Diphenyl(phenylethynyl)phosphine d6 [Rh(III), Ir(III), Ru(II)] complexes: Preparation of homo (μ-Cl)2 and hetero (μ-Cl)(μ-PPh2C≡CPh) bridged d6-d8 compounds

Organometallics

Volumn 21, Issue 11, 2002, Pages 2314-2324

  Berenguer, Jesús R ^a   Bernechea, María ^a   Forniés, Juan ^b   Gómez, Julio ^a   Lalinde, Elena ^a  

^a UNIVERSITY OF LA RIOJA   (Spain)

^b UNIVERSITY OF ZARAGOZA   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

ACTIVATION ENERGY; CHEMICAL BONDS; COMPLEXATION; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PHOSPHORUS COMPOUNDS; PLATINUM COMPOUNDS; POSITIVE IONS; REDUCTION; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION ANALYSIS;

BINUCLEAR COMPLEXES;

ORGANOMETALLICS;

EID: 0038575378     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om020052s     Document Type: Article

References (92)

1. (a) Went, M. J. Polyhedron 1995, 465 and references therein.
2. (b) Louattani E.; Suades, J. J. Organomet, Chem. 2000, 604, 234.
3. (c) Jeffery, J. C.; Pereira, R. M. S.; Vargas, M. D.; Went, M. J. J. Chem. Soc., Dalton Trans. 1995, 1805.
4. (d) Lang, H.; Weinmann, M.; Winter, M.; Leise, M.; Imhof, W. J. Organomet. Chem. 1995, 503, 69.
5. (e) Louattani, E.; Suades, J.; Alvarez-Larena, A.; Piniella J. F.; Germain, G. J. Organomet. Chem. 1996, 506, 121.
6. (f) Dickson, R. S.; Desimone, T.; Parker R. J.; Fallon, G. D. Organometallics 1997, 16, 1531.
7. (g) Imhof, W.; Eber, B.; Huttener G.; Emmeride, C. J. Organomet. Chem. 1998, 447, 21.
8. (h) Jones, D. F.; Dixneuf, P. H.; Southern, T. G.; Marouille, J.; Grandjean, D.; Guenot, P. lnorg. Chem. 1981, 20, 3247.
9. (i) Jacobson, S.; Carty, A. J.; Mathew, M.; Palenik, G. J. J. Am. Chem. Soc. 1974, 96, 4330.
10. (j) Carty, A. J.; Paik, H. N.; Ng, T. W. J. Organomet. Chem. 1974, 74, 279.
11. (k) Patel, H. A.; Carty, A. J.; Hota, N. K. J. Organomet. Chem. 1973, 50, 247.
12. (l) Hota, N. K.; Patel, H. A.; Carty, A. J.; Mathew, M.; Palenik, G. J. Organomet. Chem. 1971, 32, C55.
13. (m) Sappa, E.; Predieri, G.; Tiripicchio, A.; Tiripicchio-Camellini, M. J. Organomet. Chem. 1985, 297, 103.
14. (n) Carty, A. J.; Paik, H. N.; Palenik, J. G. Inorg. Chem. 1977, 16, 300.
15. (o) Carty, A. J.; Smith, W. P.; Taylor, N. J. J. Organomet. Chem. 1978, 146, C1.
16. (p) Carty, A. J.; Dimock, K.; Paik, H. N.; Palenik, G. J. J. Organomet. Chem. 1974, 70, C17.
17. (q) Bruce, M. I; Willians, M. L.; Skelton, B. W.; White, A. H. J. Organomet. Chem. 1985, 282, C53.
18. (a) Carty, A. J. Pure Appl. Chem. 1982, 54, 113 and references therein.
19. (b) Carty, A. J.; Taylor, N. J.; Smith, W. F. J. Chem. Soc., Chem. Commun. 1979, 750.
20. (c) Nuocianore, D.; MacLaughlin, S. A.; Taylor, N. J.; Carty, A. J. Organometallics 1988, 7, 106.
21. (d) Cherkas, A. A.; Randall, L. H.; MacLauglin, S. A.; Mott, G. N.; Taylor, N. J.; Carty, A. J. Organometallics 1988, 7, 969.
22. (e) Bruce, M. I.; Willians, M. L.; Patrick, J. M.; White, A. H. J. Chem. Soc., Dalton Trans. 1985, 1229.
23. (f) Hogarth, G.; Rechmond, S. P. J. Organomet. Chem. 1997, 534, 221.
24. (a) Bobbie, B. J.; Taylor, N. J.; Carty, A. J. J. Chem. Soc., Chem. Commun. 1991, 1511.
25. (b) Sappa, E.; Pasquinelli, A.; Tiripicchio, A.; Tiripicchio Camellini, M. J. Chem. Soc., Dalton Trans. 1989, 601.
26. (c) Davies, J. E.; Mays, M. J.; Raithby, P. R.; Sarveswaran, K.; Shields, G. P. J. Organomet. Chem. 1999, 573, 180.
27. (d) Davies, J. E.; Mays, M. J.; Raitbhy, P. R.; Sarveswaran, K.; Solan, G. A. J. Chem. Soc., Dalton Trans. 2001, 1269.
28. (e) Delgado, E.; Chi, Y.; Wang, W.; Hogart, G.; Low, P. J.; Enright, G. D.; Peng, S.-M.; Lee, G.-H.; Carty, A. J. Organometallics 1998, 17, 2936.
29. (f) Pereira, R. M. S.; Fujiwara, F. Y.; Vargas, M. D.; Braga D.; Crepioni, F. Organometallics 1997, 16, 4833.
30. (g) Benvenutti, M. H.; Vargas, M. D.; Braga, D.; Crepioni, F.; Mann, B. E.; Taylor, S. Organometallics 1993, 12, 2947.
31. (a) Carty, A. J.; Taylor, N. J.; Johnson, D. K. J. Am. Chem. Soc. 1979, 101, 5422.
32. (b) Johnson, D. K.; Rukachaisirikul, T.; Sun, Y.; Taylor, N. J.; Canty, A. J.; Carty, A. J. Inorg. Chem. 1993, 32. 5544.
33. (c) Bennett, M. A.; Cobley, Ch. J.; Rae, A. D.; Wenger, E.; Willis, A. C. Organometallics 2000, 19, 1522.
34. (d) Edwards, A. J.; Macgregor, S. A.; Rae, A. D.; Wenger, E.; Willis, A. C. Organometallics 2001, 20, 2864.
35. (e) Miquel, Y.; Cadierno, V.; Donnadieu, B.; Igau, A.; Mayoral, J. P. Organometallics 2000, 19, 54.
36. (f) Miquel, Y.; Igau, A.; Donnadieu, B.; Mayoral, J. P.; Pirio, N.; Meunier, P. J. Am. Chem. Soc. 1998, 120, 3504.
37. (g) Miquel, Y.; Igau, A.; Donnadieu, B.; Mayoral, J. P.; Dupuis, L.; Pirio, N.; Meunier, P. Chem. Commun. 1997, 279.
38. (h) Dupuis, L.; Pirio, N.; Meunier, P.; Igau, A.; Donnadieu, D.; Mayoral, P. J. Angew. Chem., Int. Ed. Engl. 1997, 36, 987.
39. (i) Bennett, M. A.; Cobley, Ch. J.; Wengers, E.; Willis, A. C. Chem. Commun. 1998, 1307.
40. (j) Rosa, P.; Le Floch, P.; Ricard, L.; Mathey, F. J. Am. Chem. Soc. 1997, 119, 9417.
41. (k) Dema, A. C.; Lukehart, Ch. M. Inorg. Chim. Acta 1997, 264, 193.
42. (l) Li, X.; Lukehart, Ch. M. Organometallics 1992, 11, 3993.
43. (m) Montlo, D.; Suades, J.; Dahan, F.; Mathieu, R. Organometallics 1990, 9, 2933. See also:
44. (n) Davies, J. E.; Mays, M. J.; Raithby, P. R.; Sarveswaran, K.; Solan, G. A. J. Chem. Soc., Dalton Trans. 2000, 3331.
45. (a) Liu, X.; Mok, K. F.; Leung, P.-H. Organometallics 2001, 20, 3918.
46. (b) Dickson, R. S.; De Simone, T.; Parker, R. J.; Fallon, G. D. Organometallics 1997, 16, 1531.
47. (c) Simpson, R. T.; Jacobson, S. E.; Carty, A. J. J. Chem. Soc. Chem. Commun. 1973, 388.
48. (d) Carty, A. J.; Jacobson, S. E.; Simpson, R. T. J. Am. Chem. Soc. 1975, 97, 7254.
49. (e) Carty, A. J.; Johnson, D. K.; Jacobson, S. E. J. Am. Chem. Soc. 1979, 101, 5612.
50. (f) Taylor, N. J.; Jacobson, S. E.; Carty, A. J. Inorg. Chem. 1975, 14, 2648. See also ref 7d.
51. (a) Louattani, E.; Lledos, A.; Suades, J.; Alvarez-Larena, A.; Piniella, F. Organometallics 1995, 14, 1053. See also:
52. (b) Rossenberg, D.; Drenth, W. Tetrahedron 1971, 27, 3893.
53. (c) Albright, T. A., Freeman, W. J.; Schweizer, E. E. J. Am. Chem. Soc. 1975, 97, 2946.
54. (a) Louattani, E.; Suades, J. Inorg. Chim. Acta 1999, 291, 207.
55. (b) Louattani, E.; Suades, J.; Mathieu, R. J. Organomet. Chem. 1991, 421, 395.
56. (c) Hengefeld, A.; Nast, R. J. Organomet. Chem. 1983, 252, 375.
57. (d) Hempsali, H. D.; Hyde, E. M.; Mentzer, E.; Saw, B. L. J. Chem. Soc., Dalton Trans. 1997, 2285.
58. (e) Wong, Y. S.; Jacobson, S.; Chieh, P. C.; Carty, A. J. Inorg. Chem. 1974, 13, 284.
59. (f) Wheelock, K. S.; Nelson, J. H.; Jonassen, M. B. Inorg. Chim. Acta 1970, 4, 399.
60. (g) King, R. B.; Efraty, A. Inorg. Chim. Acta 1970, 4, 319.
61. (h) Simpson, R. T.; Carty, A. J. J. Coord. Chem. 1973, 2, 207.
62. (i) Bardaji, M.; Laguna, A.; Jones, P. G. Organometallics 2001, 20, 3906.
63. Ara, I.; Falvello, L. R.; Fernandez, S.; Formés, J.; Lalinde, E.; Martín, A.; Moreno, M. T. Organometallics 1997, 16, 5923.
64. Forniés, J.; Lalinde, E.; Martín, A.; Moreno, M. T.; Welch, A. J. J. Chem. Soc., Dalton Trans. 1995, 1333.
65. (a) Chartmant, J. P. H.; Forniés; J.; Gómez, J.; Lalinde, E.; Moreno, M. T.; Orpen, A. G.; Solano, S. Angew. Chem., Int. Ed. Engl. 1999, 38, 3058.
66. (b) Ara, I.; Forniés, J.; García, A.; Gómez, J.; Lalinde, E.; Moreno M. T. Chem. Eur. J., in press.
67. (a) Tilley, T. D.; Grubbs, R. H.; Bercaw, J. E. Organometallics 1984, 3, 274.
68. (b) Arligui, T.; Border, C.; Chaudret, B.; Devillers, J.; Poilblanc, R. Organometallics 1989, 8, 1308.
69. Ji, H.; Nelson, J. H.; Decian, A.; Fischer, J.; Solujic, L.; Milosavljevio, E. B. Organometallics 1992, 11, 401.
70. Geary, W. J. Coord. Chem. Rev. 1971, 7, 81.
71. Dromi, D.; Arena, C. G.; Nicolo, F.; Bruno, G.; Faraone, F. J. Organomet. Chem. 1995, 485, 115 and references therein.
72. For Rh: (a) Eisen, M. S.; Haskel, A.; Chen, H.; Olmstead, M. M.; Smith, D. P.; Maestre, M. F.; Fish, R. H. Organometallics 1995, 14, 2806.
73. (b) Barthel-Rosa, L. P.; Catalano, V. J.; Maitra, K.; Nelson, J. H.
74. (c) Carmona, D.; Lahoz, F. J.; Oro, L.; Lamata, M. P.; Viguri, F.; San Jose, E. Organometallics 1996, 15, 2961. For Ir:
75. (d) Atherton, M. J.; Faweett, J.; Holloway, J. H.; Hope, E. G.; Karacar, A.; Russell, D.; Saunders, G. C. J. Chem. Soc., Dalton Trans. 1997, 1811. For Ru:
76. (e) de los Rios, I.; Jimenez Tenorio, M. J.; Puerta, M. C.; Valerga, P. Organometallics 1998, 17, 4392.
77. (a) Ara, I; Berenguer, J. R.; Eguizábal, E.; Forniés, J.; Lalinde, E.; Martín, A. Eur. J. Inorg. Chem. 2001, 1631.
78. (b) Stang, P. J.; Huang, Y.-H.; Arif, A. M. Organometallics 1992, 11, 23.
79. 31P-NMR Spectroscopy in Stereochemical Analysis (Methods in Stereochemical Analysis, 8); VCH: New York, 1987; p 91.
80. (a) Younus, M.; Long, N. J.; Raithby, P. R.; Lewis, J. J. Organomet. Chem. 1998, 570, 55.
81. (b) Harriman, A.; Hissler, M.; Ziessel, R.; De Cian, A.; Fischer, J. J. Chem. Soc., Dalton Trans. 1995, 4067.
82. (c) Hissler, M.; Ziessel, R. J. Chem. Soc., Dalton Trans. 1995, 893.
83. (d) Sato, M.; Mugi, E. J. Organomet. Chem. 1996, 508, 159.
84. (e) A search in the CSD (version 5.22) gives only 12 examples of Ru(II)-Ptd(II) X-ray characterized binuclear complexes.
85. Ara, I.; Berenguer, J. R.; Eguizábal, E.; Formés, J.; Lalinde, E.; Martín, A.; Martínez, F. Organomelallics 1998, 17, 4578.
86. Usón, R.; Forniés, J.; Tomás, M.; Menjón, B. Organometallics 1985, 4, 1912.
87. Kang, J. W.; Moseley, K.; Maitlis, P. J. J. Am. Chem. Soc. 1969, 91, 5970.
88. Carty, A. J.; Hota, N. K.; Ng, T. W.; Pate, H. A.; O'Connor, T. J. Can. J. Chem. 1971, 49, 2706.
89. Otwinowski, Z.; Minor, W. In Methods in Enzymology; Carter, C. W., Jr., Sweet, R. M., Eds.; Academic Press: New York, 1997; Vol. 276A, p 307.
90. Blessing, R. H. Acta Crystallogr. 1995, A51, 33.
91. Beurskens, P. T.; Beurskens, G.; Bosman, W. P.; de Gelder, R.; García-Granda, S.; Gould, R. O.; Smith, J. M. M.; Smykalla, C. The DIRDIF92 program system; Technical Report of the Crystallography Laboratory; University of Nijmegen: The Netherlands, 1992.
92. Sheldrick, G. M. SHELX-97, a program for the refinement of crystal structures; University of Göttingen: Göttingen, Germany, 1997.