Syntheses, structures, and reactivity studies of half-open ruthenocenes and their oxodienyl analogues

Organometallics

Volumn 21, Issue 4, 2002, Pages 592-605

  Navarro Clemente, M Elena ^a   Saavedra, Patricia Juárez ^a   Vásquez, Marisol Cervantes ^a   Angeles Paz Sandoval, M ^a   Arif, Atta M ^b   Ernst, Richard D ^b  

^a DEPARTAMENTO DE FÍSICA   (Mexico)

^b UNIVERSITY OF UTAH   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ADDITION REACTIONS; CHEMICAL BONDS; COMPLEXATION; PEROXIDES; TOLUENE;

LEWIS BASES;

ORGANOMETALLICS;

EID: 0012713587     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om010735s     Document Type: Article

References (63)

1. (a) Trakarnpruk, W.; Arif, A. M.; Ernst, R. D. Organometallics 1992, 11, 1686.
2. (b) Trakarnpruk, W.; Rheingold, A. L.; Haggerty, B. S.; Ernst, R. D. Organometallics 1994, 13, 3914.
3. (c) Kulsomphob, V.; Ernst, K. A.; Lam, K.-C.; Rheingold, A. L.; Ernst, R. D. Inorg. Chim. Acta 1999, 296, 170.
4. (d) Kulsomphob, V.; Turpin, G. C.; Lam, K.-C.; Youngkin, C.; Trakarnpruk, W.; Carroll, P.; Rheingold, A. L.; Ernst, R. D. J. Chem. Soc., Dalton Trans. 2000, 3086.
5. Gutierrez, J. A.; Navarro, M. E.; Paz-Sandoval, M. A.; Arif, A. M.; Ernst, R. D. Organometallics 1999, 18, 1068.
6. Trakarnpruk, W.; Arif, A. M.; Ernst, E. D. Organometallics 1994, 13, 2423.
7. (a) Ernst, R. D. Chem. Rev. 1988, 88, 1255.
8. (b) Bosch, H. W.; Hund, U.; Nietlispach, D.; Salzer, A. Organometallics 1992, 11, 2087.
9. Navarro-Clemente, M. E.; Chazaro, L. F.; Gonzalez, F. J.; Paz-Sandoval, M. A. J. Electroanal. Chem. 2000, 480, 18.
10. Nagashima, H.; Mukai, K.; Shiota, Y.; Ara, K.; Itoh, K.; Suzuki, H.; Oshima, N.; Moro-oka, Y. Organometallics 1985, 4, 1314.
11. Nagashima, H.; Mukai, K.; Shiota, Y.; Yamaguchi, K.; Ara, K.; Fukahori, T.; Suzuki, H.; Akita, M.; Moro-oka, Y.; Itoh, K. Organometallics 1990, 9, 799.
12. Gemel, C.; Mereiter, K.; Schmid, R.; Kirchner, K. Organometallics 1996, 15, 532.
13. Gemel, C.; Kalt, D.; Mereiter, K.; Sapunov, V. N.; Schmid, R.; Kirchner, K. Organometallics 1997, 16, 427.
14. Itoh, K.; Masuda, K.; Ikeda, H. Organometallics 1993, 12, 2752.
15. Kirchner, K.; Mereiter, K.; Schmid, R. J. Chem Soc., Chem. Commun. 1994, 161.
16. Kirchner, K.; Mereiter, K.; Umfahrer, A.; Schmid, R. Organometallics 1994, 13, 1886.
17. Mauthner, K.; Mereiter, K.; Schmid, R.; Kirchner, K. Organometallics 1994, 13, 5054.
18. Gemel, C.; Mereiter, K.; Schmid, R.; Kirchner, K. Organometallics 1995, 14, 1405.
19. Kirchner, K.; Mauthner, K.; Mereiter, K.; Schmid, R. J. Chem. Soc., Chem. Commun. 1993, 892.
20. Jia, G.; Ng, W. S.; Chu, H. S.; Wong, W.-T.; Yu, N.-T.; Williams I. D. Organometallics 1999, 18, 3597, and references therein.
21. Rios, I.; Jimenez-Tenorio, M.; Padilla, J.; Puerta, M. C.; Valerga, P. J. Chem Soc., Dalton Trans. 1996, 377.
22. Gemel, C.; Mereiter, K.; Schmid, R.; Kirchner, K. Organometallics 1997, 16, 5601.
23. Fan, L.; Turner, M. L.; Adams, H.; Bailey, N. A.; Maitlis, P. M. Organometallics 1995, 14, 676.
24. Knowles, D. R. T.; Adams, H.; Maitlis, P. M. Organometallics 1998, 17, 1741.
25. Guzev, O. V.; Morozova, L. N.; Peganova, T. A.; Antipin, M. Y.; Lyssenko, K. A.; Noels, A. F.; O'Leary, S. R.; Maitlis, P. M. J. Organomet. Chem. 1997, 536, 191.
26. Fan, L.; Wei, C.; Aigbirhio, F. I.; Turner, M. L.; Gusev, O. V.; Morozova, L. N.; Knowles, D. R. T.; Maitlis, P. M. Organometallics 1996, 15, 98, and references therein.
27. Fan, L.; Turner, M. L.; Hursthouse, M. B.; Abdul Malik, K. M.; Gusev, O. V.; Maitlis, P. M. J. Am. Chem. Soc. 1994, 116, 385.
28. Wei, C.; Aigbirhio, F.; Adams, H.; Bailey, N. A.; Hempstead, P. D.; Maitlis, P. M. J. Chem Soc., Chem. Commun. 1991, 883.
29. Suzuki, H.; Kakigano, T.; Fukui, H.; Tanaka, M.; Moro-oka, Y. J. Organomet. Chem. 1994, 473, 295.
30. 13C δ = not observed
31. (b) Koelle, U.; Kossakowski, J. J. Organomet. Chem. 1989, 362, 383.
32. Fish, R. W.; Giering, W. P.; Marten, D.; Rosenblum M. J. Organomet. Chem. 1976, 105, 101.
33. Bleeke, J. R.; Peng W.-J. Organometallics 1984, 3, 1422.
34. Gibson, D. H.; Hsu, W.-L.; Steinmetz, A. L.; Johnson B. V. J. Organomet. Chem. 1981, 208, 89.
35. 32a Separation of 4na′ from the green soluble product can be carried out chromatographically on alumina by elution with ethanol.
36. Rios, I.; Jimenez-Tenorio, M.; Padilla, J.; Puerta, M. C.; Valerga, P. Organometallics 1996, 15, 4565.
37. (a) Rondon, D.; Delbeau, J.; He, X.-D.; Sabo-Etienne, S.; Chaudret, B. J. Chem. Soc., Dalton Trans. 1994, 1895, and references therein
38. (b) Chaudret, B. Bull. Soc. Chim. Fr. 1995, 132, 268.
39. (c) Rondon, D.; He, X.-D.; Chaudret B. J. Organomet. Chem. 1992, 433, C18.
40. (d) Rondon, R.-D.; Chaudret, B.; He, X.-D.; Labroue, D. J. Am. Chem. Soc. 1991, 113, 5671, and references therein.
41. (a) Initial elution of the product mixture on alumina using 1:1 hexane/ether led to a 55% recovery of 1. Subsequent elution with ether led to two orange bands, the second of which was 5.
42. 33c
43. (c) Cheng, M.-H.; Cheng, C.-Y.; Wang, S.-L.; Peng, S.-M.; Liu, R.-S. Organometallics 1990, 9, 1853.
44. (a) Carreno, R.; Urbanos, F.; Dahan, F.; Chaudret, B. New J. Chem. 1994, 18, 449.
45. (b) Masuda, K.; Ohkita, H.; Kurumatani, S.; Itoh, K. Organometallics 1993, 12, 2221.
46. (a) Fagan, P. J.; Ward, M. D.; Caspar, J. V.; Calabrese, J. C.; Krusio, P. J. J. Am. Chem. Soc. 1988, 110, 2981.
47. (b) Fagan, P. J.; Ward, M. D.; Calabrese, J. C. J. Am. Chem. Soc. 1989, 111, 1698.
48. Bauer, A.; Englert, U.; Geyser, S.; Podewils, F.; Salzer A. Organometallics 2000, 19, 5471.
49. (a) Benyunes, S. A.; Day, J. P.; Green, M.; Al-Saadoon, A. W.; Waring, T. L. Angew. Chem., Int. Ed. Engl. 1990, 29, 1416.
50. (b) Trakarnpruk, W. Ph.D. Thesis, University of Utah, 1993.
51. Moreno, B.; Sabo-Etienne, S.; Dahan, F.; Chaudret, B. J. Organomet. Chem. 1995, 498, 139.
52. Consiglio, G.; Morandini, F.; Ciani, G.; Sironi, A.; Kretschmer, M. J. Am. Chem. Soc. 1983, 105, 1391.
53. Torres-Lubian, R.; Rosales-Hoz, M. J.; Arif, A. M.; Ernst, R. D.; Paz-Sandoval M. A. J. Organomet. Chem. 1999, 585, 68.
54. Mauthner, K.; Mereiter, K.; Schmid, R.; Kirchner, K. Inorg. Chim. Acta 1995, 236, 95.
55. Albers, M. O.; Liles, D. C.; Robinson, D. J.; Shaver, A.; Singleton E. Organometallics 1987, 6, 2347.
56. (a) Valentine, J. S. Chem. Rev. 1973, 73, 235.
57. (b) Savariault, J.-M.; Lehmann M. S. J. Am. Chem. Soc. 1980, 102, 1298.
58. Sato, M.; Asai, M. J. Organomet. Chem. 1996, 508, 121.
59. Jimenez-Tenorio, M.; Puerta, M. C.; Valerga P. Inorg. Chem. 1994, 33, 3515.
60. Jimenez-Tenorio, M.; Puerta, M. C.; Valerga P. J. Am. Chem. Soc. 1993, 115, 9794.
61. McGinnety, J. A.; Payne, N. C.; Ibers J. A. J. Am. Chem. Soc. 1969, 91, 6301.
62. Schrenk, J. L.; McNair, A. M.; McCormick, F. B.; Mann, K. R. Inorg. Chem. 1986, 25, 3501.
63. Ernst, R. D.; Freeman, J. W.; Swepston, P. N.; Wilson, D. R. J. Organomet. Chem. 1991, 402, 17.