Synthesis and structural characterization of 2-mercapto-1-tert- butylimidazole and its Group 12 metal derivatives (HmimtBu) 2MBr2 (M = Zn, Cd, Hg)

Journal of Chemical Crystallography

Volumn 33, Issue 5-6, 2003, Pages 437-445

  White, Jennifer L ^a   Tanski, Joseph M ^b   Churchill, David G ^b   Rheingold, Arnold L ^c   Rabinovich, Daniel ^a  

^a University of NC at Charlotte   (United States)

^b Och Spine at New York Presbyterian Hospitals   (United States)

^c UNIVERSITY OF DELAWARE   (United States)

Author keywords

2 mercapto 1 alkylimidazole; Cadmium; Crystal structure; Mercury; Thione complexes; Zinc

Indexed keywords

2 MERCAPTO 1 TERT BUTYLIMIDAZOLE; CADMIUM DERIVATIVE; IMIDAZOLE DERIVATIVE; LIGAND; MERCURY DERIVATIVE; METAL DERIVATIVE; UNCLASSIFIED DRUG; ZINC DERIVATIVE;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL BOND; CHEMICAL STRUCTURE; GEOMETRY; MOLECULAR INTERACTION; SOLID STATE; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 0038124423     PISSN: 10741542     EISSN: None     Source Type: Journal    
DOI: 10.1023/A:1024242400616     Document Type: Article

References (31)

1. (a) Raper, E.S. Coord. Chem. Rev. 1985, 61, 115-184.
2. (b) Akrivos, P.D. Coord. Chem. Rev. 2001, 213, 181-210.
3. (a) Garner, M.; Reglinski, J.; Cassidy, I.; Spicer, M.D.; Kennedy, A.R. Chem. Commun. 1996, 1975-1976.
4. (b) Kimblin, C.; Hascall, T.; Parkin, G. Inorg. Chem. 1997, 36, 5680-5681.
5. Trofimenko, S. Scorpionates: The Coordination Chemistry of Polypyrazolylborate Ligands; Imperial College Press: London, 1999.
6. (a) Kimblin, C.; Bridgewater, B.M.; Churchill, D.G.; Parkin, G. Chem. Commun. 1999, 2301-2302.
7. (b) Tesmer, M.; Shu, M.; Vahrenkamp, H. Inorg. Chem, 2001, 40, 4022-4029.
8. Alvarez, H.M.; Krawiec, M.; Donovan-Merket, B.T.; Fouzi, M.; Rabinovich, D. Inorg. Chem. 2001, 40, 5736-5737.
9. White, J.L.; Tanski, J.M.; Rabinovich, D.J. Chem. Soc., Dalton Trans. 2002, 2987-2991.
10. Alvarez, H.M.; Tran, T.B.; Richter, M.A.; Alyounes, D.M.; Rabinovich, D. ; Tanski, J.M.; Krawiec, M. Inorg. Chem. 2003, 42, 2149-2156.
11. Cassidy, C.S.; Reinhardt, L.A.; Cleland, W.W.; Frey, P.A. J. Chem. Soc., Perkin Trans. 2 1999, 635-641.
12. (a) Raper, E.S.; Creighton, J.R.; Oughtred, R.E.; Nowell, I.W. Acta Crystallogr, Sect. B 1983, 39, 355-360.
13. (b) Vampa, G.; Benvenuti, S.; Severi, F.; Malmusi, L.; Antolini, L. J. Heterocyclic Chem. 1995, 32, 227-234.
14. (a) Ansell, G.B. J. Chem. Soc., Perkin Trans. 2 1972, 841-843.
15. (b) Huang, J.; Schanz, H.-J.; Stevens, E.D.; Nolan, S.P.; Capps, K.B.; Bauer, A.; Hoff, C.D. Inorg. Chem. 2000, 39, 1042-1045.
16. (c) Cox, P.J.; Sohal, B.; Skellern, G.G.; Love, S.W.; Shankland, N. Acta Crystallogr. Sect. C 1996, 52, 3152-3154.
17. (d) Moreno, E.; López-Castro, A.; Márquez, R. Acta Crystallogr., Sect. C 1985, 41, 767-769.
18. (e) Herrmann, W.A.; Köcher, C.; Gooßen, L.J.; Artus, G.R.J. Chem. - Eur. J. 1996, 2, 1627-1636.
19. (f) Raper, E.S.; Jackson, A.R.W.; Gardiner, D.J. Inorg. Chim. Acta 1984, 84, L1-L4.
20. (g) Williams, D.J.; Poor, P.H.; Ramirez, G.; Heyl, B.L. Inorg. Chim. Acta 1988, 147, 221-226.
21. (a) Bell, N.A.; Branston, T.N.; Clegg, W.; Creighton, J.R.; Cucurull-Sánchez, L.; Elsegood, M.R.J.; Raper, E.S. Inorg. Chim. Acta 2000, 303, 220-227.
22. (b) Popovic, Z.; Matkovic-Calogovic, D.; Soldin, Z.; Pavlovic, G.; Davidovic, N.; Vikic-Topic, D. Inorg. Chim. Acta 1999, 294, 35-46.
23. (c) Popovic, Z.; Soldin, Z.; Matkovic-Calogovic, D.; Pavlovic, G.; Rajic, M.; Giester, G. Eur. J. Inorg. Chem. 2002, 171-180.
24. (d) Atherton, Z.; Goodgame, D.M.L.; Menzer, S.; Williams, D.J. Inorg. Chem. 1998, 37, 849-858.
25. (e) Bell, N.A.; Coles, S.J.; Constable, C.P.; Hibbs, D.E.; Hursthouse, M.B.; Manzor, R.; Raper, E.S.; Sammon, C. Inorg. Chim. Acta 2001, 323, 69-77.
26. (f) Williams, D.J.; Ly, T.A.; Mudge, J.W.; Pennington, W.T.; Schimek, G.L. Acta Crystallogr., Sect. C 1997, 53, 415-416.
27. (g) Baraldi, M.; Malavasi, W.; Grandi, R.J. Chem. Crystallogr. 1996, 26, 63-66.
28. CSD, version 5.23 (April 2002). Allen, F.H.; Kennard, O. Chem. Des. Automat. News 1993, 8, 1 and 31-37.
29. Trinajstic, N. Tetrahedron Lett. 1968, 1529-1532.
30. Errington, R.J. Advanced Practical Inorganic and Metalorganic Chemistry; Blackie Academic & Professional: London, 1997.
31. Sheldrick, G.M. Siemens XRD, Madison, WI.