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0039979912
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note
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4 Detailed synthetic procedures and full structural characterization of 1a-f will be described elsewhere.
-
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15
-
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0040572759
-
-
note
-
15 4: 3 was treated with sodium borohydride in methanol in the presence of methyl iodide. Detailed synthetic procedures and full structural characterization of 2-5 will be described elsewhere.
-
-
-
-
16
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-
0039387739
-
-
note
-
Molecular modeling using Spartan 4.1.1 (Wavefunction Inc., Irvine, CA) estimated that the Se...F distance is approximately 3.0 Å for 3-5, which is shorter than the sum of van der Waals radii of Se (1.9 Å) and F (1.47 Å).
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17
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0039979911
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note
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19F NMR for 1c is not clear at this moment.
-
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23
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