Advances in methodology for the validation of methods according to the International Organization for Standardization: Application to the determination of benzoic and sorbic acids in soft drinks by high-performance liquid chromatography

Journal of Chromatography A

Volumn 992, Issue 1-2, 2003, Pages 11-27

  García, Inmaculada ^a   Ortiz, M Cruz ^a   Sarabia, Luis ^a   Vilches, Carmen ^b   Gredilla, Elisa ^b  

^a UNIVERSITY OF BURGOS   (Spain)

^b Servicio de Programas de Salud y Prevención de la Dirección Técnica de Recursos Humanos y Gestión de Centros Gerencia de Servicios Sociales   (Spain)

Author keywords

Accuracy; Benzoic acid; Chemometrics; Food analysis; Organic acids; Regression analysis; Robust testing; Soft drinks; Sorbic acid; Validation

Indexed keywords

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; NUMERICAL ANALYSIS; ORGANIC ACIDS;

LENTH METHOD;

CHROMATOGRAPHIC ANALYSIS;

BENZOIC ACID DERIVATIVE; SORBIC ACID;

ACCURACY; ANALYTIC METHOD; ARTICLE; BEVERAGE; CALIBRATION; CHEMOMETRIC ANALYSIS; EVALUATION; FOOD ANALYSIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ORGANIZATION; PRIORITY JOURNAL; STANDARDIZATION; VALIDATION PROCESS;

EID: 0037432538     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0021-9673(03)00246-2     Document Type: Article

References (41)

1. International Standard ISO/IEC 17025, General requirements for the competence of testing and calibration laboratories, International Organization for Standardization, Geneva, 1999.
2. International Standard ISO 5725-1, Accuracy (trueness and precision) of measurement methods and results - General Principles and definitions, International Organization for Standardization, Geneva, 1994.
3. International Standard ISO 5725-4, Accuracy (trueness and precision) of measurement methods and results - Basic methods for the determination of the trueness of a standard measurement method, International Organization for Standardization, Geneva, 1994.
4. International Standard ISO 5725-2. Accuracy (trueness and precision) of measurement methods and results - Basic methods for the determination of the repeatability and reproducibility of a standard measurement method, International Organization for Standardization, Geneva, 1994.
5. International Standard ISO 5725-3, Accuracy (trueness and precision) of measurement methods and results - Intermediate measures of the precision of a standard measurement method, International Organization for Standardization, Geneva, 1994.
6. International Standard ISO 5725-5, Accuracy (trueness and precision) of measurement methods and results - Alternative methods for the determination of the precision of a standard measurement method, International Organization for Standardization, Geneva, 1994.
7. International Standard ISO 11843-1, Capability of detection - Terms and definitions. International Organization for Standardization, Geneva, Switzerland, 1997.
8. International Standard ISO 11843-2. Capability of detection - Methodology in the linear calibration case, International Organization for Standardization, Geneva, 2000.
9. Guide, The Fitness for Purpose of Analytical Methods, A Laboratory Guide to Method Validation and Related Topics, EURACHEM, Teddington, UK, 1998.
10. Varman A.H., Sutherland J.P. Beverages - Technology, Chemistry and Microbiology. 1994;Chapman and Hall, London, UK.
11. Method 983.16, Benzoic Acid and Sorbic Acid in Food, Association of Official Analytical Chemists (AOAC), Gaithersburg, MD, 1995.
12. Bui L.V., Cooper C. J. Assoc. Off. Anal. Chem. 70:1987;892.
13. Chen Q.C., Wang J. J. Chromatogr. A. 937:2001;57.
14. Tfouni S.A.V., Toledo M.C.F. Food Control. 13:2002;117.
15. Castineira A., Pena R.M., Herreo C. J. High. Resolut. Chrom. 23:2000;647.
16. Inczédy J., Lengyed T., Ure A.M., Gelencsér A., Hulanicki A. International Union of Pure and Applied Chemistry (IUPAC), Compendium of Analytical Nomenclature. 1998;Blackwell, Oxford.
17. Günzler H. Accreditation and Quality Assurance in Analytical Chemistry. 1996;Springer, Berlin.
18. Sanz M.B., Sarabia L.A., Herrero A., Ortiz M.C. Talanta. 56:2002;1039.
19. Cuadros L., Blanc R., García A.M., Bosque J.M. Chemom. Intell. Lab. Syst. 41:1998;57.
20. Plackett R.L., Burman J.P. Biometrika. 33:1946;305.
21. Montgomery D.C. Design and Analysis of Experiments. 1997;Wiley, New York.
22. Lewis G.A., Mathieu D., Phan-Tan-Luu R. Pharmaceutical Experimental Design. 1999;Marcel Dekker, New York.
23. Youden W.Y. Statistical Techniques for Collaborative Tests. 1972;Association of Official Analytical Chemists (AOAC), Washington.
24. D. Mathieu, J. Nony, R. Phan-Tan-Luu, L. Prai, NEMROD-W, version 99.1, Marseille, 2000.
25. Massart D.L., Vandeginste B.G.M., Buydens L.M.C., De Jong S., Lewi P.J., Smeyers-Verbeke J. Handbook of Chemometrics and Qualimetrics: Part A. 1997;Elsevier, Amsterdam.
26. Lenth R.V. Technometrics. 31:1989;469.
27. Sanz M.B., Sarabia L.A., Herrero A., Ortiz M.C. Talanta. 56:2002;1039.
28. Rousseeuw P.J., Leroy A.M. Robust Regression and Outlier Detection. 1987;Wiley, New York.
29. Ortiz M.C., Arcos J., Juarros J.V., López Palacios J., Sarabia L. Anal. Chem. 65:1993;678.
30. STATGRAPHICS Plus for Windows 4.0. Statistical Graphics Corp.
31. Huber P.J. Robust Statistics. 1981;Wiley, New York.
32. Analyst. 114:1989;1699.
33. Thompson M., Wood R. J. AOAC Int. 76:1993;926.
34. Hampel F.R., Ronchetti E.M., Rousseeuw P.J., Stahel W.A. Robust Statistics: The Approach Based on Influence Functions. 1985;Wiley, Zurich.
35. Sanz M.B., Ortiz M.C., Herrero A., Sarabia L.A. Quim. Anal. 18:1999;117.
36. L.A. Sarabia, M.C. Ortiz, INTERLAB, Burgos, 1995 (available free from the authors).
37. M.C. Ortiz, L.A. Sarabia, in: R. Cela (Ed.), Avances en Quimiometría Práctica. Universidad de Santiago de Compostela: Servicio de Publicaciones e Intercambio Científico. Santiago de Compostela, 1994, p. 189.
38. Horwitz W. Anal. Chim. 67A:1982;54.
39. Ortiz M.C., Sarabia L.A. Trends Anal. Chem. 13:1994;1.
40. Sanz M.B., Sarabia L.A., Herrero A., Ortiz M.C. Anal. Chim. Acta. 446:2001;295.
41. Clayton C.A., Hines J.W., Elkins P.D. Anal. Chem. 59:1987;2506.