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Volumn 153, Issue 1, 2001, Pages 83-91

Deuterium stimulated-echo-type PGSE NMR experiments for measuring diffusion: Application to a liquid crystal

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ARTICLE;

EID: 0035742318     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.2001.2418     Document Type: Article
Times cited : (27)

References (55)
  • 1
    • 33646376290 scopus 로고
    • Spin diffusion measurements: Spin echoes in the presence of a time-dependent field gradient
    • E.O. Stejskal J.E. Tanner Spin diffusion measurements: Spin echoes in the presence of a time-dependent field gradient J. Chem. Phys. 42 1965 288 292
    • (1965) J. Chem. Phys. , vol.42 , pp. 288-292
    • Stejskal, E.O.1    Tanner, J.E.2
  • 2
    • 36849101148 scopus 로고
    • Use of the stimulated echo in NMR diffusion studies
    • J.E. Tanner Use of the stimulated echo in NMR diffusion studies J. Chem. Phys. 52 1970 2523 2526
    • (1970) J. Chem. Phys. , vol.52 , pp. 2523-2526
    • Tanner, J.E.1
  • 3
    • 34047191652 scopus 로고
    • Fourier transform pulsed-gradient spin-echo studies of molecular diffusion
    • P. Stilbs Fourier transform pulsed-gradient spin-echo studies of molecular diffusion Prog. Nucl. Magn. Reson. Spectrosc. 19 1987 1 45
    • (1987) Prog. Nucl. Magn. Reson. Spectrosc. , vol.19 , pp. 1-45
    • Stilbs, P.1
  • 4
    • 85120223715 scopus 로고
    • P.T. Callaghan Principles of Nuclear Magnetic Resonance Microscopy 1991 Clarendon Press Oxford
    • (1991)
    • Callaghan, P.T.1
  • 5
    • 0031498272 scopus 로고    scopus 로고
    • Pulsed-field gradient nuclear magnetic resonance as a tool for studying translational diffusion: Part I. Basic theory
    • W.S. Price Pulsed-field gradient nuclear magnetic resonance as a tool for studying translational diffusion: Part I. Basic theory Concepts Magn. Reson. 9 1997 299 336
    • (1997) Concepts Magn. Reson. , vol.9 , pp. 299-336
    • Price, W.S.1
  • 6
    • 0032352438 scopus 로고    scopus 로고
    • Pulsed-field gradient nuclear magnetic resonance as a tool for studying translational diffusion: Part II. Experimental aspects
    • W.S. Price Pulsed-field gradient nuclear magnetic resonance as a tool for studying translational diffusion: Part II. Experimental aspects Concepts Magn. Reson. 10 1998 197 237
    • (1998) Concepts Magn. Reson. , vol.10 , pp. 197-237
    • Price, W.S.1
  • 7
    • 0001376261 scopus 로고
    • One- and two-dimensional pulse sequences for diffusion experiments in the fringe field of superconducting magnets
    • R. Kimmich E. Fischer One- and two-dimensional pulse sequences for diffusion experiments in the fringe field of superconducting magnets J. Magn. Reson. A 106 1994 229 235
    • (1994) J. Magn. Reson. A , vol.106 , pp. 229-235
    • Kimmich, R.1    Fischer, E.2
  • 8
    • 44949277365 scopus 로고
    • NMR measurement of small self-diffusion coefficients in the fringe field of superconducting magnets
    • R. Kimmich W. Unrath G. Schnur E. Rommel NMR measurement of small self-diffusion coefficients in the fringe field of superconducting magnets J. Magn. Reson. 91 1991 136 140
    • (1991) J. Magn. Reson. , vol.91 , pp. 136-140
    • Kimmich, R.1    Unrath, W.2    Schnur, G.3    Rommel, E.4
  • 10
    • 0032385498 scopus 로고    scopus 로고
    • Measurement of translational molecular diffusion using ultrahigh magnetic field gradient NMR
    • B. Geil Measurement of translational molecular diffusion using ultrahigh magnetic field gradient NMR Concepts Magn. Reson. 10 1998 299 321
    • (1998) Concepts Magn. Reson. , vol.10 , pp. 299-321
    • Geil, B.1
  • 11
    • 0000496869 scopus 로고    scopus 로고
    • Self-diffusion coefficient in plastic crystals by multiple-pulse NMR in large static field gradients
    • I. Chang G. Hinze G. Diezemann F. Fujara H. Sillescu Self-diffusion coefficient in plastic crystals by multiple-pulse NMR in large static field gradients Phys. Rev. Lett. 76 1996 2523 2526
    • (1996) Phys. Rev. Lett. , vol.76 , pp. 2523-2526
    • Chang, I.1    Hinze, G.2    Diezemann, G.3    Fujara, F.4    Sillescu, H.5
  • 13
    • 0000883351 scopus 로고    scopus 로고
    • First direct measurement of the spin diffusion rate in a homogeneous solid
    • W. Zhang D.G. Cory First direct measurement of the spin diffusion rate in a homogeneous solid Phys. Rev. Lett. 80 1998 1324 1327
    • (1998) Phys. Rev. Lett. , vol.80 , pp. 1324-1327
    • Zhang, W.1    Cory, D.G.2
  • 14
    • 0032060855 scopus 로고    scopus 로고
    • Pulsed gradient NMR probes for solid state studies
    • W. Zhang D.G. Cory Pulsed gradient NMR probes for solid state studies J. Magn. Reson. 132 1998 144 149
    • (1998) J. Magn. Reson. , vol.132 , pp. 144-149
    • Zhang, W.1    Cory, D.G.2
  • 15
    • 0033641015 scopus 로고    scopus 로고
    • 13C PGSE NMR experiment with heteronuclear dipolar decoupling to measure diffusion in liquid crystals and solids
    • 13C PGSE NMR experiment with heteronuclear dipolar decoupling to measure diffusion in liquid crystals and solids J. Magn. Reson. 142 2000 102 110
    • (2000) J. Magn. Reson. , vol.142 , pp. 102-110
    • Dvinskikh, S.V.1    Sitnikov, R.2    Furó, I.3
  • 16
    • 0034184469 scopus 로고    scopus 로고
    • Combining PGSE NMR with homonuclear dipolar decoupling
    • S.V. Dvinskikh I. Furó Combining PGSE NMR with homonuclear dipolar decoupling J. Magn. Reson. 144 2000 142 149
    • (2000) J. Magn. Reson. , vol.144 , pp. 142-149
    • Dvinskikh, S.V.1    Furó, I.2
  • 17
    • 0000657454 scopus 로고    scopus 로고
    • Cross-relaxation effects in stimulated-echo-type PGSE NMR experiments by bipolar and monopolar gradient pulses
    • S.V. Dvinskikh I. Furó Cross-relaxation effects in stimulated-echo-type PGSE NMR experiments by bipolar and monopolar gradient pulses J. Magn. Reson. 146 2000 283 289
    • (2000) J. Magn. Reson. , vol.146 , pp. 283-289
    • Dvinskikh, S.V.1    Furó, I.2
  • 18
    • 0035744261 scopus 로고    scopus 로고
    • Measurement of the principal values of the anisotropic diffusion tensor in an unoriented sample by exploiting the chemical shift anisotropy: 19F PGSE NMR with homonuclear decoupling
    • 19F PGSE NMR with homonuclear decoupling J. Magn. Reson. 148 2001 73 77
    • (2001) J. Magn. Reson. , vol.148 , pp. 73-77
    • Dvinskikh, S.V.1    Furó, I.2
  • 19
    • 0001107146 scopus 로고
    • The determination of translational diffusion constants in liquid crystals from pulsed field gradient double quantum spin echo decays
    • J.F. Martin L.S. Selwyn R.R. Vold R.L. Vold The determination of translational diffusion constants in liquid crystals from pulsed field gradient double quantum spin echo decays J. Chem. Phys. 76 1982 2632 2634
    • (1982) J. Chem. Phys. , vol.76 , pp. 2632-2634
    • Martin, J.F.1    Selwyn, L.S.2    Vold, R.R.3    Vold, R.L.4
  • 20
    • 36749105484 scopus 로고
    • Study of anisotropic diffusion of oriented molecules by multiple quantum spin echoes
    • D. Zax A. Pines Study of anisotropic diffusion of oriented molecules by multiple quantum spin echoes J. Chem. Phys. 78 1983 6333 6334
    • (1983) J. Chem. Phys. , vol.78 , pp. 6333-6334
    • Zax, D.1    Pines, A.2
  • 21
    • 0000592856 scopus 로고
    • An application of pulse-gradient double-quantum spin echoes to diffusion measurements on molecules with scalar-coupled spins
    • L.E. Kay J.H. Prestegard An application of pulse-gradient double-quantum spin echoes to diffusion measurements on molecules with scalar-coupled spins J. Magn. Reson. 67 1986 103 113
    • (1986) J. Magn. Reson. , vol.67 , pp. 103-113
    • Kay, L.E.1    Prestegard, J.H.2
  • 22
    • 0030606182 scopus 로고    scopus 로고
    • Multiple-quantum pulsed gradient NMR diffusion experiments on quadrupolar (I>1/2) spins
    • L. v. Dam B. Andreasson L. Nordenskiöld Multiple-quantum pulsed gradient NMR diffusion experiments on quadrupolar (I>1/2) spins Chem. Phys. Lett. 262 1996 737 743
    • (1996) Chem. Phys. Lett. , vol.262 , pp. 737-743
    • v. Dam, L.1    Andreasson, B.2    Nordenskiöld, L.3
  • 23
    • 0000449031 scopus 로고
    • The measurement of diffusion using deuterium pulsed field gradient nuclear magnetic resonance
    • P.T. Callaghan M.A. Le Gros D.N. Pinder The measurement of diffusion using deuterium pulsed field gradient nuclear magnetic resonance J. Chem. Phys. 79 1983 6372 6381
    • (1983) J. Chem. Phys. , vol.79 , pp. 6372-6381
    • Callaghan, P.T.1    Le Gros, M.A.2    Pinder, D.N.3
  • 24
    • 0000419932 scopus 로고    scopus 로고
    • Orientational order and micelle size in the nematic phase of the cesium pentadecafluorooctanoate-water system from the anisotropic self-diffusion of water
    • H. Jóhannesson I. Furó B. Halle Orientational order and micelle size in the nematic phase of the cesium pentadecafluorooctanoate-water system from the anisotropic self-diffusion of water Phys. Rev. E 53 1996 4904 4917
    • (1996) Phys. Rev. E , vol.53 , pp. 4904-4917
    • Jóhannesson, H.1    Furó, I.2    Halle, B.3
  • 25
    • 33744456822 scopus 로고    scopus 로고
    • Accurate anisotropic water-diffusion measurements in liquid crystals
    • I. Furó H. Jóhannesson Accurate anisotropic water-diffusion measurements in liquid crystals J. Magn. Reson. A 119 1996 15 21
    • (1996) J. Magn. Reson. A , vol.119 , pp. 15-21
    • Furó, I.1    Jóhannesson, H.2
  • 26
    • 45449122556 scopus 로고
    • Deuteron two-dimensional exchange NMR in solids
    • C. Schmidt B. Blümich H.W. Spiess Deuteron two-dimensional exchange NMR in solids J. Magn. Reson. 79 1988 269 290
    • (1988) J. Magn. Reson. , vol.79 , pp. 269-290
    • Schmidt, C.1    Blümich, B.2    Spiess, H.W.3
  • 27
    • 85120196458 scopus 로고    scopus 로고
    • K. Schmidt-Rohr, and, H. W. Spiess, Multidimensional Solid-State NMR and Polymers, Academic Press, London, 1994.
  • 28
    • 33646620078 scopus 로고
    • Time-reversal experiments in dipolar-coupled spin systems
    • W.-K. Rhim A. Pines J.S. Waugh Time-reversal experiments in dipolar-coupled spin systems Phys. Rev. B 3 1971 684 696
    • (1971) Phys. Rev. B , vol.3 , pp. 684-696
    • Rhim, W.-K.1    Pines, A.2    Waugh, J.S.3
  • 30
    • 33947577104 scopus 로고
    • Solid-state NMR imaging by magic sandwich echoes
    • S. Matsui Solid-state NMR imaging by magic sandwich echoes Chem. Phys. Lett. 179 1991 187 190
    • (1991) Chem. Phys. Lett. , vol.179 , pp. 187-190
    • Matsui, S.1
  • 31
    • 0000869328 scopus 로고
    • Spatially resolved homonuclear solid-state NMR. III. Magic-echo and rotary-echo phase-encoding imaging
    • D.E. Demco S. Hafner R. Kimmich Spatially resolved homonuclear solid-state NMR. III. Magic-echo and rotary-echo phase-encoding imaging J. Magn. Reson. 96 1992 307 322
    • (1992) J. Magn. Reson. , vol.96 , pp. 307-322
    • Demco, D.E.1    Hafner, S.2    Kimmich, R.3
  • 32
    • 0003015252 scopus 로고
    • Mapping molecular orientation by solid-state NMR imaging
    • M.A. Hepp J.B. Miller Mapping molecular orientation by solid-state NMR imaging J. Magn. Reson. A 111 1994 62 69
    • (1994) J. Magn. Reson. A , vol.111 , pp. 62-69
    • Hepp, M.A.1    Miller, J.B.2
  • 34
    • 85120230585 scopus 로고    scopus 로고
    • R. Kimmich NMR Tomography, Diffusometry, Relaxometry 1997 Springer-Verlag Berlin
    • (1997)
    • Kimmich, R.1
  • 35
    • 0034367786 scopus 로고    scopus 로고
    • Solid-state NMR imaging methods. Part II: Line narrowing
    • D.E. Demco B. Blümich Solid-state NMR imaging methods. Part II: Line narrowing Concepts Magn. Reson. 12 2000 269 288
    • (2000) Concepts Magn. Reson. , vol.12 , pp. 269-288
    • Demco, D.E.1    Blümich, B.2
  • 36
    • 0001538267 scopus 로고
    • A deuterium NMR study of chain ordering in the liquid crystals 4,4′-di-n-heptyloxyazoxybenzene and 4-n-octyl-4′-cyanobiphenyl
    • N. Boden L.D. Clark R.J. Bushby J.W. Emsley G.R. Luckhurst C.P. Stockley A deuterium NMR study of chain ordering in the liquid crystals 4,4′-di-n-heptyloxyazoxybenzene and 4-n-octyl-4′-cyanobiphenyl Mol. Phys. 42 1981 565 594
    • (1981) Mol. Phys. , vol.42 , pp. 565-594
    • Boden, N.1    Clark, L.D.2    Bushby, R.J.3    Emsley, J.W.4    Luckhurst, G.R.5    Stockley, C.P.6
  • 37
    • 0000351734 scopus 로고    scopus 로고
    • Correlation of deuterium quadrupolar couplings and carbon-13 chemical shifts in ordered media by multiple-quantum NMR
    • D. Sandström H. Zimmermann Correlation of deuterium quadrupolar couplings and carbon-13 chemical shifts in ordered media by multiple-quantum NMR J. Phys. Chem. B 104 2000 1490 1493
    • (2000) J. Phys. Chem. B , vol.104 , pp. 1490-1493
    • Sandström, D.1    Zimmermann, H.2
  • 38
    • 0000745176 scopus 로고
    • Quadrupolar echo deuteron magnetic resonance spectroscopy in ordered hydrocarbon chains
    • J.H. Davis K.R. Jeffrey M. Bloom M.I. Valic T.P. Higgs Quadrupolar echo deuteron magnetic resonance spectroscopy in ordered hydrocarbon chains Chem. Phys. Lett. 42 1976 390 394
    • (1976) Chem. Phys. Lett. , vol.42 , pp. 390-394
    • Davis, J.H.1    Jeffrey, K.R.2    Bloom, M.3    Valic, M.I.4    Higgs, T.P.5
  • 42
    • 0000492115 scopus 로고
    • Multiple quantum NMR spectroscopy on I>1 nuclei in anisotropic systems
    • I. Furó B. Halle Multiple quantum NMR spectroscopy on I>1 nuclei in anisotropic systems Molec. Phys. 76 1992 1169 1197
    • (1992) Molec. Phys. , vol.76 , pp. 1169-1197
    • Furó, I.1    Halle, B.2
  • 43
    • 0002546377 scopus 로고
    • Nuclear spin relaxation
    • R.R. Vold Nuclear spin relaxation J.W. Emsley Nuclear Magnetic Resonance of Liquid Crystals 1985 Reidel Dordrecht 253 288
    • (1985) , pp. 253-288
    • Vold, R.R.1
  • 44
    • 0002360668 scopus 로고
    • Density matrix calculations of the relaxation of two deuterons in an ordered medium
    • R. Poupko R.L. Vold R.R. Vold Density matrix calculations of the relaxation of two deuterons in an ordered medium J. Magn. Reson. 34 1979 67 81
    • (1979) J. Magn. Reson. , vol.34 , pp. 67-81
    • Poupko, R.1    Vold, R.L.2    Vold, R.R.3
  • 45
    • 0000335246 scopus 로고
    • Deuterium relaxation of a partially oriented methyl group. II. Density matrix calculations of multiple quantum spin-echo linewidths
    • D. Jaffe R.L. Vold R.R. Vold Deuterium relaxation of a partially oriented methyl group. II. Density matrix calculations of multiple quantum spin-echo linewidths J. Magn. Reson. 46 1982 496 502
    • (1982) J. Magn. Reson. , vol.46 , pp. 496-502
    • Jaffe, D.1    Vold, R.L.2    Vold, R.R.3
  • 47
    • 0346678929 scopus 로고    scopus 로고
    • Multiple-time correlation functions in spin-3/2 solid-state NMR spectroscopy
    • R. Böhmer Multiple-time correlation functions in spin-3/2 solid-state NMR spectroscopy J. Magn. Reson. 147 2000 78 88
    • (2000) J. Magn. Reson. , vol.147 , pp. 78-88
    • Böhmer, R.1
  • 48
    • 0035933964 scopus 로고    scopus 로고
    • Anisotropic self-diffusion in the nematic phase of a thermotropic liquid crystal by 1H spin-echo nuclear magnetic resonance
    • 1H spin-echo nuclear magnetic resonance J. Chem. Phys. 115 2001 1946 1950
    • (2001) J. Chem. Phys. , vol.115 , pp. 1946-1950
    • Dvinskikh, S.V.1    Furó, I.2
  • 49
    • 0001422799 scopus 로고
    • Diffusion in thermotropic liquid crystals
    • G.J. Krüger Diffusion in thermotropic liquid crystals Phys. Rep. 82 1982 229 269
    • (1982) Phys. Rep. , vol.82 , pp. 229-269
    • Krüger, G.J.1
  • 50
    • 0022929540 scopus 로고
    • Forced Rayleigh scattering in nCB's (n=5–9) with methyl red and binary mass diffusion constants
    • M. Hara H. Takezoe A. Fukuda Forced Rayleigh scattering in nCB's ( n =5–9) with methyl red and binary mass diffusion constants Jpn. J. Appl. Phys. 25 1986 1756 1761
    • (1986) Jpn. J. Appl. Phys. , vol.25 , pp. 1756-1761
    • Hara, M.1    Takezoe, H.2    Fukuda, A.3
  • 51
    • 36449004203 scopus 로고
    • Translational diffusion in a smectic-A phase by electron spin resonance imaging: the free-volume model
    • J.K. Moscicki Y.-K. Shin J.H. Freed Translational diffusion in a smectic-A phase by electron spin resonance imaging: the free-volume model J. Chem. Phys. 99 1993 634 649
    • (1993) J. Chem. Phys. , vol.99 , pp. 634-649
    • Moscicki, J.K.1    Shin, Y.-K.2    Freed, J.H.3
  • 52
    • 0001253832 scopus 로고
    • Specifically deuterated intermediates for the synthesis of liquid crystals and liquid-crystalline polymers
    • H. Zimmermann Specifically deuterated intermediates for the synthesis of liquid crystals and liquid-crystalline polymers Liq. Cryst. 4 1989 591 618
    • (1989) Liq. Cryst. , vol.4 , pp. 591-618
    • Zimmermann, H.1
  • 53
    • 0009636902 scopus 로고    scopus 로고
    • Magnetic field induced alignment of the director in a smectic A phase: Surface effects
    • J.W. Emsley G.R. Luckhurst P. Pedrielli Magnetic field induced alignment of the director in a smectic A phase: Surface effects Chem. Phys. Lett. 320 2000 255 261
    • (2000) Chem. Phys. Lett. , vol.320 , pp. 255-261
    • Emsley, J.W.1    Luckhurst, G.R.2    Pedrielli, P.3
  • 54
    • 0042936805 scopus 로고
    • Self-diffusion in normal and heavy water in the range 1–45°
    • R. Mills Self-diffusion in normal and heavy water in the range 1–45° J. Phys. Chem. 77 1973 685 688
    • (1973) J. Phys. Chem. , vol.77 , pp. 685-688
    • Mills, R.1
  • 55
    • 84946364724 scopus 로고
    • Nuclear magnetic relaxation in spin-1 systems: The response to three-pulse sequence II. Inhomogeneous B0 field
    • 0 field Mol. Phys. 37 1979 59 71
    • (1979) Mol. Phys. , vol.37 , pp. 59-71
    • Ahmad, S.B.1    Packer, K.J.2


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