Solid state separated-local-field NMR spectroscopy on half-integer quadrupolar nuclei: Principles and applications to borane analysis

Journal of the American Chemical Society

Volumn 125, Issue 24, 2003, Pages 7451-7460

  Grinshtein, Julia ^a   Frydman, Lucio ^a  

^a WEIZMANN INSTITUTE OF SCIENCE   (Israel)

Author keywords

[No Author keywords available]

Indexed keywords

SOLID STATES;

MOLECULAR DYNAMICS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PROTONS; STRUCTURE (COMPOSITION);

BORON COMPOUNDS;

BORANE DERIVATIVE; BORON;

ACCELERATION; ARTICLE; CHEMICAL ANALYSIS; CHEMICAL STRUCTURE; MOLECULAR DYNAMICS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PROTON TRANSPORT; QUANTUM MECHANICS; SOLID STATE;

BORANES; MAGNETIC RESONANCE SPECTROSCOPY; QUANTUM THEORY;

EID: 0038450253     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja0214025     Document Type: Article

References (48)

1. Cohen, M. H.; Reif, F. Solid State Phys. 1957, 5, 321.
2. Abragam, A. Principles of Nuclear Magnetism; Oxford University Press: New York, 1961.
3. Anderson, M. W., Duer, M. J., Eds. New NMR Techniques for Quadrupolar Nuclei. Solid State NMR 1999, 15.
4. Fitzgerald, J., Ed. Solid State NMR of Inorganic Materials; ACS Symposium Series 717; American Chemical Society: Washington, DC, 1999.
5. Smith, M. E.; vanEck, E. R. H. Prog. NMR Spectroscopy 1999, 34, 159.
6. Andrew, E. R.; Bradbury, A.; Eades, R. G. Nature 1958, 182, 1659.
7. Lowe, I. J. Phys. Rev. Lett. 1959, 2, 285.
8. Wooten, E. W.; Muller, K. T.; Pines, A. Acc. Chem. Res. 1992, 25, 209.
9. Chmelka, B. F.; Zwanziger, J. W. NMR: Basic Principles and Progress. 1994, 33, 79.
10. Frydman, L. Annu. Rev. Phys. Chem. 2001, 52, 463.
11. Gerstein, B. C.; Dybowski, C. Transient Techniques in NMR of Solids: An Introduction to Theory and Practice; Academic Press: Orlando, FL, 1985.
12. Amoureux, J. P.; Fernandez, C.; Carpentier, L.; Cochon, E. Phys. Status Solidi A 1992, 132, 461.
13. Gullion, T.; Schaefer, J. Adv. Magn. Reson. 1989, 13, 57.
14. Griffiths, J. M.; Griffin, R. G. Anal. Chim. Acta 1993, 283, 1081.
15. Schmidt-Rohr, K.; Spiess, H. W. Multidimensional Solid-State NMR and Polymers; Academic Press: London, 1994.
16. Dusold, S.; Sebald, A. Annu. Rep. NMR Spectrosc. 2001, 41, 185.
17. Munowitz, M. G.; Griffin, R. G. J. Chem. Phys. 1982, 76, 2848.
18. Munowitz, M. G.; Griffin, R. G.; Bodenhausen, G.; Wang, T. H. J. Am. Chem. Soc. 1981, 103, 2529.
19. Schaefer, J.; McKay, R. A.; Stejskal, E. O.; Dixon, W. T. J. Magn. Reson. 1983, 52, 123.
20. Schaefer, J.; Stejskal, E. O.; McKay, R. A.; Dixon, W. T. Macromolecules 1984, 17, 1479.
21. Roberts, J. E.; Harbison, G. S.; Munowitz, M. G.; Herzfeld, J.; Griffin, R. G. J. Am. Chem. Soc. 1987, 109, 4163.
22. Palmas, P.; Tekely, P.; Canet, D. Solid State NMR 1995, 4, 105.
23. McElheny, D.; deVita, E.; Frydman, L. J. Magn. Reson. 2000, 143, 321.
24. Frydman, L.; Harwood, J. S. J. Am. Chem. Soc. 1995, 117, 5367.
25. Grinshtein, J.; Grant, C. V.; Frydman, L. J. Am. Chem. Soc. 2002, 124, 13344.
26. Bennett, A. E.; Rienstra, C. M.; Auger, M.; Lakshmi, K. V.; Griffin, R. G. J. Chem. Phys. 1995, 103, 6951.
27. Hong, M.; Gross, J. D.; Griffin, R. G. J. Phys. Chem. B 1997, 101, 5869.
28. Hong, M.; Gross, J. D.; Rienstra, C. M.; Griffin, R. G.; Kumashiro, K. K.; Schmidt-Robr, K. J. Magn. Reson. 1997, 129, 85.
29. deVita, E.; Frydman, L. J. Magn. Reson. 2001, 148, 327.
30. Lipscomb, W. N. Boron Hydrides; Benjamin: New York, 1963.
31. Grimes, R. N. ACS Symposium Series 827; American Chemical Society: Washington, DC, 2002; p 20.
32. Casanova, J., Ed. Borane, Carborane, Carbocation Continuum; Wiley: New York, 1998.
33. Greenwood, N. N. Coord. Chem. Rev. 2002, 226, 61.
34. Ramachandran, P. V.; Brown, H. C. ACS Symposium Series 783; American Chemical Society: Washington, DC, 2001; p 1.
35. Brauer, D. J.; Kruger, C. Acta Crystallogr. 1973, B29, 1684.
36. Alexander, S. J. Chem. Phys. 1962, 37, 967.
37. Kaplan, J. J. Chem. Phys. 1958, 29, 462.
38. Ernst, R. R.; Bodenhausen, G.; Wokaun, A. Principles of Nuclear Magnetic Resonance in One and Two Dimensions; Clarendon: Oxford, 1987.
39. McConnell, H. M. J. Chem. Phys. 1958, 28, 430.
40. Niedzu, K. Mol. Struct. Energ. 1988, 5, 357.
41. Clouse, A. O.; Moody, D. C.; Rietz, R. R.; Rospberry, T.; Schaeffer, R. J. Am. Chem. Soc. 1973, 95, 2496.
42. Brown, S. P.; Wimperis, S. J. Magn. Reson. 1997, 124, 279.
43. Brown, S. P.; Heyes, S. J.; Wimperis, S. J. Magn. Reson. 1996, A119, 280.
44. Medek, A.; Harwood, J. S.; Frydman, L. J. Am. Chem. Soc. 1995, 117, 12779.
45. Milliot, Y.; Man, P. P. Solid State NMR 2002, 21, 21.
46. Kasper, J. S.; Lucht, C. M.; Harker, D. Acta Crystallogr. 1950, 3, 436.
47. Madhu, P. K.; Goldbourt, A.; Frydman, L.; Vega, S. Chem. Phys. Lett. 1999, 307, 41.
48. Madhu, P. K.; Goldbourt, A.; Frydman, L.; Vega, S. J. Chem. Phys. 2000, 112, 2377.