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0042272356
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note
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4/THF) followed by oxidation with TPAP/NMO.
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7
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0000476716
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Blanchette, M. A.; Choy, W.; Davis, J. T.; Essenfeld, A. P.; Masamune, S.; Roush, W. R.; Sakai, T. Tetrahedron Lett. 1984, 25, 2183.
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84986384797
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Barium manganate is a mild and effective oxidant for the conversion of dienols to dienones: (a) Denmark, S. E.; Hite, G. A. Helv. Chim. Acta 1988, 71, 195.
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0043274754
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See also ref 9a
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(c) See also ref 9a.
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0345520231
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(a) Bender, J. A.; Blize, A. E.; Browder, C. C.; Giese, S.; West, F. G. J. Org. Chem. 1998, 63, 2430.
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15
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0041771570
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note
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3, 125 MHz) δ 221.6, 146.3, 146.3, 129.1, 128.4., 108.8, 108.4, 100.9, 56.6, 51.9, 48.8, 33.3, 27.2, 25.1, 21.9, 18.4, 17.7, 11.2.
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16
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0001992172
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0000646877
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Trost, B. M., Fleming, I., Eds.; Pergamon: Oxford
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(b) Denmark, S. E. In Comprehensive Organic Synthesis; Trost, B. M., Fleming, I., Eds.; Pergamon: Oxford, 1991; Vol. 5, pp 751-784.
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Denmark, S.E.1
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18
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0041771571
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note
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For other examples of selective protonation from the convex face of the enolate intermediate, see refs 4, 5, and 9a.
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19
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0000059738
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(a) Tanis, S. P.; Deaton, M. V.; Dixon, L. A.; McMills, M. C.; Raggon, J. W.; Collins, M. A. J. Org. Chem. 1998, 63, 6914.
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4243952009
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31
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0042773459
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note
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We thank an anonymous reviewer for the suggestion of this intriguing possibility.
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