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Volumn 43, Issue 35, 2002, Pages 6127-6131

Synthesis of silica-bound amylose by phosphorolytic elongation of immobilised maltoheptaosyl hydrazides

Author keywords

Hydrazides; Immobilised amylose; Maltooligosaccharides; Phosphorolytic synthesis; Silane linkers; Silica gel

Indexed keywords

AMYLOSE; HYDRAZIDE DERIVATIVE; HYDRAZONE DERIVATIVE; SILANE DERIVATIVE; SILICON DIOXIDE;

EID: 0037179179     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(02)01293-5     Document Type: Article
Times cited : (34)

References (37)
  • 22
    • 0010010525 scopus 로고    scopus 로고
    • F 0.19 (n-butanol/methanol/water 4:3:3).
  • 23
    • 0010045982 scopus 로고    scopus 로고
    • 36: C, 44.70; H, 6.44; N, 2.27. Found: C, 44.80; H, 6.87; N, 2.31%.
  • 28
    • 0009972415 scopus 로고    scopus 로고
    • 2 silica surface was added and the suspension gently shaken at 60°C for 72 h. TMS was removed by repeatedly shaking modified silica in 10 ml/g of 0.5 % acetic acid in methanol/water (1:1) for 1 h.
  • 37
    • 0010006777 scopus 로고    scopus 로고
    • HPLC columns (0.4×25 cm) were packed using a Knauer pneumatic dual piston pump (H. Knauer GmbH, Berlin, Germany), and Knauer Vertex cartridges. The HPLC setup consisted of a Waters 6000 pump, Latek 7125 Rheodyne injector, Waters R401 refractory index detector (Waters GmbH, Eschborn, Germany), and a Hewlett-Packard 3390 A recorder/integrator (Hewlett-Packard, Ratingen, Germany); flow rate 0.5 ml/min, pressure 25 bar.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.