Direct detection of intramolecular Sb···N nonbonded interaction by 1H-13C and 1H-15N heteronuclear multiple bond correlation spectroscopy

Tetrahedron Letters

Volumn 41, Issue 7, 2000, Pages 1031-1034

  Tokunaga, Tatsuhiro ^a   Seki, Hiroko ^a   Yasuike, Shuji ^b   Ikoma, Masaaki ^b   Kurita, Jyoji ^b   Yamaguchi, Kentaro ^a  

^a CHIBA UNIVERSITY   (Japan)

^b HOKURIKU UNIVERSITY   (Japan)

Author keywords

1H 13C HMBC; 1H 15N HMBC; Intramolecular nonbonded interaction; J HMBC 2D

Indexed keywords

ANTIMONY;

ANALYTIC METHOD; ARTICLE; CHEMICAL REACTION; DRUG SYNTHESIS; MOLECULAR INTERACTION; PROTON NUCLEAR MAGNETIC RESONANCE; PULSED FIELD GEL ELECTROPHORESIS; SPECTROSCOPY; X RAY CRYSTALLOGRAPHY;

EID: 0034639667     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(99)02189-9     Document Type: Article

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11. w 0.054.
12. Neat nitromethane was referenced as 0 ppm (external standard).
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15. max) and varying the evolution time (Δ) from 10 to 290 msec in 20 msec steps. All spectra were processed with shifted Blackman Harris window for the F2 and F1 dimensions after zero filling to the F1 dimension.