Evaluation of the performance of 2D 1H PFG absorption mode DQ spectroscopy in the analysis of chemical and biological molecules

Magnetic Resonance in Chemistry

Volumn 36, Issue 9, 1998, Pages 670-680

  Dalvit, Claudio ^a   Böhlen, Jean Marc ^b  

^a NOVARTIS PHARMA AG   (Switzerland)

^b Bruker AG   (Switzerland)

Author keywords

1H NMR; Double quantum; Flip angle dependence; NMR; Pulsed field gradients; Sensitivity; Solvent suppression

Indexed keywords

BIOCHIPS; WATER ABSORPTION;

1H NMR; ANGLE DEPENDENCE; CHEMICAL AND BIOLOGICALS; DOUBLE-QUANTUM; FLIP ANGLE; FLIP-ANGLE DEPENDENCE; PERFORMANCE; PULSED FIELD GRADIENTS; SENSITIVITY; SOLVENT SUPPRESSION;

CELL CULTURE;

EID: 0040674822     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/(sici)1097-458x(199809)36:9<670::aid-omr356>3.0.co;2-s     Document Type: Article

References (53)

1. K. Wüthrich, NMR of Proteins and Nucleic Acids, Wiley, New York (1986).
2. I. Bertini and C. Luchinat, NMR of Paramagnetic Molecules in Biological Systems. Benjamin/Cummings, Menlo Park, CA (1986).
3. J. Cavanagh, W. J. Fairbrother, A G. Palmer, III and N. J. Skelton, Protein NMR Spectroscopy. Academic Press, New York (1996).
4. C. Dalvit and J. M. Böhlen, J. Magn. Reson. B 111, 76 (1996).
5. C. Dalvit and J. M. Böhlen, J. Magn. Reson. B 113, 195 (1996).
6. T. H. Mareci and R. Freeman, J. Magn. Reson. 51, 531 (1983).
7. L. Braunschweiler, G. Bodenhausen and R. R. Ernst, Mol. Phys. 48, 535 (1983).
8. M. Rance and P. E. Wright, J. Magn. Reson. 66, 372 (1986).
9. T. J. Norwood, Prog. Nucl. Magn. Reson. Spectrosc. 24, 295 (1992).
10. M. Rance, O. W. Sørensen, G. Bodenhausen, G. Wagner, R. R. Ernst and K. Wüthrich, Biochem. Biophys. Res. Commun. 117, 479 (1983).
11. C. H. Sotak, D. M. Freeman and R. E. Hurd, J. Magn. Reson. 78, 355 (1988).
12. R. E. Hurd and D. M. Freeman, Proc. Natl. Acad. Sci. USA 86, 4402 (1989).
13. W. Nosel, L. A. Trimble, J. F. Shen and P. S. Allen, Magn. Reson. Med. 11, 398 (1989).
14. J. Keeler, R. T. Clowes, A. L. Davis and E. D. Laue, Methods Enzymol. 239, 145 (1994).
15. D. J. States, R. A. Haberkorn and D. J. Ruben, J. Magn. Reson. 48, 286 (1982).
16. J. Balbach and H. Kessler, J. Magn. Reson. B 105, 83 (1994).
17. D. Marion and K. Wüthrich, Biochem. Biophys. Res. Commun. 113, 967 (1983).
18. M. McCoy and W. S. Warren, J. Chem Phys. 93, 858 (1990).
19. R. Bowtell, R. M. Bowley and P. Glover, J. Magn. Reson. 88, 643 (1990).
20. D. Abergel, M. A. Delsuc and J. Y. Lallemand, J. Chem. Phys. 96, 1657 (1992).
21. W. S. Warren, Q. He, M. McCoy and F. C. Spano, J. Chem. Phys. 96, 1659 (1992).
22. W. S. Warren, W. Richter, A. H. Andreotti and B. T. Farmer, II, Science 262, 2005 (1993).
23. R. Bowtell and A. Peters, J. Magn. Reson. A. 115, 55 (1995).
24. S. Lee, W. Richter, S. Vathyam and W. S. Warren, J. Chem. Phys. 105, 874 (1996).
25. P. Broekaert, A. Vlassebroek, J. Jeener, G. Lippens and J. M. Wieruszeski, J. Magn. Reson. A. 120, 97 (1996).
26. M. Levitt, Concepts Magn. Reson. 8, 77 (1996).
27. C. Dalvit and J. M. Böhlen, J. Magn. Reson. 126, 149 (1997).
28. G. Bodenhausen, R. Freeman and D. L. Turner, J. Magn. Reson. 27, 511 (1977).
29. A. Bax and S. S. Pochapsky, J. Magn. Reson. 99, 638 (1992).
30. C. Dalvit and J. M. Böhlen, Magn. Reson. Chem. 34, 829 (1996).
31. C. Dalvit and J. M. Böhlen, NMR Biomed. 10, 285 (1997).
32. T. H. Mareci and R. Freeman, J. Magn. Reson. 48, 158 (1982).
33. N. C. Nielsen, H. Thøgersen and O. W. Sørensen, J. Am. Chem. Soc. 117, 11365 (1995).
34. R. R. Ernst, G. Bodenhausen and A. Wokaun, Principles of Nuclear Magnetic Resonance in One and Two Dimensions. Clarendon Press, Oxford (1987).
35. C. Dalvit, J. Magn. Reson. B 112, 282 (1996).
36. G. Kontaxis, J. Stonehouse, E. D. Laue and J. Keeler, J. Magn. Reson. A 111, 70 (1994).
37. D. Canet and M. Decorps, in Dynamics of Solutions and Fluid Mixture by NMR, edited by J. J. Delpuech, p. 310. Wiley, New York (1995).
38. T. Parella, Magn. Reson. Chem. 34, 329 (1996).
39. P. C. M. Van Zijl, M. O. Johnson, S. Mori and R. E. Hurd, J. Magn. Reson. A 113, 265 (1995).
40. D. L. Mattiello, W. S. Warren, L. Müller and B. T. Farmer, II, J. Am. Chem. Soc. 118, 3253 (1996).
41. A. L. Davis, E. D. Laue, J. Keeler, D. Moskau and J. Lohman, J. Magn. Reson. 94, 637 (1991).
42. L. Braunschweiler and R. R. Ernst, J. Magn. Reson. 53, 521 (1983).
43. A. Bax and D. G. Davis, J. Magn. Reson. 65, 355 (1985).
44. M. Piotto, V. Saudek and V. Sklenar, J. Biomol. NMR 2, 661 (1992).
45. O. W. Sørensen, M. Rance and R. R. Ernst, J. Magn. Reson. 56, 527 (1984).
46. A. L. Davis, G. Estcourt, J. Keeler, E. D. Laue and J. J. Titman, J. Magn. Reson. A 105, 167 (1993).
47. C. Griesinger, G. Otting, K. Wüthrich and R. R. Ernst, J. Am. Chem. Soc. 110, 7870 (1988).
48. M. Rance, O. W. Sørensen, W. Leupin, H. Kogler, K. Wüthrich and R. R. Ernst, J. Magn. Reson. 61, 67 (1985).
49. A. Jerschow and N. Müller, J. Magn. Reson. A 123, 222 (1996).
50. M. Liu, J. K. Nicholson and J. C. Lindon, Anal. Chem. 68, 3370 (1996).
51. M. Lin and M. J. Shapiro, J. Org. Chem. 61, 7617 (1996).
52. N. Birlirakis and G. Guittet, J. Am. Chem. Soc. 118, 13083 (1996).
53. C. Redfield and C. M. Dobson, Biochemistry 27, 122 (1988).