Crystallographic characterization of the esterification pathway of group V alkoxides

Polyhedron

Volumn 21, Issue 23, 2002, Pages 2333-2345

  Boyle, Timothy J ^a   Andrews, Nicholas L ^a   Alam, Todd M ^a   Rodriguez, Mark A ^a   Santana, Jessica M ^a   Scott, Brian L ^a  

^a SANDIA NATIONAL LABORATORIES   (United States)

Author keywords

Esterification; Group V; Metal alkoxides; Niobium; Single crystal X ray; Tantalum

Indexed keywords

CARBOXYLATION; ESTERIFICATION; ESTERS; LIGANDS; NIOBIUM; TANTALUM;

ALKOXIDES; CRYSTALLOGRAPHIC CHARACTERIZATION; GROUP V; METAL ALKOXIDES; METAL CENTRES; OXO LIGANDS; REACTION MIXTURE; SINGLE-CRYSTAL X-RAY; STERICALLY DEMANDING; STOICHIOMETRIC REACTION;

SINGLE CRYSTALS;

METAL DERIVATIVE; NIOBIUM; TANTALUM;

ARTICLE; CRYSTAL STRUCTURE; CRYSTALLOGRAPHY; ESTERIFICATION; SOLID STATE; STOICHIOMETRY; STRUCTURE ANALYSIS; TEMPERATURE DEPENDENCE;

EID: 0037108650     PISSN: 02775387     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0277-5387(02)01186-5     Document Type: Article

References (24)

1. D.C. Bradley, R.C. Mehrotra, I.P. Rothwell, A. Singh, Alkoxo and Aryloxo Derivatives of Metals, Academic Press, San Diego, CA. 2001.
2. D.C. Bradley. Chem. Rev. 89 (1989) 1317.
3. D.C. Bradley, R.C. Mehrotra, D.P. Gaur, Metal Alkoxides, Academic Press, New York, 1978.
4. C.D. Chandler, C. Roger, M.J. Hampden-Smith, Chem. Rev. 93 (1993) 1205.
5. L.G. Hubert-Pfalzgraf, New J. Chem. II (1987) 663.
6. I. Gautier-Luneau, A. Mosset, J. Galy, Z. Kristallogr. 180 (1987) 83.
7. S. Doeuff, Y. Dromzee, F. Taulelle, C. Sanchez, Inorg. Chem. 28 (1989) 4439.
8. S. Doeuff, Y. Dromzee, C. Sanchez, C.R. Acad. Sci. Paris 308 (1989) 1409.
9. T.J. Boyle, R.P. Tyner, T.M. Alam, B.L. Scott, J.W. Ziller, B.G. Potter, Jr., J. Am. Chem. Soc. 121 (1999) 12104.
10. T.J. Boyle, T.M. Alam, C.J. Tafoya, B.L. Scott, Inorg. Chem. 37 (1998) 5588.
11. U. Schubert, E. Arpac, W. Glaubitt, A. Helmerich, C. Chau, Chem. Mater. 4 (1992) 291.
12. I. Laaziz, A. Larbot, C. Guizard, J. Durand, L. Cot, J. Joffre, Acta Crystallogr., Sect. C 46 (1990) 2332.
13. X. Lei, M. Shang, T.P. Fehlner, Organometallics 15 (1996) 3779.
14. T.J. Boyle, T.M. Alam, E.R. Mechenbeir, B. Scott, J.W. Ziller, Inorg. Chem. 36 (1997) 3293.
15. T.J. Boyle, T.M. Alam, D. Dimos, G.J. Moore, C.D. Buchheit, H.N. Al-Shareef, E.R. Mechenbier, B.R. Bear, Chem. Mater. 9 (1997) 3187.
16. T.J. Boyle, D.M. Pedrotty, B. Scott, J.W. Ziller, Polyhedron 17 (1997) 1959.
17. T.J. Boyle, J.J. Gallegos, III, D.M. Pedrotty, E.R. Mechenbier, B.L. Scott, J. Coord. Chem. 47 (1999) 155.
18. T.J. Boyle, T.M. Alam, C.J. Tafoya, E.R. Mechenbeir, J.W. Ziller, Inorg. Chem. 38 (1999) 2422.
19. T.J. Boyle, T.M. Alam, M.A. Rodriguez, C.A. Zechmann, Inorg. Chem. 91 (2002) 2574.
20. T.J. Boyle, T.M. Alam, K.P. Peters, M.A. Rodriguez, Inorg. Chem. 40 (2002) 6281.
21. L.G. Hubert-Pfalzgraf, V. Abada, S. Halut, J. Roziere, Polyhedron 16 (1997) 581.
22. D.D. Perrin, W.L.F. Armarego, Purification of Laboratory Chemicals, Pergamon Press, New York, 1988.
23. The listed versions of SAINT, SMART, XSHELL, and SADABS Software from Bruker Analytical X-Ray Systems Inc., 6300 Enterprise Lane, Madison, WI 53719 were used in analysis.
24. R.D. Shannon, Acta Crystallogr., Sect. A A32 (1976) 751.