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0011492215
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note
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2 gives 2 along with ca. 30% of unidentified side-products.
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15
-
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0011484669
-
-
note
-
31P NMR.
-
-
-
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16
-
-
0011435106
-
-
note
-
1H} N•IR spectrum. The complex was not isolated due to fast decomposition in solution (half-life ca. 6 h in THF at 20 °C), leading to the formation of a mixture of unidentified products.
-
-
-
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18
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0000188543
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Herold, S.; Mezzetti, A.; Venanzi, L. M.; Albinatti, A.; Lianza, F.; Gerfin, T.; Gramlich, V. Inorg. Chim. Acta 1995, 235, 215.
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19
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0034300998
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and references therein
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Stoop, R.M.1
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20
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0011490891
-
-
note
-
10 in THF at -40 °C.
-
-
-
-
21
-
-
0011392195
-
-
note
-
2 was confirmed by collecting the released gas and GC analysis.
-
-
-
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22
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0001181882
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and references therein
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Slugovc, C.; Mereiter, K.; Schmid, R.; Kirchner, K. Organometallics 1998, 17, 827, and references therein.
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Slugovc, C.1
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23
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0001269602
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The values of cis P-N and trans P-N constants in metallo-complexes normally lie within 0-6 Hz and 25-95 Hz, respectively. See for example: Kuznetsov, V. F. Facey, G. A.; Yap, G. P. A.; Alper, H. Organometallics 1999, 18, 4706.
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25
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0006037880
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(c) Heaton, B. T.; Jacob, C.; Monks, G. L.; Hursthouse M. B.; Ghatak, I.; Somervile, R. G.; Heggie, W.; Page, P. R.; Villax, I. J. Chem. Soc., Dalton Trans. 1996, 61.
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0000513455
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0001126655
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29
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0001287342
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and references therein
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31
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0011490892
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-
note
-
Addition of seed crystals leads to complete crystallization within 3 h, otherwise it may take several days.
-
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33
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0011394098
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Sheldrick, G.M.1
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