Improved quantitative solution state 13C NMR analysis of ethylene-1-octene copolymers

Polymer

Volumn 44, Issue 12, 2003, Pages 3483-3489

  Adriaensens, P J ^a   Karssenberg, F G ^b   Gelan, J M ^a   Mathot, V B F ^b,c  

^a HASSELT UNIVERSITY   (Belgium)

^b EINDHOVEN UNIVERSITY OF TECHNOLOGY   (Netherlands)

^c DSM RESEARCH   (Netherlands)

Author keywords

Chromium(III)triacetylacetonate; Homogeneous ethylene 1 octene copolymer; Quantitative 13C NMR

Indexed keywords

MICROSTRUCTURE; MONOMERS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; OPTIMIZATION; SIGNAL TO NOISE RATIO; SOLUTIONS;

COMONOMER INVERSION;

COPOLYMERS;

CHROMIUM DERIVATIVE; CHROMIUM TRIACETYLACETONATE; COPOLYMER; ETHYLENE 1 OCTENE COPOLYMER; POLYETHYLENE; UNCLASSIFIED DRUG;

ACCURACY; ALGORITHM; ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CONTINUOUS STIRRED TANK REACTOR; NUCLEAR OVERHAUSER EFFECT; QUANTITATIVE ANALYSIS; SIGNAL NOISE RATIO; VISCOSITY;

POLYMER SCIENCE;

EID: 0037911454     PISSN: 00323861     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0032-3861(03)00256-8     Document Type: Article

References (38)

1. Hosoda S, Uemura A, Shigematsu Y, Yamamoto I, Kojima K. Stud Surf Sci Catal 1994;89:365.
2. Hwang Y-C, Chum S, Guerra R, Sehanobish K. Antec '94 SPE 1994; 111:3414.
3. Sinn H, Kaminsky W. Angew Chem Int Ed 1980;19:390.
4. Mathot V. Polycon '84 LLDPE. London: The Plastics and Rubber Institute, Chameleon Press; 1984. p. 1.
5. Schouterden P, Groeninckx G, van der Heyden B, Jansen F. Polymer 1987;28:2099.
6. Hosoda S. Polym J 1988;20:383.
7. Elston CT. Can Patent 1967;984:213.
8. Hunter BK, Russell KE, Scammell MV, Thompson SL. J Polym Sci Part A: Polym Chem Ed 1984;22:1383.
9. Minick J, Moet A, Hiltner A, Baer E, Chum SP. J Appl Polym Sci 1995;58:1371.
10. Mathot VBF, Scherrenberg RL, Pijpers MFJ, Engelen YMT. In: Hosoda S, editor. New Trends in Polyolefin Science and Technology. Trivandrum (India): Research Signpost; 1996. p. 71. ISBN: 81-86481-12-5.
11. Mathot VBF. In: Mathot VBF, editor. Calorimetry and Thermal Analysis of Polymers. Chapter 9: The Crystallization and Melting Region. Munich/Vienna/New York: Hanser Publishers; 1994. p. 231.
12. Vanden Eynde S, Mathot VBF, Koch MHJ, Reynaers H. Polymer 2000;41:3437. see also p. 4889.
13. Deblieck RAC, Mathot VBF. J Mater Sci Lett 1988;7:1276.
14. Bensason S, Minick J, Moet A, Chum S, Hiltner A, Baer E. J Polym Sci Part B: Polym Phys 1996;34:1301.
15. van Ruiten J, van Dieren F, Mathot VBF. In: Dosière M, editor. Crystallization of Polymers. NATO ASI-C Series, 405, on Mathematical and Physical Sciences; 1993.
16. Carman CJ, Harrington RA, Wilkes CE. Macromolecules 1977;10: 536.
17. Randall JC. J Polym Sci Polym Phys Ed 1977;15:1451.
18. Ray GJ, Johnson PE, Knox JR. Macromolecules 1977;10:773.
19. Horii F, Zhu Q, Kitamaru R, Yamaoka H. Macromolecules 1990;23: 977.
20. Hansen EW, Blom R, Bade OM. Polymer 1997;38:4295.
21. Harris RK. Nuclear magnetic resonance spectroscopy. London: Pitman Books Limited; 1983.
22. Freeman R, Hill HDW, Kaptein R. J Magn Reson 1972;7:327.
23. Galland GB, Mauler RS, de Menezes SC, Quijada R. Polym Bull 1995;34:599.
24. Quijada R, Dupont J, Miranda MSL, Scipioni RS, Galland GB. Macromol Chem Phys 1995;196:3991.
25. Simanke AG, Galland GB, Freitas L, da Jornada JAH, Quijada R, Mauler RS. Polymer 1999;40:5489.
26. Villar MA, Failla MD, Quijada R, Mauler RS, Vallés EM, Galland GB, Quinzani LM. Polymer 2001;42:9269.
27. Prasad JV, Rao PVC, Garg VN. Eur Polym J 1991;27:251.
28. Ottenbourgs BT, Adriaensens PJ, Reekmans BJ, Carleer RA, Vanderzande DJ, Gelan JM. Ind Engng Chem Res 1995;34:1364.
29. Sanders JKM, Hunter BK. Modern NMR spectroscopy. Oxford: Oxford University Press; 1987.
30. Noggle JH, Schirmer RE. The nuclear overhauser effect. New York: Academic Press; 1971.
31. Kalinowski HO, Berger S, Braun S. Carbon-13 NMR spectroscopy. New York: Wiley; 1988.
32. de Pooter M, Smith PB, Dohrer KK, Bennett KF, Meadows MD, Smith CG, Schouwenaars HP, Geerards RA. J Appl Polym Sci 1991; 42:399.
33. Liu W, Rinaldi PL, McIntosh LH, Quirk RP. Macromolecules 2001; 34:4757.
34. Randall JC. J Macromol Sci, Rev Macromol Chem Phys 1989;C29: 201.
35. (a) Mathot VBF, Fabrie ChCM. J Polym Sci, Part B: Polym Phys 1990;28:2487.
36. (b) Mathot VBF, Fabrie ChCM, Tiemersma-Thoone GPJM, van der Velden GPM. J Polym Sci, Part B: Polym Phys 1990; 28:2509.
37. Xu G, Ruckenstein E. Macromolecules 1998;31:4724.
38. Cheng HN. Macromolecules 1984;17:1950.