Simple and facile reduction of azides to amines: Synthesis of DNA interactive pyrrolo[2,1-c][1,4]benzodiazepines

Tetrahedron Letters

Volumn 43, Issue 37, 2002, Pages 6629-6631

  Kamal, Ahmed ^a   Reddy, P S M M ^a   Reddy, D Rajasekhar ^a  

^a INDIAN INSTITUTE OF CHEMICAL TECHNOLOGY   (India)

Author keywords

Amines; Hydriodic acid; Pyrrolobenzodiazepines; Reductive cyclization

Indexed keywords

ACID; AMINE; AZIDE; BENZODIAZEPINE DERIVATIVE; HYDRIODIC ACID; UNCLASSIFIED DRUG;

ARTICLE; DRUG STRUCTURE; DRUG SYNTHESIS; METHODOLOGY; REDUCTION;

EID: 0037048481     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(02)01453-3     Document Type: Article

References (18)

1. Scriven E.V., Turnbull K. Chem. Rev. 88:1988;297.
2. Smith S.C., Heathcock C.H. J. Org. Chem. 57:1992;6339.
3. McDonald F.E., Danishefsky S.J. J. Org. Chem. 57:1992;7001.
4. Ito M., Koyakumaru K., Tayaka T.H. Synthesis. 1995;376.
5. Rao H.S.P., Siva P. Synth. Commun. 24:1994;549.
6. Alvarez S.G., Fisher G.B., Singavam B. Tetrahedron Lett. 36:1995;2567.
7. Molina P., Diaz I., Tarraga A. Tetrahedron. 51:1995;5617.
8. Ramesha A.R., Bhat S., Chandrasekaran S. J. Org. Chem. 60:1995;7682.
9. Capperucci A., Degl' Innocenti A., Funicello M., Mauriello G., Scafato P., Spagnolo P. J. Org. Chem. 60:1995;2254.
10. Kamal A., Reddy B.S.P., Reddy B.S.N. Tetrahedron Lett. 37:1996;6803.
11. Huang Y., Zhang Y., Wang Y. Tetrahedron Lett. 38:1997;1065.
12. Molander G.A. Chem. Rev. 92:1992;29.
13. Kamal A., Rao N.V., Laxman E. Tetrahedron Lett. 38:1997;6945.
14. Krasnec L. Z. Chem. 11:1971;110.
15. Kumar J.S.D., Ho M.M., Toyokuni T. Tetrahedron Lett. 42:2001;5601.
16. Gregson S.J., Howard P.W., Hartley J.A., Brooks N.A., Adams L.J., Jenkins T.C., Kelland L.R., Thurston E. J. Med. Chem. 44:2001;737.
17. Kamal A., Rao M.V., Laxman N., Ramesh G., Reddy G.S.K. Curr. Med. Chem. Anti-Cancer Agents. 2:2002;215.
18. +, 100), 171, 144, 103, 70, 43.