Improved gas chromatographic-mass spectrometric determination of the N-methylcarbamoyl adduct at the N-terminal valine of globin, a metabolic product of the solvent N, N-dimethylformamide

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 778, Issue 1-2, 2002, Pages 357-365

  Mráz, Jaroslav ^a   Dušková, Šárka ^a   Gálová, Eva ^a   Nohová, Hana ^a   Krausová, Pavla ^a   Linhart, Igor ^b   Šimek, Petr ^c  

^a NATIONAL INSTITUTE OF PUBLIC HEALTH   (Czech Republic)

^b INSTITUTE OF CHEMICAL TECHNOLOGY   (Czech Republic)

^c INSTITUTE OF ENTOMOLOGY   (Czech Republic)

Author keywords

Globin; N, N Dimethylformamide; N Methylcarbamoylvaline adduct

Indexed keywords

AMINO ACIDS; DEGRADATION; GAS CHROMATOGRAPHY; MASS SPECTROMETRY;

BIOLOGICAL MONITORING;

ORGANIC COMPOUNDS;

3 METHYL 5 ISOBUTYLHYDANTOIN; 3 METHYL 5 ISOPROPYLHYDANTOIN; GLOBIN; HYDANTOIN DERIVATIVE; N METHYLCARBAMOYLVALINE; N,N DIMETHYLFORMAMIDE; UNCLASSIFIED DRUG; VALINE;

ACCURACY; AMINO TERMINAL SEQUENCE; ANALYTIC METHOD; ARTICLE; BIOLOGICAL MONITORING; BLOOD ANALYSIS; CALIBRATION; CONTROLLED STUDY; DEGRADATION; GAS CHROMATOGRAPHY; HEMOLYSIS; HUMAN; HYDROLYSIS; MALE; MASS SPECTROMETRY; MODEL; NONHUMAN; NORMAL HUMAN; OCCUPATIONAL EXPOSURE; PRIORITY JOURNAL; RAT; STANDARD; SYNTHESIS; VALIDATION PROCESS;

CALIBRATION; DIMETHYLFORMAMIDE; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GLOBINS; HEMOLYSIS; HUMANS; REPRODUCIBILITY OF RESULTS; SOLVENTS; VALINE;

EID: 0037027023     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0378-4347(01)00455-8     Document Type: Article

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