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Volumn 122, Issue 3, 2000, Pages 525-531

The elusive formaldonitrone, CH2=N(H)-O. Preparation in the gas phase and characterization by variable-time neutralization-reionization mass spectrometry, and ab initio and density functional theory calculations

Author keywords

[No Author keywords available]

Indexed keywords

NITRONE DERIVATIVE;

EID: 0039838613     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja993234v     Document Type: Article
Times cited : (14)

References (85)
  • 29
    • 0000485933 scopus 로고
    • For reviews see: (a) Wesdemiotis, C.; McLafferty, F. W. Chem. Rev. 1987, 87, 485. (b) Terlouw, J. K.; Schwarz, H. Angew. Chem., Int. Ed. Engl. 1987, 26, 805. Holmes, J. L. Mass Spectrom. Rev. 1989, 8, 513. Terlouw, J. K. Adv. Mass Spectrom. 1989, 11, 984. (e) McLafferty, F. W. Science 1990, 247, 925. (f) Turecek, F. Org. Mass Spectrom. 1992, 27, 1087. (g) Goldberg, N.; Schwarz, H. Acc. Chem. Res. 1994, 27, 347. (h) Schalley, C. A.; Hornung, G.; Schroder, D.; Schwarz, H. Chem. Soc. Rev. 1998, 27, 91. Turecek, F. J. Mass Spectrom. 1998, 33, 779.
    • (1987) Chem. Rev. , vol.87 , pp. 485
    • Wesdemiotis, C.1    McLafferty, F.W.2
  • 30
    • 84985580763 scopus 로고
    • For reviews see: (a) Wesdemiotis, C.; McLafferty, F. W. Chem. Rev. 1987, 87, 485. (b) Terlouw, J. K.; Schwarz, H. Angew. Chem., Int. Ed. Engl. 1987, 26, 805. Holmes, J. L. Mass Spectrom. Rev. 1989, 8, 513. Terlouw, J. K. Adv. Mass Spectrom. 1989, 11, 984. (e) McLafferty, F. W. Science 1990, 247, 925. (f) Turecek, F. Org. Mass Spectrom. 1992, 27, 1087. (g) Goldberg, N.; Schwarz, H. Acc. Chem. Res. 1994, 27, 347. (h) Schalley, C. A.; Hornung, G.; Schroder, D.; Schwarz, H. Chem. Soc. Rev. 1998, 27, 91. Turecek, F. J. Mass Spectrom. 1998, 33, 779.
    • (1987) Angew. Chem., Int. Ed. Engl. , vol.26 , pp. 805
    • Terlouw, J.K.1    Schwarz, H.2
  • 31
    • 84994943974 scopus 로고
    • For reviews see: (a) Wesdemiotis, C.; McLafferty, F. W. Chem. Rev. 1987, 87, 485. (b) Terlouw, J. K.; Schwarz, H. Angew. Chem., Int. Ed. Engl. 1987, 26, 805. Holmes, J. L. Mass Spectrom. Rev. 1989, 8, 513. Terlouw, J. K. Adv. Mass Spectrom. 1989, 11, 984. (e) McLafferty, F. W. Science 1990, 247, 925. (f) Turecek, F. Org. Mass Spectrom. 1992, 27, 1087. (g) Goldberg, N.; Schwarz, H. Acc. Chem. Res. 1994, 27, 347. (h) Schalley, C. A.; Hornung, G.; Schroder, D.; Schwarz, H. Chem. Soc. Rev. 1998, 27, 91. Turecek, F. J. Mass Spectrom. 1998, 33, 779.
    • (1989) Mass Spectrom. Rev. , vol.8 , pp. 513
    • Holmes, J.L.1
  • 32
    • 0001084538 scopus 로고
    • For reviews see: (a) Wesdemiotis, C.; McLafferty, F. W. Chem. Rev. 1987, 87, 485. (b) Terlouw, J. K.; Schwarz, H. Angew. Chem., Int. Ed. Engl. 1987, 26, 805. Holmes, J. L. Mass Spectrom. Rev. 1989, 8, 513. Terlouw, J. K. Adv. Mass Spectrom. 1989, 11, 984. (e) McLafferty, F. W. Science 1990, 247, 925. (f) Turecek, F. Org. Mass Spectrom. 1992, 27, 1087. (g) Goldberg, N.; Schwarz, H. Acc. Chem. Res. 1994, 27, 347. (h) Schalley, C. A.; Hornung, G.; Schroder, D.; Schwarz, H. Chem. Soc. Rev. 1998, 27, 91. Turecek, F. J. Mass Spectrom. 1998, 33, 779.
    • (1989) Adv. Mass Spectrom. , vol.11 , pp. 984
    • Terlouw, J.K.1
  • 33
    • 0025064024 scopus 로고
    • For reviews see: (a) Wesdemiotis, C.; McLafferty, F. W. Chem. Rev. 1987, 87, 485. (b) Terlouw, J. K.; Schwarz, H. Angew. Chem., Int. Ed. Engl. 1987, 26, 805. Holmes, J. L. Mass Spectrom. Rev. 1989, 8, 513. Terlouw, J. K. Adv. Mass Spectrom. 1989, 11, 984. (e) McLafferty, F. W. Science 1990, 247, 925. (f) Turecek, F. Org. Mass Spectrom. 1992, 27, 1087. (g) Goldberg, N.; Schwarz, H. Acc. Chem. Res. 1994, 27, 347. (h) Schalley, C. A.; Hornung, G.; Schroder, D.; Schwarz, H. Chem. Soc. Rev. 1998, 27, 91. Turecek, F. J. Mass Spectrom. 1998, 33, 779.
    • (1990) Science , vol.247 , pp. 925
    • McLafferty, F.W.1
  • 34
    • 84989093057 scopus 로고
    • For reviews see: (a) Wesdemiotis, C.; McLafferty, F. W. Chem. Rev. 1987, 87, 485. (b) Terlouw, J. K.; Schwarz, H. Angew. Chem., Int. Ed. Engl. 1987, 26, 805. Holmes, J. L. Mass Spectrom. Rev. 1989, 8, 513. Terlouw, J. K. Adv. Mass Spectrom. 1989, 11, 984. (e) McLafferty, F. W. Science 1990, 247, 925. (f) Turecek, F. Org. Mass Spectrom. 1992, 27, 1087. (g) Goldberg, N.; Schwarz, H. Acc. Chem. Res. 1994, 27, 347. (h) Schalley, C. A.; Hornung, G.; Schroder, D.; Schwarz, H. Chem. Soc. Rev. 1998, 27, 91. Turecek, F. J. Mass Spectrom. 1998, 33, 779.
    • (1992) Org. Mass Spectrom. , vol.27 , pp. 1087
    • Turecek, F.1
  • 35
    • 0000346053 scopus 로고
    • For reviews see: (a) Wesdemiotis, C.; McLafferty, F. W. Chem. Rev. 1987, 87, 485. (b) Terlouw, J. K.; Schwarz, H. Angew. Chem., Int. Ed. Engl. 1987, 26, 805. Holmes, J. L. Mass Spectrom. Rev. 1989, 8, 513. Terlouw, J. K. Adv. Mass Spectrom. 1989, 11, 984. (e) McLafferty, F. W. Science 1990, 247, 925. (f) Turecek, F. Org. Mass Spectrom. 1992, 27, 1087. (g) Goldberg, N.; Schwarz, H. Acc. Chem. Res. 1994, 27, 347. (h) Schalley, C. A.; Hornung, G.; Schroder, D.; Schwarz, H. Chem. Soc. Rev. 1998, 27, 91. Turecek, F. J. Mass Spectrom. 1998, 33, 779.
    • (1994) Acc. Chem. Res. , vol.27 , pp. 347
    • Goldberg, N.1    Schwarz, H.2
  • 36
    • 0032371428 scopus 로고    scopus 로고
    • For reviews see: (a) Wesdemiotis, C.; McLafferty, F. W. Chem. Rev. 1987, 87, 485. (b) Terlouw, J. K.; Schwarz, H. Angew. Chem., Int. Ed. Engl. 1987, 26, 805. Holmes, J. L. Mass Spectrom. Rev. 1989, 8, 513. Terlouw, J. K. Adv. Mass Spectrom. 1989, 11, 984. (e) McLafferty, F. W. Science 1990, 247, 925. (f) Turecek, F. Org. Mass Spectrom. 1992, 27, 1087. (g) Goldberg, N.; Schwarz, H. Acc. Chem. Res. 1994, 27, 347. (h) Schalley, C. A.; Hornung, G.; Schroder, D.; Schwarz, H. Chem. Soc. Rev. 1998, 27, 91. Turecek, F. J. Mass Spectrom. 1998, 33, 779.
    • (1998) Chem. Soc. Rev. , vol.27 , pp. 91
    • Schalley, C.A.1    Hornung, G.2    Schroder, D.3    Schwarz, H.4
  • 37
    • 0031660730 scopus 로고    scopus 로고
    • For reviews see: (a) Wesdemiotis, C.; McLafferty, F. W. Chem. Rev. 1987, 87, 485. (b) Terlouw, J. K.; Schwarz, H. Angew. Chem., Int. Ed. Engl. 1987, 26, 805. Holmes, J. L. Mass Spectrom. Rev. 1989, 8, 513. Terlouw, J. K. Adv. Mass Spectrom. 1989, 11, 984. (e) McLafferty, F. W. Science 1990, 247, 925. (f) Turecek, F. Org. Mass Spectrom. 1992, 27, 1087. (g) Goldberg, N.; Schwarz, H. Acc. Chem. Res. 1994, 27, 347. (h) Schalley, C. A.; Hornung, G.; Schroder, D.; Schwarz, H. Chem. Soc. Rev. 1998, 27, 91. Turecek, F. J. Mass Spectrom. 1998, 33, 779.
    • (1998) J. Mass Spectrom. , vol.33 , pp. 779
    • Turecek, F.1
  • 55
    • 9344269016 scopus 로고
    • For the various frequency correction factors see, for example: (a) Rauhut, G.; Pulay. R. J. Phys. Chem. 1995, 99, 3093. (b) Finley, J. W.; Stephens, P. J. J. Mol Struct. (THEOCHEM) 1995, 227, 357. Wong. M. W. Chem. Phys. Lett. 1996, 256, 391. Scott, A. P.; Radom, L. J. Phys. Chem. 1996, 100, 16502.
    • (1995) J. Phys. Chem. , vol.99 , pp. 3093
    • Pulay, R.1
  • 56
    • 9344269016 scopus 로고
    • For the various frequency correction factors see, for example: (a) Rauhut, G.; Pulay. R. J. Phys. Chem. 1995, 99, 3093. (b) Finley, J. W.; Stephens, P. J. J. Mol Struct. (THEOCHEM) 1995, 227, 357. Wong. M. W. Chem. Phys. Lett. 1996, 256, 391. Scott, A. P.; Radom, L. J. Phys. Chem. 1996, 100, 16502.
    • (1995) J. Mol Struct. (THEOCHEM) , vol.227 , pp. 357
    • Finley, J.W.1    Stephens, P.J.2
  • 57
    • 0030570305 scopus 로고    scopus 로고
    • For the various frequency correction factors see, for example: (a) Rauhut, G.; Pulay. R. J. Phys. Chem. 1995, 99, 3093. (b) Finley, J. W.; Stephens, P. J. J. Mol Struct. (THEOCHEM) 1995, 227, 357. Wong. M. W. Chem. Phys. Lett. 1996, 256, 391. Scott, A. P.; Radom, L. J. Phys. Chem. 1996, 100, 16502.
    • (1996) Chem. Phys. Lett. , vol.256 , pp. 391
    • Wong, M.W.1
  • 58
    • 0011083273 scopus 로고    scopus 로고
    • For the various frequency correction factors see, for example: (a) Rauhut, G.; Pulay. R. J. Phys. Chem. 1995, 99, 3093. (b) Finley, J. W.; Stephens, P. J. J. Mol Struct. (THEOCHEM) 1995, 227, 357. Wong. M. W. Chem. Phys. Lett. 1996, 256, 391. Scott, A. P.; Radom, L. J. Phys. Chem. 1996, 100, 16502.
    • (1996) J. Phys. Chem. , vol.100 , pp. 16502
    • Scott, A.P.1    Radom, L.2
  • 63
    • 0342304134 scopus 로고    scopus 로고
    • note
    • 40 A reference ion was prepared from 2-propanol and its CAD and NR mass spectra were obtained for comparison.
  • 67
    • 0343173679 scopus 로고    scopus 로고
    • note
    • 2 = 0.66.
  • 69
    • 0343609177 scopus 로고    scopus 로고
    • note
    • NR) 45(13.2), 44(12.4), 43(13.0), 42(3.9), 41(0.8), 31(0.2), 30(3.8), 29(13.8), 28(6.8), 27(3.1), 26(5.8), 25(2.6), 24(0.9), 19(0.2), 18(0.5), 17(0.7), 16(1.2), 15(6.6), 14(4.7), 13(2.7), 12(2.1).
  • 70
    • 0342304131 scopus 로고    scopus 로고
    • note
    • -1 internal energy at 523 K.
  • 71
    • 0342739210 scopus 로고    scopus 로고
    • note
    • -1.20
  • 72
    • 0342304130 scopus 로고    scopus 로고
    • note
    • -1.20
  • 76
    • 0342739209 scopus 로고    scopus 로고
    • note
    • The error limits do not include the uncertainties in the experimental enthalpies of formation that were used to evaluate eqs 1-3.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.