Octametallic and hexadecametallic ferric wheels

Angewandte Chemie - International Edition

Volumn 41, Issue 22, 2002, Pages 4318-4321

  Jones, Leigh F ^a   Batsanov, Andrei ^b   Brechin, Euan K ^a   Collison, David ^a   Helliwell, Madeleine ^a   Mallah, Talal ^c   McInnes, Eric J L ^a   Piligkos, Stergios ^a  

^a UNIVERSITY OF MANCHESTER   (United Kingdom)

^b DURHAM UNIVERSITY   (United Kingdom)

^c UNIVERSITÉ PARIS SACLAY   (France)

Author keywords

Cluster compunds; EPR spectroscopy; Iron; Magneti properties; Metal metal interactions

Indexed keywords

MAGNETISM; SYNTHESIS (CHEMICAL);

IRON WHEELS;

IRON COMPOUNDS;

IRON COMPLEX; METAL COMPLEX;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL STRUCTURE; MAGNETISM; MATERIALS TESTING; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 0038767379     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/1521-3773(20021115)41:22<4318::AID-ANIE4318>3.0.CO;2-I     Document Type: Article

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19. int = 0.1432), R
20. = 0.0952 and wR2 = 0.2717 using 8547 reflections with 1 > 2σ(1). CCDC-189565 and -189566 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12. Union Road. Cambridge CB2 1EZ, UK; fax: (+44)1223-336-033; or deposit@ccdc.cam.ac.uk).
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24. 2(MeCN)]. This has been confirmed by determination of the complete crystal and molecular structure: orthorhombic, space group Fdd, a = 20.9903, b = 25.4990, c = 46.6602 Å.