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6]acetone, 298 K): δ = 82.7.
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0343699693
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int = 0.1570) and were used in all calculations. Final R = 0.0842 (for observed data with 1 > 2σ(I)). Cristallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-155449. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: (+44)1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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