Neutron and temperature-resolved synchrotron X-ray powder diffraction study of akaganéite

American Mineralogist

Volumn 88, Issue 5, 2003, Pages 782-788

  Post, Jeffrey E ^a   Heaney, Peter J ^b   Von Dreele, Robert B ^c   Hanson, Jonathan C ^d  

^a SMITHSONIAN INSTITUTION   (United States)

^b PENNSYLVANIA STATE UNIVERSITY   (United States)

^c LOS ALAMOS NATIONAL LABORATORY   (United States)

^d BROOKHAVEN NATIONAL LABORATORY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ATOMS; CHLORINE; DIFFRACTION; HEMATITE; HYDROGEN BONDS; METADATA; RIETVELD REFINEMENT; THERMAL EXPANSION; X RAY POWDER DIFFRACTION; X RAYS;

CRYSTAL STRUCTURE REFINEMENT; INTERMEDIATE PHASE; NEUTRON POWDER DIFFRACTION DATA; SEPARATION DISTANCES; SYNCHROTRON X RAY POWDER DIFFRACTION; UNIT CELL PARAMETERS; WEAK HYDROGEN BOND; ZERO THERMAL EXPANSION;

CRYSTAL ATOMIC STRUCTURE;

AKAGANEITE; CRYSTAL STRUCTURE; IRON HYDROXIDE; RIETVELD ANALYSIS;

EID: 0037832483     PISSN: 0003004X     EISSN: None     Source Type: Journal    
DOI: 10.2138/am-2003-5-607     Document Type: Article

References (26)

1. Brown, G.E., Sueno, S., and Prewitt, C.T. (1973) A new single-crystal heater for the precession camera and four-circle diffractometer. American Mineralogist, 58, 698-704.
2. Buchwald, V.F. and Clarke, R.S., Jr. (1989) Corrosion of Fe-Ni alloys by Cl-containing akaganéite (β-FeOOH): the Antarctic meteorite case. American Mineralogist, 74, 656-667.
3. Cai, J., Liu, J., Gao, Z., Navrotsky, A., and Suib, S.L. (2001) Synthesis and anion exchange of tunnel structure akaganéite. Chemistry of Materials, 13, 4595-4602.
4. Calbet, J.M.G. and Franco, M.A.A. (1981) Structural porosity of synthetic akaganéite. Journal of Inorganic Nuclear Chemistry, 43, 257-263.
5. Dezsi, I., Keszthelyi, L., Kulgawczuk, D., Molnar, B., and Eissa, N.A. (1967) Mossbauser study of beta- and delta-FeOOH and their disintegration products. Physica Status Solidi, 22, 617-622.
6. Finger, L.W., Cox, D.E., and Jephcoat, A.P. (1994) A correction for powder diffraction peak asymmetry due to axial divergence. Journal of Applied Crystallography, 27, 892-900.
7. Glasser, L.S.D. and Ingram, L. (1968) Refinement of the crystal structure of groutite, α-MnOOH. Acta Crystallographica, B24, 1233-1236.
8. Gualtieri, A.F. and Venturelli, P. (1999) In situ study of the goethite-hematite phase transformation by real time synchrotron powder diffraction. American Mineralogist, 84, 895-904.
9. Hammersley A.P., Svensson S.O., Hanfland M., Fitch A.N., and Hausermann D. (1996) Two-dimensional detector software: From real detector to idealised image or two-theta scan. High Pressure Research, 14, 235-248.
10. xO (wüstite) in hot brine from the AtlantisII deep (Red Sea) and the uptake of amino acids by synthetc β-FeOOH-Cl. Geochimica et Cosmochimica. Acta, 47, 1465-1470.
11. Ishikawa, T. and Inouye, R. (1975) Role of chlorine in beta-FeOOH on its thermal change and reactivity to sulfur-dioxide. Bulletin of the Chemical Society of Japan, 48, 1580-1584.
12. 16 und Akaganéite. Neues Jahrbuch für Mineralogie Abhandlungen, 113, 29-49.
13. Larson, A.C. and Von Dreele, R.B. (2001) GSAS-General Structure Analysis System. Los Alamos National Laboratory Report No. LAUR 86-748.
14. Mackay, A.L. (1960) β-ferric oxyhydroxise. Mineralogical Magazine, 32, 545-557.
15. Merono, M.D., Morales, J., and Tirado, J.L. (1985) Thermal behavior of synthetic akaganéite under different experimental conditions. Thermochimica Acta, 92, 525-528.
16. Morales, J., Tirado, J.L., and Macias, M. (1984) Changes in crystallite size and microstrains of hematite derived from the thermal decomposition of synthetic akaganéite. Journal of Solid State Chemistry, 53, 303-312.
17. Naono, H., Fujiwara, R., Sugioka, H., Sumiya, K., and Yanazawa, H (1982) Micropore formation due to thermal decomposition of acicular micro-crystals of beta-FeOOH. Journal of Colloid Interface Science, 87, 317-332.
18. Parida, K.M. (1988) Physico-chemical characteristics of thermally treated akaganéite (β-FeOOH). Journal of Material Science, 23, 1201-1205.
19. Post, J.E. and Bish, D.L. (1989) Rietveld refinement of crystal structures using powder X-ray diffraction data. In D.L. Bish and J.E. Post, Eds., Modern Powder Diffraction, 20, 277-308. Reviews in Mineralogy, Mineralogical Society of America, Washington, D.C.
20. Post, J.E. and Buchwald, V.F. (1991) Crystal structure refinement of akaganéite. American Mineralogist, 76, 272-277.
21. Post, J.E., Von Dreele, R.B., and Buseck, P.R. (1982) Symmetry and cation displacements in hollandites: structure refinements of hollandite, cryptomelane, and priderite. Acta Crystallographica, B38, 1056-1065.
22. Stephens, P.W. (1999) Phenomenological model of anisotropic peak broadening in powder diffraction. Journal of Applied Crystallography, 32, 281-289.
23. Szytuta, A., Burewicz, A, Dimitrijevic, Z., Krasnicki, S., Rzany, H., Todorovic, J., and Wolski, W. (1968) Neutron diffraction studies of α-FeOOH. Physica Status Solidi, 26, 429-434.
24. 3. Journal of Applied Crystallography, 20, 79-83.
25. Von Dreele, R.B., Jorgensen, J.D., and Windsor, C. G. (1982) Rietveld refinement with spallation neutron powder diffraction data. Journal of Applied Crystallography, 15, 581-589.
26. Weckler, B. and Lutz, H.D. (1998) Lattice vibration spectra. Part XCV. Infrared spectroscopic studies on the iron oxide hydroxides geothite (α), akaganéite (β), lepidochrosite (γ), and feroxyhite (δ). European Journal of Solid State Inorganic Chemistry, 35, 531-544.