Rational design of open-framework coordination solids - Synthesis and structure of [Co5(OH)2{1,2,4,5-(O2C)4C 6H2}2(H2O) 4]·xH2O

European Journal of Inorganic Chemistry

Volumn , Issue 11, 2001, Pages 2739-2741

  Gutschke, Siegfried O H ^a   Price, Daniel J ^b   Powell, Annie K ^a   Wood, Paul T ^c  

^a UNIVERSITY OF KARLSRUHE   (Germany)

^b UNIVERSITY OF SOUTHAMPTON   (United Kingdom)

^c UNIVERSITY OF CAMBRIDGE   (United Kingdom)

Author keywords

Carboxylate ligands; Cobalt; Mesoporous materials; Synthesis design

Indexed keywords

CARBOXYLATION; CHELATION; COBALT; COORDINATION REACTIONS; MESOPOROUS MATERIALS; METAL IONS;

CARBOXYLATE LIGANDS; CO-ORDINATIVELY UNSATURATED; METALS IONS; OPEN FRAMEWORKS; RATIONAL DESIGN; SYNTHESIS DESIGN; UNSATURATED METALS;

HYDROTHERMAL SYNTHESIS;

CARBOXYLIC ACID; COBALT COMPLEX; LIGAND; METAL ION;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; DEHYDRATION; HEATING; REACTION ANALYSIS; SOLID; SYNTHESIS;

EID: 0034748547     PISSN: 14341948     EISSN: None     Source Type: Journal    
DOI: 10.1002/1099-0682(200111)2001:11<2739::AID-EJIC2739>3.0.CO;2-1     Document Type: Article

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22. 2 to give R1 = 0.0572 for F > 4σ(F) and wR2 = 0.1582, S = 0.926 for all data. Crystallographic data (excluding structure factors) for the structure(s) reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-157236. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK [Fax: (internat.) +44-1223/336-033; E-mail: deposit@ccdc.cam.ac.uk].
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