In situ infrared measurements on TiO2 flames: Gas and particle concentrations

AIChE Journal

Volumn 48, Issue 1, 2002, Pages 59-68

  Arabi Katbi, Osama I ^a,d   Pratsinis, Sotiris E ^a,c   Morrison Jr , Philip W ^b  

^a University of Cincinnati   (United States)

^b Case Western Reserve University ^*  (United States)

^c ETH ZURICH   (Switzerland)

^d Degussa Corporation   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ABSORPTION; CONCENTRATION (PROCESS); FOURIER TRANSFORM INFRARED SPECTROSCOPY; SOOT; TEMPERATURE MEASUREMENT; THERMOCOUPLES;

SURFACE TEMPERATURE;

TITANIUM OXIDES;

CARBON DIOXIDE; METHANE; OXYGEN; TITANIUM DERIVATIVE; TITANIUM TETRAISOPROPOXIDE; UNCLASSIFIED DRUG; WATER;

FLAME; INFRARED SPECTROSCOPY;

ABSORPTION; ARTICLE; CALCULATION; COMPARATIVE STUDY; CONCENTRATION (PARAMETERS); DATA BASE; EMISSION TOMOGRAPHY; FIRE; FLAME PHOTOMETRY; GAS; INFRARED SPECTROSCOPY; MEASUREMENT; MOLECULAR DYNAMICS; PARTICLE SIZE; SOOT; TEMPERATURE; TEMPERATURE MEASUREMENT; THERMODYNAMICS; VALIDATION PROCESS;

EID: 0036160240     PISSN: 00011541     EISSN: None     Source Type: Journal    
DOI: 10.1002/aic.690480108     Document Type: Article

References (26)

1. Arabi-Katbi, O. I., S. E. Pratsinis, P. W. Morrison, Jr., and C. M. Megaridis, "Monitoring of Flame Synthesis of Titania Nanoparticles by In Situ Fourier Transform Infrared (FTIR) Spectroscopy and Thermophoretic Sampling," Combust. Flame, 124, 560 (2000).
2. Arabi-Katbi, O. I., "Flame Synthesis of Titania Nanoparticles: Analysis Using In Situ Fourier Transform Infrared (FTIR) Spectroscopy and Thermophoretic Sampling," MS Thesis, Univ. of Cincinnati, Cincinnati, OH (1999).
3. Bengtsoon, P. E., L. Martinsoon, M. Alden, and S. Kröll, "Rotational CARS Thermometry in Sooty Flames," Comb. Sci. Technol., 81, 129 (1992).
4. Best, P. E., R. M. Carangelo, J. R. Markham, and P. R. Solomon, "Extension of Emission-Transmission Technique to Particulate Samples Using FT-IR," Combust. Flame, 66, 47 (1986).
5. Best, P. E., P. L. Chien, R. M. Carangelo, P. R. Solomon, M. Danchak, and I. Ilovici, "Tomographic Reconstruction of FT-IR Emission and Transmission Spectra in a Sooty Laminar Diffusion Flame: Species Concentration and Temperatures," Combust. Flame, 85, 309 (1991).
6. Boedeker, L. R., and G. M. Dobbs, "Soot Distribution and CARS Temperature Measurements in Axisymmetric Laminar Diffusion Flames with Several Fuels," Proc. Int. Symp. on Combustion, The Combustion Institute, Baltimore, p. 1097 (1986).
7. Bohren, C. F., and D. R. Huffman, Absorption and Scattering of Light by Small Particles, Wiley, New York (1983).
8. Collis, D. C., and M. J. Williams, "Two-Dimensional Convection from Heated Wires at Low Reynolds Numbers," J. Fluid Mech., 6, 357 (1959).
9. Farrow, R. L., R. P. Lucht, W. L. Flower, and R. E. Palmer, "Coherent Anti-Stokes Raman Spectroscopic Measurements of Temperature and Acetylene Spectra in a Sooting Diffusion Flame," Proc. Int. Symp. on Combustion, The Combustion Institute, Baltimore, p. 1307 (1984).
10. Govatzidakis, G. J., "Thermocouple Thermometry in Soot Bearing Flames," BS Thesis, Brown University, Providence, RI (1993).
11. Griffiths, G. J., and J. A. de Haseth, Fourier Transform Infrared Spectrometry, Wiley, New York (1986).
12. Kent, J. H., and H. G. Wagner, "Why Do Diffusion Flames Emit Smoke?" Comb. Sci. TechnoL, 41, 245 (1984).
13. Köylu, Ü. Ö., and G. M. Faeth, "Spectral Extinction Coefficients of Soot Aggregates from Turbulent Diffusion Flames," J. Heat Transfer, 118, 415 (1996).
14. Lide, D. R., CRC Handbook of Chemistry and Physics, 72nd ed., CRC Press, Boston, MA (1982).
15. 2 Coated Thermocouples," Comb. Sci. Technol., 36, 205 (1984).
16. Markham, J. M., Y. P. Zhang, R. M. Carangelo, and P. R. Solomon, "FT-IR Emission/Transmission Tomography of a Coal Flame," Proc. Int. Symp. on Combustion, The Combustion Institute, Baltimore, p. 1869 (1990).
17. Morrison, P. W., Jr., and J. R. Haigis, "In Situ Infrared Measurements of Film and Gas Properties During the Plasma Deposition of Amorphous Hydrogenated Silicon," J. Vac. Sci. Technol. A, 11, 490 (1993).
18. 2 Particles," Chem. Mater., 9, 2702 (1997).
19. Morrison, P. W., Jr., J. E. Cosgrove, J. R. Markham, and P. R. Solomon, "In Situ IR Spectroscopy of an Oxygen-Acetylene Flame During Diamond Film Growth," Carbon, 28, 767 (1990).
20. Morrison, P. W., Jr., and O. Taweechokesupsin, "Calculation of Gas Spectra for Quantitative Fourier Transform Infrared Spectroscopy of Chemical Vapor Deposition," J. Electrochem. Soc., 145, (9), 3212 (1998).
21. Solomon, P. R., P. E. Best, R. M. Carangelo, J. R. Markham, P-L. Chien, R. J. Santoro, and H. G. Semerjian, "FT-IR Emission/Transmission Spectroscopy for In Situ Combustion Diagnostics," Proc. Int. Symp. on Combustion, The Combustion Institute, Baltimore, p. 1763 (1986).
22. Solomon, P. R., and P. E. Best, "Fourier Transform Infrared Emission/Transmission Spectroscopy in Flames," Combustion Measurements, N. Chigier, ed., Hemisphere Publishing Corp., New York, pp. 385-444 (1991).
23. Rothman, L. S., R. Gamache, A. Goldman, L. Brown, R. Toth, H. Pickett, R. Poynter, J. Flaud, C. Camy-Peyret, A. Barbe, N. Husson, C. Rinsland, and M. Smith, "The HITRAN Database: 1986 Edition," Appl. Opt., 26, 4058 (1987).
24. Rothman, L., R. Gamache, R. Tipping, C. Rinsland, M. Smith, D. Benner, V. Malathy Devi, J. M. Flaud, C. Camy-Peyret, A. Perrin, A. Goldman, S. Massie, L. Brown, and R. Toth, "The HITRAN Molecular Database: Edition of 1991 and 1992," J. Quant. Spectrosc. Radiat. Transfer, 48, 469 (1992).
25. Vemury, S., and S. E. Pratsinis, "Charging and Coagulation During Flame Synthesis of Silica," J. Aerosol Sci., 27, 951 (1996).
26. Vijayakumar, R., and K. T. Whitby, "Flat Flame Ultrafine Aerosol Generator," Aerosol Sci. Technol., 3, 17 (1984).