A New Policy for the Estimation of the Course of Supersaturation in Batch Crystallization

Canadian Journal of Chemical Engineering

Volumn 74, Issue 3, 1996, Pages 372-384

  Fevotte, G ^a   Klein, J P ^a  

^a UNIVERSITÉ LYON 1   (France)

Author keywords

Batch cooling crystallization; Nucleation; On line calorimetry; Process identification; Seeding

Indexed keywords

CALORIMETRY; CRYSTAL GROWTH; ESTIMATION; MONITORING; NUCLEATION; SUPERSATURATION;

BATCH COOLING CRYSTALLIZATION; CRYSTALLIZATION CONTROL; ON-LINE CALORIMETRY;

CRYSTALLIZATION;

EID: 0030173183     PISSN: 00084034     EISSN: None     Source Type: Journal    
DOI: 10.1002/cjce.5450740308     Document Type: Article

References (35)

1. M. Agarwal and D. Bonvin, "Limitations of the Extended Kalman Filter for Batch Reactors", in "Preprints IFAC Int. Symp. Dycord + '89", Maastricht, The Netherlands, August 21-23 (1988), pp. 287-294.
2. Bourne, J. R., M. Buerli and W. Regenass, "Heat Transfer and Power Measurements in Stirred Tanks Using Heat Flow Calorimetry", Chem. Eng. Sci. 36, 347-354 (1981).
3. Canegallo, S., G. Storti, M. Mobidelli and S. Carra, "Densimetry for On-line Conversion Monitoring in Emulsion Homo- and Copolymerization", J. Appl. Polymer Sci. 47, 961-979 (1993).
4. Chien, D. C. H. and A. Penlidis, "On-line Sensors for Polymerization Reactors", J. M. S.- Rev. Macromol. Chem. Phys. C30, 1-42 (1990).
5. Févotte, G. and J. P. Klein, "Application of On-line Calorimetry to the Advanced Control of Batch Crystallizers", Chem. Eng. Sci. 49, 1323-1336 (1994a).
6. Févotte, G. and J. P. Klein, "A Bench Scale Evaporative Calorimeter for Diagnostic and Control Possibilities in Vacuum Processes", Thermochim. Acta 236, 81-91 (1994b).
7. Févotte, G. and J. P. Klein, "Crystallization Calorimetry for the Assessment of Batch Seeding and Cooling Policies", Chem. Eng. J. 59, 143-152 (1995).
8. Grob, B., R. Riesen and K. Vogel, "Reaction Calorimetry for the Development of Chemical Reactors", Thermochim. Acta 114, 83-93 (1987).
9. Gutwald, T. and A. Meersman, "Batch Cooling Crystallization at Constant Supersaturation: Technique and Experimental Results", Chem. Eng. Technol. 13, 229-237 (1990).
10. Helt, J. E. and M. A. Larson, "Effect of Temperature on the Crystallization of Potassium Nitrate by Direct Measurement of Supersaturation", AIChE J. 23, 822-830 (1977).
11. Hlozny, L., A. Sato and N. Kubota, "On-line Measurement of Supersaturation During Batch Cooling Crystallization of Ammonium Alum", J. Chem. Eng. Japan 25, 5, 604-606 (1992).
12. Hub, L., "Universal System for Investigation of Thermic Hazards", Thermochim. Acta 85, 361-364 (1985).
13. Karlsen, L. G., H. Søøberg and J. Villadsen, "Optimal Data Acquisition for Heat Flow Calorimeter", Thermochim. Acta 72, 83-94 (1984).
14. Karlsen, L. G. and J. Villadsen, "Isothermal Reaction Calorimeters-I.A Literature Review", Chem. Eng. Sci. 42, 1165-1173 (1987a).
15. Karlsen, L. G. and J. Villadsen, "Isothermal Reaction Calorimeters-II. Data Treatment", Chem. Eng. Sci. 42, 1153-1164 (1987b).
16. König, A., H. H. Emons and V. L. Rylov, "Calorimetric Determination of the Kinetic Parameters of Crystallization", Translated from Zhurnal Prikladnoi Khimii 63, 10, 2231-2236 (1990).
17. Landau, I. D., in "Adaptive Control - The Model Reference Approach", J. M. Mendel, Ed., Marcel Dekker, New York (1979), Chpt. 7.
18. Ljung, L. L. and T. Söderstrom, "Theory and Practice of Recursive Identification", MIT Press, Cambridge, MA (1983).
19. MacGregor, J. F., "On-line Reactor Energy Balances via Kalman Filtering", Proc. IFAC-PRP 6 Automation, Akron, OH, U.S.A., Oct. Pergamon Press, Oxford (1986).
20. Marison, I. W. and U. von Stockar, "A Novel Bench-scale Calorimeter for Biological Process Development Work", Thermochim. Acta 85, 493-496 (1985).
21. Marison, I. W., B. Birou and U. von Stockar, "Use of a Novel Heat-flux Calorimeter for the Measurement of Heat Generated During Growth of K. fraglis on Lactose", Thermochim. Acta 85, 497-500 (1985).
22. Miller, S. M. and J. B. Rawlings, "Model Identification and Control Strategies for Batch Cooling Crystallizers", AIChE J. 40, 1312-1327 (1994).
23. Moritz, H. U., "Polymerization Calorimetry - a Powerful Tool for Reactor Control", in "Polymer Reaction Engineering", K. H. Reichert and U. Geiseler, Eds. VCH Verlag, Berlin (1989), pp. 248-266.
24. Nyvlt, J., "Effect of the Kinetics Parameters on the Behaviour and Product CSD of Batch Crystallizers", AIChE Symp. Series 153 (72), 61-63 (1976).
25. Qiu, Y. and A. C. Rasmuson, "Nucleation and Growth of Succinic Acid in a Batch Cooling Crystallizer", AIChE J. 37, 1293-1304 (1991).
26. Qiu, Y. and A. C. Rasmuson, "Estimation of Crystallization Kinetics from Batch Cooling Experiments", AIChE J. 40, 799-812 (1994).
27. Rawlings, J. B., S. M. Miller and W. R. Witkowski, "Model Identification and Control of Solution Crystallization Processes: A Review", Ind. Eng. Chem. Res. 32, 1275-1296 (1993).
28. Regenass, W. "Calorimetric Monitoring of Industrial Chemical Processes", Thermochim. Acta 95, 351-368 (1985).
29. Riebel, U., V. Kofler and F. Löffler, "Control of Supersaturation in Instationary Suspension Crystallization", in "Proc. 11th Int. Symp. on Industrial Crystallization", A. Mersmann, Ed., Garmisch Partenkirchen, Germany (1990), pp. 595-599.
30. Riesen, R., "Optimization of Industrial Crystallization Processes", Chem. Plants Processing, July, 26-29 (1992).
31. Rohani, S. and K. Paine, "Measurement of Solid Concentration of a Soluble Compound in a Saturated Slurry", Can. J. Chem. Eng. 65, 163-165 (1987).
32. Schmidt, C. U. and K. H. Reichert, "Reaction Calorimeter. A Contribution to Safe Operation of Exothermic Polymerization", 10th ISCRE, Chem. Eng. Sci. 43, 2133-2137 (1987).
33. Schuler, H. and C. U. Schmidt, "Calorimetric State Estimators for Chemical Reactor Diagnosis and Control: Review of Methods and Applications", Chem. Eng. Sci. 47, 899-915 (1992).
34. Shah, S. L. and W. R. Cluett, "Recursive Least Squares Based Estimation Schemes for Self Tuning Control", Can. J. Chem. Eng. 69, 89-96 (1991).
35. Sikdar, S. K. and A. D. Randolph, "Secondary Nucleation of Two Fast Growth Systems in a Mixed Suspension Crystallizer: Magnesium Sulfate and Citric Acid Water Systems", AIChE J. 22, 110-117 (1976).