.; Advances in Chemistry 236; American Chemical Society: Washington, DC, 1993; pp 623-642.
31. Barashkov, N. N.; Gunder, O. A. Fluorescent Polymers; Ellis Horwood: New York, 1994.
32. LeGrand, D. G., Bendler, J. T., Eds. Handbook of Polycarbonate Science and Technology; Marcel Dekker: New York, 2000.
33. King, J. A., Jr. In Solvent-Free Polymerizations and Processes. Minimization of Conventional Organic Solvents; Long, T. E., Hunt, M. O., Eds.; ACS Symposium Series 713; American Chemical Society: Washington, DC, 1998; pp 49-77.
34. Factor, A. In Polymer Durability. Degradation, Stabilization, and Lifetime Prediction; Clough, R. L., Billingham, N. C., Gillen, K. T., Eds.; Advances in Chemistry Series 249; American Chemical Society: Washington, DC, 1996; pp 59-76.
35. Brunelle, D. J.; Boden, E. P.; Shannon, T. G. J. Am. Chem. Soc. 1990, 112, 2399-2402.
36. Carnahan, J. C.; Lemmon, J. P.; Potyrailo, R. A.; Leib, T. K.; Warner, G. L. Method for parallel melt-polymerization. U.S. Patent 6,307,004 B1, 2001.
37. Potyrailo, R. A.; Lemmon, J. P. Method for direct measurement of polycarbonate compositions by fluorescence. U.S. Patent 6,193,850, 2001.
38. Carr-Brion, K. G.; Clarke, J. R. P. Sampling Systems for Process Analyzers: Butterworth-Heinemann: Oxford, England, 1996.
39. ASTM E 1655-97, Standard Practices for Infrared, Multivariate, Quantitative Analysis; ASTM: West Conshohocken. PA. 1997.
40. Spivack, J. L.; Cawse, J. N.; Whisenhunt, D. W., Jr.; Johnson, B. F.; Shalyaev, K. V.; Male, J.; Pressman, E. J.; Ofori, J.; Soloveichik, G.; Patel, B. P.; Chuck, T. L.; Smith, D. J.; Jordan, T. M.; Brennan, M. R.; Kilmer, R. J. ; Williams, E. D. Appl. Catal., A 2003, ASAP Article.
41. Potyrailo, R. A.; Lemmon, J. P.; Leib, T. K. Aromatic polycarbonate characterization. U.S. Patent 6,541,264 B1, 2003.
42. Potyrailo, R. A.; May, R. J.; Shaffer, R. E.; Lemmon, J. P.; Wroczynski, R. J. Method for high-throughput fluorescence screening of polymerization reactions. U.S. Patent 6,589,788 B1, 2003.
43. Lettmann, C.; Hinrichs, H.; Maier, W. F. Angew. Chem., Int. Ed. 2001, 40, 3160-3164.
44. Potyrailo, R. A.; Lemmon, J. P.; Flanagan, W. P.; Johnson, R. N. Method and apparatus for high-throughput chemical screening: U.S. Patent 6,572,-828 B1, 2003.
45. Hwang, I.-W.; Song, N. W.; Kim, D.; Park, Y. T.; Kim, Y.-R. J. Polym. Sci., B 1999, 37, 2901-2908.
46. Nango, M.; Kimura, Y.; Ihara, Y.; Kuroki, N. Macromolecules 1988, 21, 2330-2335.
47. Lee, H. J.; Nakayama, Y.; Matsuda, T. Macromolecules 1999, 32. 6989-6995.
48. Evans, C. A.; Miller, S. J. Curr. Opin. Chem. Biol. 2002, 6, 333-338.