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Tetrahedron Letters

Volumn 43, Issue 32, 2002, Pages 5611-5615

Synthesis of 4-pentenoic and 5-hexenoic acids on polystyrene resin and their use as cleavable linkers

(2) Guo, MaoJun a Varady, Laszlo a

a ARQULE INC (United States)

Author keywords

[No Author keywords available]

Indexed keywords

4 PENTENOIC ACID; ACID; POLYSTYRENE;

ARTICLE; COMBINATORIAL CHEMISTRY; EXTRACTION; SOLID; SYNTHESIS;

EID: 0037025764 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(02)01111-5 Document Type: Article

Times cited : (4)

References (25)

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11
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- Merrifield resin was purchased from Novabiochem, loading 1.20 mmol/g

12
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- PS-Benzaldehyde was purchased from Argonaunt, loading 1.29 mmol/g. It was dried at 50°C overnight under vacuum

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14
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- 4NOH in methanol (2 equiv.) was added and the suspension was kept under reflux for 48 h with stirring. After removing liquid and washed with THF, the resin was suspended in THF containing 10% concentrated HCl and stirred at room temperature for 1 h. Liquid was drained and resin was washed with THF. The resin was dried in vacuum at 50°C overnight

15
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- The reagent is 5 equiv. to the resin's loading

16
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- 4-Bromobutyric acid and triphenyl phosphine dissolved in THF and kept under reflux for 3 days. After removing volatile, the resulting (3-carboxypropyl) triphenylphosphonium bromide (6) was used directly

17
- 0005675810
- The reagent is 1.5 equiv. to the resin's loading

18
- 0005765415
- N-Methylaminomethyl polystyrene was purchased from Novabiochem, loading 1.13 mmol/g

19
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- note

20
- 0005736056
- note

21
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- Varady, L.¹ Rajur, S.B.² Nicewonger, R.B.³ Guo, M.-J.⁴ Ditto, L.⁵

22
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- note

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- note

24
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- Frechet, J.M.J.¹ Schuerch, C.²

25
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- Andrade, R.B.¹ Plante, O.J.² Melean, L.G.³ Seeberger, P.H.⁴

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.