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27844582885
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note
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11B NMR, mass spectrum] consistent with the assigned structure. Selected spectroscopic and spectrometric data are presented in the experimental section.
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14
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27844524447
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note
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w = 0.065. Data were measured on an Enraf-Nonius CAD4 diffractometer, graphite monochromator. The structure was solved by direct methods using SIR92 (C. Giacovazzo, University of Bari, 1992) and refined using CRYSTALS (CRYSTALS, Issue 9, Watkin, D.; Chemical Crystallography Laboratory, Oxford 1990). Atomic coordinates, bond lengths and angles, and thermal parameters have been deposited at the Cambridge Crystallographic Data Centre.
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