Analysis of oligosaccharide conformation by NMR spectroscopy utilizing 1H,1H and 1H,13c residual dipolar couplings in a dilute liquid crystalline phase

Journal of Physical Chemistry A

Volumn 105, Issue 21, 2001, Pages 5119-5122

  Lycknert, Kristina ^a   Maliniak, Arnold ^a   Widmalm, Göran ^a  

^a STOCKHOLM UNIVERSITY   (Sweden)

Author keywords

[No Author keywords available]

Indexed keywords

COMPUTER SIMULATION; CONFORMATIONS; LIQUID CRYSTALS; MAGNETIC COUPLINGS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SPECTRUM ANALYSIS;

NUCLEAR OVERHAUSER EFFECT (NOE); OLIGOSACCHARIDES;

MOLECULAR ORIENTATION;

EID: 0035979117     PISSN: 10895639     EISSN: None     Source Type: Journal    
DOI: 10.1021/jp0103068     Document Type: Article

References (31)

1. Emsley, J. W., Ed. In Nuclear Magnetic Resonance of Liquid Crystals; Reidel: Dordrecht, The Netherlands, 1985.
2. Tjandra, N.; Bax, A. Science 1997, 278, 1111-1114.
3. Hansen, M. R.; Mueller, L.; Pardi, A. Nat. Struct. Biol. 1998, 5, 1065-1074.
4. Sass, J.; Cordier, F.; Hoffmann, A.; Rogowski, M.; Cousin, A.; Omichinski, J. G.; Löwen, H.; Crzesiek, S. J. Am. Chem. Soc. 1999, 121, 2047-2055.
5. Ram, P.; Mazzola, L.; Prestegard, J. H. J. Am. Chem. Soc. 1989, 111, 3176-3182.
6. Rundlöf, T.; Landersjö, C.; Lycknert, K.; Maliniak, A.; Widmahn, G. Magn. Reson. Chem. 1998, 36, 773-776.
7. Bolon, P. J.; Prestegard. J. H. J. Am. Chem. Soc. 1998, 120, 9366-9367.
8. Kiddle, G. R.; Homans, S. W. FEBS Lett. 1998, 436, 128-130.
9. Martin-Pastor, M.; Bush, C. A. Carbohydr. Res. 2000, 323, 147-155.
10. Martin-Pastor, M.; Bush, C. A. Biochemistry 2000, 39, 4674-4683.
11. Landersjö, C.; Höög, C.; Maliniak, A.; Widmalm, G. J. Phys. Chem. B 2000, 104, 5618-5624.
12. Tian, F.; Al-Hashimi, H. M.; Caighead, J. L.; Prestegard, J. H. J. Am. Chem. Soc. 2001, 123, 485-492.
13. Staaf, M.; Höög, C.; Stevensson, B.; Maliniak, A.; Widmalm, G. Biochemistry 2001, 40, 3623-3628.
14. Tian, F.; Bolon, P. J.; Prestegard, J. H. J. Am. Chem. Soc. 1999, 121, 7712-7713.
15. Peti, W.; Griesinger, C. J. Am. Chem. Soc. 2000, 122, 3975-3976.
16. Hällgren, C.; Widmalm, G. J. Carbohydr. Chem. 1993, 12, 309-333.
17. Kupce, E.; Boyd, J.; Campbell, I. D. J. Magn. Reson., Ser. B 1995, 106, 300-303.
18. Stott, K.; Keeler, J.; Van, Q. N.; Shaka, A. J. J. Magn. Reson. 1997, 125, 302-324.
19. Willker, W.; Leibfritz, D.; Kerssebaum, R.; Bermel, W. Magn. Reson. Chem. 1993, 33, 287-292.
20. Porte, G.; Gomati, R.; El Haitamy, O.; Appell, J.; Marignan, J. J. Phys. Chem. 1986, 90, 5746-5751.
21. Piantini, U.; Sørensen, O. W.; Ernst, R. R. J. Am. Chem. Soc. 1982, 104, 6800-6801.
22. McIntyre, L.; Freeman, R. J. Magn. Reson. 1992, 96, 425-431.
23. del Río-Portilla, F.; Blechta, V.; Freeman, R. J. Magn. Reson., Ser. A 1994, 111, 132-135.
24. Rundlöf, T.; Kjellberg, A.; Damberg, C.; Nishida, T.; Widmalm, G. Magn. Reson. Chem. 1998, 36, 839-847.
25. Jones, J. A.; Grainger, D. S.; Hore, P. J.; Daniell, G. J. J. Magn. Reson., Ser. A 1993, 101, 162-169.
26. Garca-García, A.; Ponzanelli-Velázquez, G.; del Río-Portilla, F. J. Magn. Reson. 2001, 148, 214-219.
27. Komolkin, A. V.; Laaksonen, A.; Maliniak, A. J. Chem. Phys. 1994, 101, 4103-4116.
28. Stuike-Prill, R.; Meyer, B. Eur. J. Biochem. 1990, 194, 903-919.
29. Thøgersen, H.; Lemieux. R. U.; Bock, K.; Meyer, B. Can. J. Chem. 1982, 60, 44-57.
30. Tjandra, N.; Tate, S.-i.; Ono, A.; Kainosho, M.; Bax, A. J. Am. Chem. Soc. 2000, 122, 6190-6200.
31. Asensio, J. L.; Cañada, F. J.; Cheng, X.; Khan, N.; Mootoo, D. R.; Jiménez-Barbero. J. Chem. Eur. J. 2000, 6, 1035-1041.