One-step preparation of [RuCp*(η6-arene)]+ sandwich complexes

European Journal of Inorganic Chemistry

Volumn , Issue 12, 2003, Pages 2255-2263

  Schmid, Alexander ^a   Piotrowski, Holger ^a   Lindel, Thomas ^a  

^a UNIVERSITY OF MUNICH   (Germany)

Author keywords

NMR spectroscopy; Ruthenium; Sandwich complexes; Synthetic methods

Indexed keywords

RUTHENIUM COMPOUNDS;

AMINO-ACIDS; CHLOROANISOLES; COMPARATIVE EXPERIMENTS; FUNCTIONALIZED; NMR-SPECTROSCOPY; NUCLEOPHILIC SUBSTITUTIONS; SANDWICH COMPLEXES; SIDE PRODUCTS; SINGLE-STEP; SYNTHETIC METHODS;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

AMINO ACID; ANISOLE DERIVATIVE; LIGAND; METAL COMPLEX; METHANOL; POLYCYCLIC AROMATIC HYDROCARBON; RUTHENIUM DERIVATIVE;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; COMPLEX FORMATION; CRYSTAL STRUCTURE; DIASTEREOISOMER; DIELS ALDER REACTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SYNTHESIS;

EID: 0038266564     PISSN: 14341948     EISSN: None     Source Type: Journal    
DOI: 10.1002/ejic.200200579     Document Type: Article

References (44)

1. [1a] D. Leone-Stumpf, T. Lindel, Chem. Eur. J. 2001, 7, 3961-3965.
2. [1b] D. Leone-Stumpf, T. Lindel, Eur. J. Org. Chem. 2003, 1853-1858.
3. The term "peptoid" is used to describe a "peptide-like compound" ("-oid" from the Old Greek εδoς "picture"). It was originally restricted to oligomers of N-substituted glycines: R. J. Simon, R. S. Kania, R. N. Zuckermann, V. D. Huebner, D. A. Jewell, S. Banville, S. Ng, L. Wang, S. Rosenberg, C. K. Marlowe, D. C. Spellmeyer, R. Tan, A. D. Frankel, D. V. Santi, F. E. Cohen, P. A. Bartlett, Proc. Natl. Acad. Sci. USA 1992, 89, 9367-9371.
4. -); Handbook of Chemistry and Physics, 76th ed. (Ed.: D. R. Lide), CRC press, Boca Raton 1995, p. 11-64.
5. [4a] A. J. Pearson, J. G. Park, S. H. Yang, Y. H. Chuang, J. Chem. Soc., Chem. Commun. 1989, 1363-1364.
6. [4b] A. J. Pearson, J.-N. Heo, Org. Lett. 2000, 2, 2987-2990 and refs. cited therein.
7. [4c] C. W. West, D. H. Rich, Org. Lett. 1999, 1, 1819-1822 and refs. cited therein.
8. [4d] A. Marchetti, J. M. Ontoria, V. G. Matassa, Synlett 1999, SI, 1000-1002.
9. T. P. Gill, K. R. Mann, Organometallics 1982, 1, 485-488.
10. B. M. Trost, C. M. Older, Organometallics 2002, 21, 2544-2546.
11. [7a] V. S. Kaganovich, A. R. Kudinov, M. I. Rybinskaya, Izv. Akad. Nauk SSSR. Ser. Khim. 1986, 2, 492.
12. [7b] A. R. Kudinov, M. I. Rybinskaya, Yu. T. Struchkov, A. I. Yanovskii, P. V. Petrovskii, J. Organomet. Chem. 1987, 336, 187-197.
13. [8a] B. Chaudret, F. Jalón, J. Chem. Soc. Chem. Commun. 1988, 711-713.
14. [8b] B. Chaudret, F. Jalón, M. Pérez-Manrique, New J. Chem. 1990, 14, 331-338.
15. J. E. Letourneau, M. A. Wellman, D. J. Burnell, J. Org. Chem. 1997, 62, 7272-7277.
16. J. L. Schrenk, A. M. McNair, F. B. McCormick, K. R. Mann, Inorg. Chem. 1986, 25, 3501-3504.
17. [11a] T. D. Tilley, R. H. Grubbs, J. E. Bercaw, Organometallics 1984, 3, 274-278.
18. [11b] N. Oshima, H. Suzuki, Y. Moro-Oka, Inorg. Chem. 1986, 25, 3407-3412.
19. P. J. Fagan, M. D. Ward, J. C. Calabrese, J. Am. Chem. Soc. 1989, 111, 1698-1719.
20. B. Steinmetz, W. A. Schenk, Organometallics 1999, 18, 943-946.
21. W . S. Sheldrick, A. Gleichmann, J. Organomet. Chem. 1994, 470, 183-187.
22. [15a] U. Koelle, J. Kossakowski, R. Boese, J. Organomet. Chem. 1989, 378, 449-455.
23. [15b] U. Koelle, M. H. Wang, Organometallics 1990, 9, 195-198.
24. [16a] H. Lehmkuhl, M. Bellenbaum, J. Grundke, H. Mauermann, C. Krüger, Chem. Ber. 1988, 1719-1728.
25. [16b] U. Koelle, J. Kossakowski, J Organomet. Chem. 1989, 362, 383.
26. [17a] U. Koelle, J. Kossakowski, N. Klaff, L. Wesemann, U. Englert, G. E. Herberich, Angew. Chem. 1991, 103,732-3; Angew. Chem. Int. Ed. Engl. 1991, 30, 690-1.
27. [17a] U. Koelle, J. Kossakowski, N. Klaff, L. Wesemann, U. Englert, G. E. Herberich, Angew. Chem. 1991, 103,732-3; Angew. Chem. Int. Ed. Engl. 1991, 30, 690-1.
28. [17b] U. Koelle, J. Kossakowski, D. Grumbine, T. D. Tilley, Inorg. Synth. 1992, 29, 225-228.
29. [18a] A. N. Nesmeyanov, N. A. Vol'kenau, I. N. Bolesova, L. S. Shul'pina, J. Organomet. Chem. 1979, 182, C36-C38.
30. [18b] E. Román, D. Astruc, Inorg. Chim. Acta 1979, 37, L465-L466.
31. X. D. He, B. Chaudret, F. Dahan, Y.-S. Huang, Organometallics 1991, 10, 970-979.
32. M. Stebler-Roethlisberger, A. Salzer, H. B. Bürgi, A. Ludi, Organometallics 1986, 5, 298-302.
33. P. Bernhard, H. B. Bürgi, J. Hauser, H. Lehmann, A. Ludi, Inorg. Chem. 1982, 21, 3936-3941.
34. A. Bauer, U. Englert, S. Geyser, F. Podewils, A. Salzer, Organometallics 2000, 19, 5471-5476.
35. [23a] 3, 6, 8: ref. [7a].
36. [23b] 3: M. E. Navarro Clemente, P. Juárez Saavedra, M. C. Vásquez, M. A. Paz-Sandoval, A. M. Arif, R. D. Ernst, Organometallics 2002, 21, 592-605.
37. [20d]
38. [24a] L. Fan, C. Wei, F. I. Aigbirhio, M. L. Turner, O. V. Gusev, L. N. Morozova, D. R. T. Knowles, P. M. Maitlis, Organometallics 1996, 15, 98-104.
39. [24b] L. Fan, M. L. Turner, H. Adams, N. A. Bailey, P. M. Maitlis, Organometallics 1995, 14, 676-684.
40. [24c] D. R. T. Knowles, H. Adams, P. M. Maitlis, Organometallics 1998, 17, 1741-1749.
41. J. K. Evju, K. R. Mann, Organometallics 2002, 21, 993-996.
42. XRed, rev. 1.09, Stoe Data Reduction Program, Stoe, Darmstadt, Germany.
43. A. Altomare, M. C. Burla, M. Camalli, G. L. Cascarano, C. Giacovazzo, A. Guagliardi, A. G. G. Moliterni, G. Polidori, R. Spagna: SIR97: a new tool for crystal structure determination and refinement; J. Appl. Crystallogr. 1999, 32, 115-119.
44. G. M. Sheldrick, SHELXL-97, Program for Crystal Structure Refinement, University of Göttingen, Germany, 97-2 version.