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0011987876
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See Supporting Information for details
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See Supporting Information for details.
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24
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0346541206
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Minami, I.; Takahashi, K.; Shimizu, I.; Kimura, T.; Tsuji, J. Tetrahedron 1986, 42, 2971 and references therein.
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27
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0011918073
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note
-
Both diastereomers were expected to be applicable to the synthesis because the C16 stereocenter can be epimerized during the last stage. Unexpected aromatization, however, proceeded in the next iodination step when 14β was used.
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-
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28
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0011947583
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note
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(2-Nitrophenyl)ketone moiety was selected as a latent form of the indoline based on the previous results, see ref 4g.
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29
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0025779899
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Easy retro-1,4-additions of 8-aryl-2-azabicyclo[3.3.1]nonan-7-ones were reported, see: Bonjoch, J.; Quirante, J.; Solé, D.; Castells, J.; Galceran, M.; Bosch, J. Tetrahedron 1991, 47, 4417.
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30
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0000366419
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Trost, B. M., Fleming, I., Eds.; Pergamon: Oxford; Chapter 4.3
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For a general review, see: Caubère, P.; Coutrot, P. In Comprehensive Organic Synthesis; Trost, B. M., Fleming, I., Eds.; Pergamon: Oxford, 1991; Chapter 4.3, Vol. 8, p 835.
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Caubère, P.1
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31
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4243746641
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and references therein
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The transformation of strychnine to neostrychnine by normal Raney Ni in EtOH was reported, see: Beddoes, R. L.; Gorman, A. A.; Prescott, A. L. Acta Crystallogr. 1994, C50, 447 and references therein.
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0021684854
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