Salt-inclusion synthesis of Ba2MnSi2O7Cl. A fresnoite-type polar framework containing the acentric [Si2O7]6- polyanion in the anti-ReO3 type [(Ba2Mn)Cl]6+ cage

Inorganic Chemistry

Volumn 42, Issue 13, 2003, Pages 3978-3980

  Mo, Xunhua ^a   Hwu, Shiou Jyh ^a  

^a CLEMSON UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

BARIUM DERIVATIVE; CHLORIDE ION; FRESNOITE; MANGANESE DERIVATIVE; MANGANESE SILICATE CHLORIDE; OXYGEN; POLYANION; SILICONE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; CRYSTAL STRUCTURE; CRYSTALLIZATION; REACTION ANALYSIS; SYNTHESIS;

EID: 0038578145     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic0342245     Document Type: Article

References (37)

1. Some example literature and references therein: (a) Bein, T. Curr. Opin. Solid State Mater. Sci. 1999, 4, 85-96.
2. (b) Keszler, D. A. Curr. Opin. Solid State Mater. Sci. 1999, 4, 155-162.
3. (c) Yaghi, O. M.; Li, H.; Davis, C.; Richardson, D.; Groy, T. L. Acc. Chem. Res. 1998, 31, 474-484.
4. (d) Marder, S. R.; Sohn, J. E.; Stucky, G. D. Materials for Nonlinear Optics: Chemical Perspective; ACS Symposium Series 455; American Chemical Society: Washington, DC, 1991.
5. (a) Yu, J.; Wang, Y.; Shi, Z.; Xu, R. Chem. Mater. 2001, 13, 2972-2978.
6. (b) Bruce, D.; Wilkinson, A. P.; White, M. G.; Bertrand, J. A. J. Solid State Chem. 1996, 125, 228-233.
7. (c) Bruce, D.; Wilkinson, A. P.; White, M. G.; Bertrand, J. A. J. Chem. Soc., Chem. Commun. 1995, 2059-2060.
8. (a) Evans, O. R., Lin, W. Chem. Mater. 2001, 13, 3009-3017.
9. (b) Seo, J. S.; Whang, D.; Lee, H.; Jun, S.; Oh, J.; Jeon, Y.; Kim, K. Nature 2000, 404, 982-986.
10. (c) Kepert, C. J.; Prior, T. J.; Rosseinsky, M. J. J. Am. Chem. Soc. 2000, 122, 5158-5168.
11. (a) Maggard, P. A.; Stern, C. L.; Poeppelmeier, K. R. J. Am. Chem. Soc. 2001, 123, 7742-7743.
12. (b) Maggard, P. A.; Kopf, A. L.; Stern, C. L.; Poeppelmeier, K. R.; OK, K. M.; Halasyamani, P. S. Inorg. Chem. 2002, 41, 4852-4858.
13. (a) Norquist, A. J.; Heier, K. R.; Halasyamani, P. S.; Stern, C. L., Poeppelmeier, K. R. Inorg. Chem. 2001, 40, 2015-2019.
14. (b) Sykora, R. E.; Ok, K. M.; Halasyamani, P. S.; Albrecht-Schmitt, T. E. J. Am. Chem. Soc. 2002, 124, 1951-1957.
15. (a) Shehee, T. C.; Sykora, R. E.; Ok, K. M.; Halasyamani, P. S.; Albrecht-Schmitt, T. E. Inorg. Chem. 2003, 42, 457-462.
16. (b) Ok, K. M.; Goodey, J.; Broussard, J.; Halasyamani, P. S. Chem. Mater. 2002, 14, 3174-3180.
17. (c) Porter, Y.; Bhuvanesh, N. S. P.; Halasyamani, P. S. Inorg. Chem. 2001, 40, 1172-1175.
18. (d) Porter, Y.; Bhuvanesh, N. S. P.; Halasyamani, P. S. Chem. Mater. 2001, 13, 1910-1915.
19. (e) Halasyamani, P. S.; O'Hare. D. Chem. Mater. 1998, 10, 646-649.
20. (f) Halasyamani, P. S.; O'Hare, D. Inorg. Chem. 1997, 36, 6409-6412.
21. (a) Huang, Q.; Hwu, S.-J. Inorg. Chem. 2003, 42, 655-657.
22. (b) Huang, Q.; Ulutagay-Kartin, M.; Mo, X.; Hwu, S.-J. Mater. Res. Soc. Symp. Proc. 2003, 755, DD12.4.
23. (c) Hwu, S.-J.; Ulutagay-Kartin, M.; Clayhold, J. A.; Mackay, R.; Wardojo, T. A.; O'Connor, C. J.; Krawiec, M. J. Am. Chem. Soc. 2002, 124, 12404-12405.
24. (d) Huang, Q.; Hwu, S.-J.; Mo, X. Angew. Chem., Int. Ed. 2001, 40, 1690-1693.
25. (e) Huang, Q.; Ulutagay, M.; Michener, P. A.; Hwu, S.-J. J. Am. Chem. Soc. 1999, 121, 10323-10326.
26. (f) Ulutagay, M.; Shimek, G. L.; Hwu, S.-J.; Taye, H. Inorg. Chem. 1998, 37, 1507-1512.
27. (g) Etheredge, K. M. S.; Hwu, S.-J. Inorg. Chem. 1995, 34, 3123-3125.
28. 3, was obtained.
29. 3. The absolute configuration was determined on the basis of comparison using Friedel pairs. The chemical contents were confirmed by qualitative EDAX analysis. (a) Sheldrick, G. M. In Crystallographic Computing 3; Shledrick, G. M., Kruger, C., Goddard, R., Eds.; Oxford University Press: London, 1985; pp 175-189. (b) Sheldrick, G. M. In SHELXTL, Version 6.1 Structure Determination Software Programs; Bruker Analytical X-ray Systems Inc.: Madison, WI, 2001.
30. 3. The absolute configuration was determined on the basis of comparison using Friedel pairs. The chemical contents were confirmed by qualitative EDAX analysis. (a) Sheldrick, G. M. In Crystallographic Computing 3; Shledrick, G. M., Kruger, C., Goddard, R., Eds.; Oxford University Press: London, 1985; pp 175-189. (b) Sheldrick, G. M. In SHELXTL, Version 6.1 Structure Determination Software Programs; Bruker Analytical X-ray Systems Inc.: Madison, WI, 2001.
31. Halasyamani, P. S.; Poeppelmeier, K. R. Chem. Mater. 1998, 10, 2753-2769.
32. Ulutagay-Kartin, M.; Hwu, S.-J.; Clayhold, J. A. Inorg. Chem. 2003, 42, 2405-2409.
33. Rodrígues, F.; Nuñez, P.; Marco de Lucas, M. C. J. Solid State Chem. 1994, 110, 370-383.
34. Shannon, R. D. Acta Crystallogr., Sect. A. 1976, 32, 751-767.
35. Moore, P. B.; Louisnathan, J. Science 1967, 156, 1361-1362.
36. Kunz, M.; Brown, I. D. J. Solid State Chem. 1995, 115, 395-406.
37. The powder X-ray diffraction studies show that the cell volume decreases by 0.9% as the temperature increases from 123 to 423 K, while the largest decrease is 0.5% in a and increase by 0.1% in c.