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Volumn 65, Issue 2, 2000, Pages 432-437

Practical asymmetric synthesis of (S)-MA20565, a wide-spectrum agricultural fungicide

Author keywords

[No Author keywords available]

Indexed keywords

FUNGICIDE; MA 20565; UNCLASSIFIED DRUG;

EID: 0034723238     PISSN: 00223263     EISSN: None     Source Type: Journal    
DOI: 10.1021/jo991271z     Document Type: Article
Times cited : (76)

References (37)
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    • Hutson, D. H.; Miyamoto, J., Ed.; Wiley: Chichester
    • Reviews: (a) Clough, J. M.; Godfrey. C. R. A. In The Strobilurin Fungicides; Hutson, D. H.; Miyamoto, J., Ed.; Wiley: Chichester, 1998; p 109. (b) Sauter, H.; Steglich, W.; Anke, T. Angew. Chem., Int. Ed. Engl. 1999, 38, 1328.
    • (1998) The Strobilurin Fungicides , pp. 109
    • Clough, J.M.1    Godfrey, C.R.A.2
  • 9
    • 0033577815 scopus 로고    scopus 로고
    • Reviews: (a) Clough, J. M.; Godfrey. C. R. A. In The Strobilurin Fungicides; Hutson, D. H.; Miyamoto, J., Ed.; Wiley: Chichester, 1998; p 109. (b) Sauter, H.; Steglich, W.; Anke, T. Angew. Chem., Int. Ed. Engl. 1999, 38, 1328.
    • (1999) Angew. Chem., Int. Ed. Engl. , vol.38 , pp. 1328
    • Sauter, H.1    Steglich, W.2    Anke, T.3
  • 11
  • 12
    • 0343258644 scopus 로고    scopus 로고
    • Oda, M.; Katsurada, M.; Shiga, Y.; Ohno, F.; Tanaka, K.; Tomita, Y.; Okano, K.; Shirasaki, M.; Takehara, J.; Iwane, H. WO 98/23582, 1998
    • Oda, M.; Katsurada, M.; Shiga, Y.; Ohno, F.; Tanaka, K.; Tomita, Y.; Okano, K.; Shirasaki, M.; Takehara, J.; Iwane, H. WO 98/23582, 1998.
  • 27
    • 0343694310 scopus 로고    scopus 로고
    • Aldrich catalog (1998-1999, Japan): 3-bromobenzotrifluoride; 11 000 yen (100 g), 3-(trifluoromethyl)aniline; 4900 yen (100 g)
    • Aldrich catalog (1998-1999, Japan): 3-bromobenzotrifluoride; 11 000 yen (100 g), 3-(trifluoromethyl)aniline; 4900 yen (100 g).
  • 28
    • 0033515561 scopus 로고    scopus 로고
    • Recently, asymmetric transfer hydrogenation of 6 was improved up to 97% ee by chiral rhodium complex. Murata, K.; Ikariya, T.; Noyori, R. J. Org. Chem. 1999, 64, 2186.
    • (1999) J. Org. Chem. , vol.64 , pp. 2186
    • Murata, K.1    Ikariya, T.2    Noyori, R.3
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    • Wyss, H.; Mettler, H. P.; Previdoli, F. EP 341,693, 1989
    • Wyss, H.; Mettler, H. P.; Previdoli, F. EP 341,693, 1989.
  • 31
    • 0342823871 scopus 로고    scopus 로고
    • note
    • 2O, L-tartaric acid was selected due to higher cost of D-tartaric acid. Aldrich catalog (1998-1999, Japan): D-tartaric acid; 7800 yen (99% ee, 100 g), L-tartaric acid; 2700 yen (99% ee, 500 g).
  • 32
    • 0342823870 scopus 로고    scopus 로고
    • note
    • N,N-Diethylaniline and n-heptane could be recycled by fractional distillation of the filtrate.
  • 33
    • 0343258641 scopus 로고    scopus 로고
    • note
    • 2O [2:1 (v/v)] was 95:5.
  • 34
    • 0343694308 scopus 로고    scopus 로고
    • note
    • (Z)-Ketoxime ethers were not detected at all by HPLC.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.