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2, and worked up in the usual way.
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0039958376
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β-Anomers were detected in 5-10% yield with 2-O-benzylated NPGs.
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0039366127
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In a typical proof of regioselectivity, the product was acylated and the downshifted proton analyzed for two large (e.g., 6) or two small (e.g., 7) couplings.
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35
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27 are alternatives for diffuse and compact, but the former terms have other mechanistic connotations that may be inappropriate in the present context. HARD and SOFT are also possibilities, but which is which?
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