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13
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85037272295
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note
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F = + 0.42 and Δδ = + 0.14, respectively.
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14
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85037261480
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note
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1a and 2a-c melt at 173-175°C, 108-110°C, 78-80°C, and 113-115°C, respectively, and halogen bonded co-crystals 3a-c melt at 210°C, 160°C, and 105°C, respectively.
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15
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85037285430
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note
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-1) 3049, 3015; 2a: 1468, 944, 761; 2b: 1497, 956, 789; 2c 1492, 995, 721; 3a: 3053, 3015, 1464, 943, 760; 3b: 3052, 3017, 1481, 955, 788; 3c: 3050, 3015, 994, 721;.
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Amico, V.; Meille, S.V.; Corradi, E.; Messina, M.T.; Resnati, G.; J. Am. Chem. Soc. 1998, 120, 8261. Messina, M.T.; Metrangolo, P.; Resnati, G.; in Asymmetric Fluoroorganic Chemistry: Synthesis, Applications and Future Directions, ACS Symposium Series No 746, chapter 17, Ramachandran, P. V. (Ed.), American Chemical Society, Washington DC, 1999. Lunghi, A.; Cardillo, P.; Messina, M.T.; Metrangolo, P.; Panzeri, W.; Resnati, G.; J. Fluorine Chem. 1998, 91, 191.
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0032547250
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ACS Symposium Series No 746, chapter 17, Ramachandran, P. V. (Ed.), American Chemical Society, Washington DC
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Messina, M.T.1
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0032493941
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85037260978
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note
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13.
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0030567353
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Lommerse, J.P.M.; Stone, A.J.; Taylor, R.; Allen, F.H.; J. Am. Chem. Soc. 1996, 118, 3108.
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85037260630
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note
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2) were 0.043 and 0.069, respectively. 1 lies on a C2 crystallographic axis, so the methyl group C9 is disordered, 2a lies on a centre of symmetry.
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24
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0033555633
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Grebe, J.; Geiseler, G.; Harms, K.; Neumüller, B.; Dehnicke, K.; Angew. Chem. Int. Ed. 1999, 38, 222.
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0345879116
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33746508285
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Bailey, R.D.; Drake, G.W.; Grabarczyk, M.; Hanks, T.W.; Hook, L.L.; Pennington, W.T.; J. Chem. Soc., Perkin Trans. 2 1997, 2773. Bailey, R.D.; Buchanan, M.L.; Pennington, W. D.; Acta Cryst. 1992, C48, 2259. Uchida T.; Kimura, K.; Acta Cryst. 1984, C40, 139.
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0345879116
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Bailey, R.D.; Drake, G.W.; Grabarczyk, M.; Hanks, T.W.; Hook, L.L.; Pennington, W.T.; J. Chem. Soc., Perkin Trans. 2 1997, 2773. Bailey, R.D.; Buchanan, M.L.; Pennington, W. D.; Acta Cryst. 1992, C48, 2259. Uchida T.; Kimura, K.; Acta Cryst. 1984, C40, 139.
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Uchida, T.1
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85037262373
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note
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(1-x,1-y,1-z) and F2···H7, 2.51(3) and 2.64(4) Å, respectively). These contacts are more responsible for keeping the tolyl, pyridyl, and tetrafluorobenzene rings in a nearly coplanar arrangement rather than for driving the self-assembly of the HC and PFC modules into 3a.
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37049090121
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Bessel, C.A.; See, R.F.; Jameson, D.L.; Churchill, M.R.; Takeuchi, K.J.; J. Chem. Soc., Dalton Trans. 1992, 3223.
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Takeuchi, K.J.5
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0000033652
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0000033652
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Armspach, D.; Constble, E.C.; Housecraft, C.E.; Neuburger, M.; Zehnder, M.; New J. Chem. 1996, 20, 331. Constable, E.C.; Thompson, A.M.W.C.; Tocher, D.A.; Daniels, M.A.M.; New J. Chem. 1992, 16, 855.
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84889530612
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Constable, E.C.; Khan, F.K.; Marquez, V.E.; Raithby, P.R.; Acta Crystallogr. 1992, C48, 932. Storrier, G.D.; Colbran, S.B.; Craig, D.C.; J. Chem. Soc., Dalton Trans. 1997, 3011.
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Constable, E.C.1
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Constable, E.C.; Khan, F.K.; Marquez, V.E.; Raithby, P.R.; Acta Crystallogr. 1992, C48, 932. Storrier, G.D.; Colbran, S.B.; Craig, D.C.; J. Chem. Soc., Dalton Trans. 1997, 3011.
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Storrier, G.D.1
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manuscript in preparation
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Corradi, E.; Meille, S.V.; Messina, M.T.; Metrangolo, P.; Resnati, G.; manuscript in preparation.
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Corradi, E.1
Meille, S.V.2
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0001858387
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Allen, F.H.; Biradha, K.; Desiraju, G.R.; Hoy, V.J.; Howard, J.A.K.; Sarma, J.A.R.P.; Thaimattam, R.; J. Chem. Soc., Chem. Commun. 1997, 101. Pedireddi, V.R.; Ranganathan, A.; Tetrahedron Lett., 1998, 39, 1803.
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