Improving batch cooling seeded crystallization of an organic weed-killer using on-line ATR FTIR measurement of supersaturation

Journal of Crystal Growth

Volumn 226, Issue 2-3, 2001, Pages 348-362

  Lewiner, F ^a   Fevotte G ^a   Klein, J P ^a   Puel, F ^b  

^a UNIVERSITÉ LYON 1   (France)

^b CRIT   (France)

Author keywords

A1. Crystal morphology; A2. Growth from solution; A2. Seed crystals; B1. Organic compounds

Indexed keywords

ATOMIC FORCE MICROSCOPY; COOLING; CRYSTAL STRUCTURE; FOURIER TRANSFORM INFRARED SPECTROSCOPY; ORGANIC COMPOUNDS; SOLUBILITY; SUPERSATURATION;

CRYSTAL SIZE DISTRIBUTION; SEED CRYSTALS;

CRYSTALLIZATION;

EID: 0035365990     PISSN: 00220248     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-0248(01)01395-1     Document Type: Article

References (22)

1. Application of ATR FTIR spectroscopy for on-line determination of solute concentration and solution supersaturation
2. A robust chemometrics approach to inferential estimation of supersaturation
3. Particle size and shape control in crystallization process
4. Application of in situ ATR FTIR to the on line monitoring of batch crystallisation with agglomeration
5. On line ATR FTIR measurement of supersaturation during solution crystallization processes, Calibration and applications on three solute/solvant systems
6. Why is seeding of organic substances in the batch crystallization still treated as an art?