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85088333698
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note
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1H NMR characterisation of both the free-base and the diamagnetic zinc complex.
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31
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20644467652
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note
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In most of these compounds, a gaussian transformation has to be performed to observe the meta coupling constant for this proton which otherwise appears as a large singlet.
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32
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2142836369
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0000519324
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35
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20644441436
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note
-
The same reaction has been tested with 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) as a nonnucleophilic base but, in our hands, this procedure was not reproducible.
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-
-
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36
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20644448109
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note
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In the case of TAPP, the four aniline aromatic rings are connected to the carbon atoms in the meso positions numbered 5, 10, 15, 20.
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-
-
-
37
-
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85088332227
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note
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2 are: δ = 1.23 (t, 6 H), 3.51 (q, 4 H), 2.18 (s, 2 H).
-
-
-
-
38
-
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20644468911
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-
note
-
The same difference is found between benzyl chloride (δ = 4.5) and diethylbenzyl malonate (δ = 3.6).
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-
-
-
39
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20644461807
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To be published: the coordination of the zinc atom in a chiral bis-strapped porphyrin by the oxygen atom of an amide bond has been observed both in the solid state and in solution
-
To be published: the coordination of the zinc atom in a chiral bis-strapped porphyrin by the oxygen atom of an amide bond has been observed both in the solid state and in solution.
-
-
-
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41
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20644449356
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note
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Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-154271 Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK [Fax: (internat.) + 44-1223/336-033; E-mail: deposit@ccdc.cam.ac.uk].
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