Characterization of microporous copper(II) dicarboxylates (fumarate, terephthalate, and trans-1,4-cyclohexanedicarboxylate) by gas adsorption

Chemistry Letters

Volumn , Issue 2, 2001, Pages 122-123

  Seki, Kenji ^a   Takamizawa, Satoshi ^b   Mori, Wasuke ^b  

^a OSAKA GAS CO LTD   (Japan)

^b KANAGAWA UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0035531821     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.2001.122     Document Type: Article

References (18)

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18. The apparatus was equipped with the Cahn-2000 microbalance contained within a SUS steel pressure chamber which was connected with two separate lines for evacuation and adsorbate gas pressurization. After the each sample was set in the apparatus, the adsorbed molecules in the pore and on the surface were removed heating under reduced pressure. After becoming the constant weight, methane was dosed into the adsorption chamber. After each increment for the temperature and sample weight, sufficient time was allowed to stabilize, then the change of the weight of sample was measured. After the buoyancy had been corrected to the obtained amount of the weight change, the absorbed amount was calculated.