Syntheses and structure of dimeric yttrium tris [bis(trimethylsilyl)phosphanide]; X-ray structures of [(thf)LiCl · (thf)2LiPtBu2]2 and Y [CH(SiMe3)2]3

Inorganica Chimica Acta

Volumn 269, Issue 1, 1998, Pages 91-100

  Westerhausen, Matthias ^a   Hartmann, Manfred ^a   Schwarz, Wolfgang ^b  

^a UNIVERSITY OF MUNICH   (Germany)

^b UNIVERSITY OF STUTTGART   (Germany)

Author keywords

Crystal structures; Lithium complexes; Phosphanide complexes; Yttrium complexes

Indexed keywords

AROMATIC HYDROCARBONS; ATOMS; CHLORINE COMPOUNDS; CRYSTAL STRUCTURE; LIGANDS; LITHIUM COMPOUNDS; NUCLEAR MAGNETIC RESONANCE; PHOSPHORUS;

BRIDGING LIGANDS; COUPLING CONSTANTS; CRYSTALLOGRAPHIC DATA; LITHIUM COMPLEX; METATHESIS REACTIONS; PHOSPHANIDE COMPLEXES; TETRAHYDROFURAN SOLUTION; YTTRIUM COMPLEXES;

YTTRIUM COMPOUNDS;

EID: 0039491387     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0020-1693(97)05776-9     Document Type: Article

References (81)

1. (a) M. Weterhausen, W. Schwarz, Z. Anorg. Allg. Chem., 604 (1991) 127;
2. (b) M. Westerhausen, W. Schwarz, Z. Anorg. Allg. Chem., 606 (1991) 177;
3. (c) B.A. Vaartstra, J.C. Huffman, W.E. Streib, K.G. Caulton, Inorg. Chem., 30 (1991) 121.
4. M. Westerhausen, W. Schwarz, Z. Anorg. Allg. Chem., 609 (1992) 39.
5. (a) H. Bürger, C. Forker, J. Goubeau, Monatsh. Chem., 96 (1965) 597;
6. (b) A.H. Clark, A. Haaland, J. Chem. Soc., Chem. Commun., (1969) 912;
7. (c) A.H. Clark, A. Haaland, Acta Chem. Scand., 24 (1970) 3024;
8. (d) H. Nöth, D. Schlosser, Inorg. Chem., 22 (1983) 2700.
9. J.S. Ghotra, M.B. Hursthouse, A.J. Welch, J. Chem. Soc., Chem. Commun., (1973) 669.
10. M. Westerhausen, M. Hartmann, A. Pfitzner, W. Schwarz, Z. Anorg. Allg. Chem., 621 (1995) 837.
11. (a) R. Anwander, W.A. Herrmann, Topics Curr. Chem., 179 (1996) 1;
12. (b) R. Anwander, Topics Curr. Chem., 179 (1996) 33.
13. (a) M. Westerhausen, W. Schwarz, Z. Naturforsch., Teil B, 47 (1992) 453;
14. (b) M. Westerhausen, H.-D. Hausen, Z. Anorg. Allg. Chem., 615 (1992) 27;
15. (c) M. Westerhausen, H.-D. Hausen, W. Schwarz, Z. Anorg. Allg. Chem., 618 (1992) 121;
16. (d) M. Westerhausen, W. Schwarz, Z. Anorg. Allg. Chem., 619 (1993) 1455.
17. M. Westerhausen, W. Schwarz, J. Organomet. Chem., 463 (1993) 51.
18. M. Westerhausen, J. Organomet. Chem., 479 (1994) 141.
19. M. Westerhausen, M. Hartmann, W. Schwarz, Inorg. Chem., 35 (1996) 2421.
20. G.W. Rabe, J. Riede, A. Schier, Organometallics, 15 (1996) 439.
21. M. Westerhausen, G. Lang, W. Schwarz, Chem. Ber., 129 (1996) 1035.
22. H.H. Karsch, G. Ferazin, H. Kooijman, O. Steigelmann, A. Schier, P. Bissinger, W. Hiller, J. Organomet. Chem., 482 (1994) 151.
23. (a) G.W. Rabe, J. Riede, A. Schier, J. Chem. Soc., Chem. Commun., (1995) 577;
24. (b) G.W. Rabe, G.P.A. Yap, A.L. Rheingold, Inorg. Chem., 34 (1995) 4521;
25. (c) G.W. Rabe, J.W. Ziller, Inorg. Chem., 34 (1995) 5378,
26. (d) G.W. Rabe, J. Riede, A. Schier, Inorg. Chem., 35 (1996) 40;
27. (e) G.W. Rabe, J. Riede, A. Schier, Inorg. Chem., 35 (1996) 2680.
28. (a) H. Wang, X. Zhou, J. Zhang, Y. Wang, Y. Hsia, R. Liu, S. Wang, New Front. Rare Earth Sci. Appl., Proc. Int. Conf. Rare Earth Dev. Appl., 1 (1985) 113;
29. (b) H.C. Aspinall, S.R. Moore, A.K. Smith, J. Chem. Soc. Dalton Trans., (1993) 993.
30. (a) M.D. Fryzuk, T.S. Haddad, J. Am. Chem. Soc., 110 (1988) 8263;
31. (b) P.B. Hitchcock, M.F. Lappert, I.A. MacKinnon, J. Chem. Soc., Chem. Commun., (1988) 1557;
32. (c) M.D. Fryzuk, T.S. Haddad, S.J. Rettig, Organometallics, 10 (1991) 2026;
33. (d) M.D. Fryzuk, T.S. Haddad amd S.J. Rettig, Organometallics, 11 (1992) 2967.
34. M. Schütze, Angew. Chem., 70 (1958) 697.
35. (a) K. Issleib, F. Krech, J. Organomet. Chem., 13 (1968) 283;
36. (b) L. Lochmann, D. Lim, J. Organomet. Chem., 28 (1971) 153;
37. (c) S.W. Hall, J.CC. Huffman, M.M. Miller, L.R. Avens, C.J. Burns, D.S.J. Arney, A.F. England, A.P. Sattelberger, Organometallics, 12 (1993) 752.
38. H.H. Karsch, F. Bienlein, T. Rupprich, F. Uhlig, E. Herrmann, M. Scheer, in W.A. Herrmann (ed.), Synthetic Methods of Organo-metallic and Inorganic Chemistry (Herrmann/Brauer), Vol. 3, Thieme, Stuttgart, p. 63, and Refs. therein.
39. (a) P.B. Hitchcock, M.F. Lappert, R.G. Smith, Inorg. Chim. Acta, 139 (1987) 183;
40. (b) M.F. Lappert, A. Singh, R.G. Smith, H.A. Stecher, A. Sen, Inorg. Synth., 27 (1990) 16.
41. C.J. Schaverien, A.G. Orpen, Inorg. Chem., 30 (1991) 4968.
42. T. Hahn (ed.), International Tables for Crystallography, Vol. A, Space Group Symmetry, Reidel, Dordrecht, 2nd edn., 1984.
43. SHELXTL PC, Siemens Analytical X-Ray Instruments Inc., 1990; SHELXTL Plus, Siemens Analytical X-Ray Instruments Inc., 1989.
44. SHELXTL PC, Siemens Analytical X-Ray Instruments Inc., 1990; SHELXTL Plus, Siemens Analytical X-Ray Instruments Inc., 1989.
45. G.M. Sheldrick, SHELXL-93, program for crystal structure determination, Universität Göttingen, Germany, 1993.
46. D.T. Cromer, J.B. Mann, Acta Crystallogr., Sect. A, 24 (1968) 321.
47. R.F. Stewart, E.R. Davidson, W.T. Simpson, J. Chem. Phys., 42 (1965) 3175.
48. F.E. Hahn, S. Rupprecht, Z. Naturforsch., Teil B, 46 (1991) 143.
49. (a) K. Gregory, P.V.R. Schleyer, R. Snaith, Adv. Inorg. Chem., 37 (1991) 47;
50. (b) R.E. Mulvey, Chem. Soc. Rev., 20 (1991) 167;
51. (c) F. Pauer, P.P. Power, in A.-M. Sapse, P.V.R. Schleyer (eds.), Lithium Chemistry: A Theoretical and Experimental Overview, Wiley, New York, 1995, p. 295.
52. C.L. Raston, C.R. Whitaker, A.H. White, J. Chem Soc., Dalton Trans., (1988) 991.
53. D. Barr, W. Clegg, R.E. Mulvey, R. Snaith, J. Chem. Soc., Chem. Commun., (1984) 79.
54. B. Werner, B. Neumüller, Z. Naturforsch., Teil B, 50 (1995) 1348.
55. G. Stieglitz, B. Neumüller, K. Dehnicke, Z. Naturforsch., Teil B, 48 (1993) 156.
56. E. Hey, P.B. Hitchcock, M.F. Lappert, A.K. Rai, J. Organomet. Chem., 325 (1987) 1.
57. (a) R.A. Jones, A.L. Stuart, T.C. Wright, J. Am. Chem. Soc., 105 (1983) 7459;
58. (b) G.W. Rabe, J. Riede, A. Schier, Acta Crystallogr., Sect. C, 52 (1996) 1350.
59. E. Hey-Hawkins, E. Sattler, J. Chem. Soc., Chem. Commun., (1992) 775.
60. P.B. Hitchcock, M.F. Lappert, R.G. Smith, R.A. Bartlett, P.P. Power, J. Chem. Soc., Chem. Commun., (1988) 1007.
61. M. Westerhausen, R. Löw, W. Schwarz, J. Organomet. Chem., 513 (1996) 213.
62. C.J. Marsden, B.A. Smart, Aust. J. Chem., 46 (1993) 749.
63. R.J.M. Konings, A.S. Booij, J. Mol. Struct, 271 (1992) 183.
64. M. Kaupp, P.V.R. Schleyer, J. Phys. Chem., 96 (1992) 7316.
65. T. Fjeldberg, R.A. Andersen, J. Mol. Struct., 128 (1985) 49.
66. P.B. Hitchcock, M.F. Lappert, A. Singh, J. Chem. Soc., Chem. Commun., (1983) 1499.
67. (a) D.H. Harris, M.F. Lappert, J. Organomet. Chem. Libr., 2 (1976) 13;
68. (b) P.G. Eller, D.C. Bradley, M.B. Hursthouse, D.W. Meek, Coord. Chem. Rev., 24 (1977) 1.
69. P. Berno, S. Gambarotta, J. Chem. Soc., Chem. Commun., (1994) 2419.
70. P.W. Wanandi, W.M. Davis, C.C. Cummins, J. Am. Chem. Soc., 117 (1995) 2110.
71. W.A. Herrmann, R. Anwander, F.C. Munck, W. Scherer, V. Dufaud, N.W. Huber, G.R.J. Artus, Z. Naturforsch. Teil B, 49 (1994) 1789.
72. T. Fjeldberg, R.A. Andersen, J. Mol. Struct., 129 (1985) 93.
73. H.A. Stecher, A. Sen, A.L. Rheingold, Inorg. Chem., 27 (1988) 1130.
74. R.A. Andersen, D.H. Templeton, A. Zalkin, Inorg. Chem., 17 (1978) 2317.
75. B. Cetinkaya, P.B. Hitchcock, M.F. Lappert, R.G. Smith, J. Chem. Soc., Chem. Commun., (1992) 932.
76. T.D. Tilley, R.A. Andersen, A. Zalkin, Inorg. Chem., 23 (1984) 2271.
77. (a) J.R.v.d. Hende, P.B. Hitchcock, M.F. Lappert, J. Chem. Soc., Chem. Commun., (1994) 1413;
78. (b) J.R.v.d. Hende, P.B. Hitchcock, S.A. Holmes, M.F. Lappert, J. Chem. Soc., Dalton Trans., (1995) 1435.
79. J.R.v.d. Hende, P.B. Hitchcock, M.F. Lappert, J. Chem. Soc., Dalton Trans., (1995) 2251.
80. R.A. Andersen, A. Zalkin, D.H. Templeton, Inorg. Chem., 20 (1981) 622.
81. W.G.v.d. Sluys, C.J. Burns, A.P. Sattelberger, Organometallics, 8 (1989) 855.