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109
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33645920774
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Amines for entries c and j were kindly provided by Glaxo-Wellcome
-
Amines for entries c and j were kindly provided by Glaxo-Wellcome.
-
-
-
-
110
-
-
33645938412
-
-
note
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3).
-
-
-
-
111
-
-
33645954702
-
-
Absolute configuration of major enantiomer of product. Absolute configurations were assigned by comparison of the sign of optical rotation with literature values
-
Absolute configuration of major enantiomer of product. Absolute configurations were assigned by comparison of the sign of optical rotation with literature values.
-
-
-
-
112
-
-
33645907326
-
-
This figure differs from that reported in our communication (see ref. 31)
-
This figure differs from that reported in our communication (see ref. 31).
-
-
-
-
113
-
-
33645930764
-
-
In contrast to our earlier report (see rEf. 31) the epoxide is in this case formed in the reaction mixture with 20% ee; a fractional crystallization occurs when using our standard work-up, resulting in isolation of the epoxide with up to 63% ee
-
In contrast to our earlier report (see rEf. 31) the epoxide is in this case formed in the reaction mixture with 20% ee; a fractional crystallization occurs when using our standard work-up, resulting in isolation of the epoxide with up to 63% ee.
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-
-
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114
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0029860777
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Y. Tu, Z.-X. Wang and Y. Shi, J. Am. Chem. Soc., 1996, 118, 9806.
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116
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0001193783
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G. Berti, B. Macchia, F. Macchia and L. Monti, J. Org. Chem., 1968, 33, 4045.
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0042523205
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0028074623
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0029929128
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