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0343240867
-
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note
-
Compound 1 was prepared by Heck coupling between 2-amino-4-(4-iodophenyl)amino-6-methoxy[1, 3, 5]triazine and methylacrylate in 68% yield. Experimental details will be published elsewhere.
-
-
-
-
15
-
-
34250626858
-
-
Dimerization efficiencies of > 80% have been observed in suitably constructed cinnamophanes: Greiving, H.; Hopf, H.; Jones, P. G.; Bubenitschek, P.; Desvergne, J.-P.; Bouas-Laurent, H. Liebigs Ann. 1995, 1949.
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Bouas-Laurent, H.6
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17
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0000810063
-
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These values are comparable to those reported for analogous imidediaminotriazine receptors: Park, T. K.; Schroeder, J.; Rebek, J., Jr. J. Am. Chem. Soc. 1991, 113, 5125.
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0001262153
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Zerkowski, J. A.; MacDonald, J. C.; Seto, C. T.; Wierda, D. A.; Whitesides, G. M. J. Am. Chem. Soc. 1994, 116, 2382. For a recent overview, see Ariga, K.; Kunitake, Y. Acc. Chem. Res. 1998, 31, 371.
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19
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0001490606
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Zerkowski, J. A.; MacDonald, J. C.; Seto, C. T.; Wierda, D. A.; Whitesides, G. M. J. Am. Chem. Soc. 1994, 116, 2382. For a recent overview, see Ariga, K.; Kunitake, Y. Acc. Chem. Res. 1998, 31, 371.
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Ariga, K.1
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0029103352
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The formation of head-to-tail dimers is more commonly observed in the solid. Crystal engineering can favor the formation of the ε-truxillate dimer [Ito, Y.; Borecka, B.; Scheffer, J, R.; Trotter, J. Tetrahedron Lett. 1995, 36, 6083], as can the use of Lewis acids in solution [ref 6].
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Ito, Y.1
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23
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0343240863
-
-
note
-
2, 400 MHz).
-
-
-
-
24
-
-
0025989335
-
-
The observed binding constant is comparable to that reported in ref 9, but lower than those for tailored barbiturate receptors [Chang, S. K.; Van Engen, D.; Fan, E.; Hamilton, A. D. J. Am. Chem. Soc. 1991, 113, 7640].
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