Quantification of pantothenic acid and folates by stable isotope dilution assays

Journal of Food Composition and Analysis

Volumn 15, Issue 4, 2002, Pages 399-409

  Rychlik, Michael ^a   Freisleben, Achim ^a  

^a DEUTSCHE FORSCHUNGSANSTALT FÜR LEBENSMITTELCHEMIE   (Germany)

Author keywords

Folates; Pantothenic acid; Stable isotope dilution assay; Water soluble vitamins

Indexed keywords

5 METHYLTETRAHYDROFOLIC ACID; DEUTERIUM; ENZYME; FOLIC ACID DERIVATIVE; FOLINIC ACID; ISOTOPE; PANTOTHENIC ACID; PTEROPTIN; STARCH; TETRAHYDROFOLIC ACID DERIVATIVE; TRIMETHYLSILYL DERIVATIVE; VITAMIN;

APPLE JUICE; ARTICLE; BROCCOLI; CONJUGATE; CONJUGATION; CONTROLLED STUDY; DATA ANALYSIS; DERIVATIZATION; FOOD ANALYSIS; FOOD COMPOSITION; GAS CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROLYSIS; ISOTOPE DILUTION ASSAY; ISOTOPE LABELING; MASS SPECTROMETRY; MILK; PUBLICATION; QUANTITATIVE ANALYSIS; RICE; SCIENTIFIC LITERATURE; SEPARATION TECHNIQUE; SPINACH; STANDARD; SYNTHESIS;

BRASSICA OLERACEA VAR. BOTRYTIS; MALUS X DOMESTICA; SPINACIA OLERACEA;

EID: 0036668875     PISSN: 08891575     EISSN: None     Source Type: Journal    
DOI: 10.1006/jfca.2002.1081     Document Type: Article

References (26)

1. Aiso, K. and Tamura, T. (1998). Trienzyme treatment for food folate analysis: optimal pH and incubation time for alpha-amylase and protease treatments. J. Nutr. Sci. Vitaminol. 44, 361-370.
2. Banno, K., Matsuoka, M., Horimoto, S., and Kato, J. (1990). Simultaneous determination of pantothenic acid and hopantenic acid in biological samples and natural products by gas chromatography-mass fragmentography. J. Chromatogr. 525, 255-264.
3. Bell, J. G. (1974). Microbiological assay of vitamins of the B group in foodstuffs. Laboratory Practice 23, 235-241.
4. Finglas, P. M., Faure, U., and Southgate, D. A. T. (1993). First BCR [Community Bureau of Reference]-intercomparison on the determination of folates in food. Food Chem. 46, 199-213.
5. Freisleben, A., Schieberle, P., and Rychlik, M. (2002). Syntheses of vitamers of folic acid to be used as internal standards in stable isotope dilution assays, J. Agric. Food Chem., in press.
6. Gounelle, J.-C., Ladjimi, H., and Prognon, P. (1989). A rapid and specific extraction procedure for folates - determination in rat liver and analysis by high-performance liquid chromatography with fluorimetric detection. Anal. Biochem. 176, 406-411.
7. 6 in biological samples by isotope dilution mass spectrometry. Anal. Biochem. 151, 159-168.
8. Haenel, H. (1956). Pantothenic acid in foods. Ernährungsforschung 1, 533.
9. Holland, B., Welch, A. A., Unwin, I. D., Buss, D. H., Paul, A. A., and Southgate, D. A. T. (1999). McCance and Widdowson's The Composition of Foods, 5th edn. The Royal Society of Chemistry and Ministry of Agriculture, Fisheries and Food, Cambridge.
10. Møoller, A. (1996). Levnedsmiddeltabeller. Levnedsmiddelstyrelsen, Søborg, Denmark.
11. Müller, H. (1993). Determination of folic acid contents in vegetables and fruits by HPLC. Z. Lebensm. Unters. Forsch. 196, 137-141.
12. Pawlosky, R. J. and Flanagan, V. P. (2001). A quantitative stable-isotope LC-MS method for the determination of folic acid in fortified foods. J. Agric. Food Chem. 49, 1282-1286.
13. Pawlosky, R. J., Flanagan, V. P., and Pfeiffer, C. M. (2001). Determination of 5-methyltetrahydrofolic acid in human serum by stable-isotope dilution high-performance liquid chromatography-mass spectrometry. Anal. Biochem. 298, 299-305.
14. Rychlik, M. (2000). Quantification of free and bound pantothenic acid in foods and blood plasma by a stable isotope dilution assay. J. Agric. Food Chem. 48, 1175-1181.
15. Rychlik, M. (2001). Mass spectrometric studies of trimethylsilylpantothenic acid and related substances. J. Mass Spectrom. 36, 556-562.
16. Rychlik, M. and Grosch, W. (1996). Identification and quantification of potent odorants formed by toasting of wheat bread. Lebensm. Wiss. Technol. 29, 515-525.
17. Rychlik, M. and Schieberle, P. (1999). Quantification of the mycotoxin patulin by a stable isotope dilution assay. J. Agric. Food Chem. 47, 3749-3755.
18. Song, W. O., Wyse, B. W. and Hansen, R.G. (1985). Pantothenic acid status of pregnant and lactating women. J. Am. Diet. Assoc. 85, 192-198.
19. Song, W. O., Smith, A., Wittwer, C., Wyse, B. W., and Hansen, R. G. (1990). Determination of plasma pantothenic acid by indirect enzyme linked immunosorbent assay. Nutr. Res. 10, 439-448.
20. Souci, S. W., Fachmann, W., and Kraut, H. (1994). Food Composition and Nutrition Tables. Medpharm Scientific Publishers, Stuttgart, Germany.
21. Srinivasan, V. and Belavady, B. (1976). Nutritional status of pantothenic acid in Indian pregnant and nursing women. Int. J. Vitam. Nutr. Res. 46, 433-438.
22. Stokes, P. and Webb, K. (1999). Analysis of some folate monoglutamates by high-performance liquid chromatography-mass spectrometry. J. Chromatogr. 864, 59-67.
23. Taylor, E. C., Henrie, R. N. and Portnoy, R. C. (1978). Pteridines. 44. A convenient synthesis of 6-formylpterin. J. Org. Chem. 43, 736-737.
24. US Department of Agriculture (2001). Agricultural Research Service, USDA Nutrient Database for Standard Referenee, Release 14, 2001. World Wide Web: http://www.nal.usda.gov/fnic.
25. Vahteristo, L., Lehikoinen, K., Ollilainen, V., and Varo, P. (1997). Application of an HPLC assay for the determination of folate derivatives in some vegetables, fruits and berries consumed in Finland. Food Chem. 59, 589-597.
26. Wilson, S. D. and Horne, D. W. (1984). High-performance liquid chromatographic determination of the distribution of naturally occurring folic acid derivatives in rat liver. Anal. Biochem. 142, 529-535.