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Volumn 122, Issue 26, 2000, Pages 6317-6318

Reactions of hexatriynes with permethyltitanocene and - zirconocene complexes: First NMR observation of a metallocene sliding along a polyyne chain [16]

Author keywords

[No Author keywords available]

Indexed keywords

ORGANOMETALLIC COMPOUND; TITANOCENE; ZIRCONOCENE;

EID: 0034608913     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja994393h     Document Type: Letter
Times cited : (37)

References (37)
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    • note
    • 5), 181.2 (C12/C17).
  • 25
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    • note
    • -3, 6470 measured reflections, 6470 were independent of symmetry, 3733 were observed (I > 2σ(I)), 619 refined parameters, R1 = 0.052, wR2 (all data) = 0.133.
  • 26
    • 0001262340 scopus 로고
    • Os, Ru
    • Selected examples for Co: (a) Rubin, Y.; Knobler, C. B.; Diederich, F. J. Am. Chem. Soc. 1990, 112, 4966. Os, Ru: (b) Low, P. J.; Udachin, K. A.; Enright, G. D.; Carthy, A. J. J. Organomet. Chem. 1999, 578, 103. Ru: (c) Adams, R. D.; Bunz, U. H. F.; Fu, W.; Roidl, G. J. Organomet. Chem. 1999, 578, 55. Rh, Fe: (d) Etches, S. J.; Hart, I. J.; Stone, F. G. A. J. Chem. Soc., Dalton Trans. 1989, 2281. V: (e) Choukroun, R.; Lorber, Ch.; Donnadieu, B.; Henner, B.; Frantz, R.; Guerin, Ch. J. Chem. Soc., Chem Commun. 1999, 1099.
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  • 27
    • 0000043204 scopus 로고    scopus 로고
    • Ru
    • Selected examples for Co: (a) Rubin, Y.; Knobler, C. B.; Diederich, F. J. Am. Chem. Soc. 1990, 112, 4966. Os, Ru: (b) Low, P. J.; Udachin, K. A.; Enright, G. D.; Carthy, A. J. J. Organomet. Chem. 1999, 578, 103. Ru: (c) Adams, R. D.; Bunz, U. H. F.; Fu, W.; Roidl, G. J. Organomet. Chem. 1999, 578, 55. Rh, Fe: (d) Etches, S. J.; Hart, I. J.; Stone, F. G. A. J. Chem. Soc., Dalton Trans. 1989, 2281. V: (e) Choukroun, R.; Lorber, Ch.; Donnadieu, B.; Henner, B.; Frantz, R.; Guerin, Ch. J. Chem. Soc., Chem Commun. 1999, 1099.
    • (1999) J. Organomet. Chem. , vol.578 , pp. 103
    • Low, P.J.1    Udachin, K.A.2    Enright, G.D.3    Carthy, A.J.4
  • 28
    • 0002685616 scopus 로고    scopus 로고
    • Rh, Fe
    • Selected examples for Co: (a) Rubin, Y.; Knobler, C. B.; Diederich, F. J. Am. Chem. Soc. 1990, 112, 4966. Os, Ru: (b) Low, P. J.; Udachin, K. A.; Enright, G. D.; Carthy, A. J. J. Organomet. Chem. 1999, 578, 103. Ru: (c) Adams, R. D.; Bunz, U. H. F.; Fu, W.; Roidl, G. J. Organomet. Chem. 1999, 578, 55. Rh, Fe: (d) Etches, S. J.; Hart, I. J.; Stone, F. G. A. J. Chem. Soc., Dalton Trans. 1989, 2281. V: (e) Choukroun, R.; Lorber, Ch.; Donnadieu, B.; Henner, B.; Frantz, R.; Guerin, Ch. J. Chem. Soc., Chem Commun. 1999, 1099.
    • (1999) J. Organomet. Chem. , vol.578 , pp. 55
    • Adams, R.D.1    Bunz, U.H.F.2    Fu, W.3    Roidl, G.4
  • 29
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    • V
    • Selected examples for Co: (a) Rubin, Y.; Knobler, C. B.; Diederich, F. J. Am. Chem. Soc. 1990, 112, 4966. Os, Ru: (b) Low, P. J.; Udachin, K. A.; Enright, G. D.; Carthy, A. J. J. Organomet. Chem. 1999, 578, 103. Ru: (c) Adams, R. D.; Bunz, U. H. F.; Fu, W.; Roidl, G. J. Organomet. Chem. 1999, 578, 55. Rh, Fe: (d) Etches, S. J.; Hart, I. J.; Stone, F. G. A. J. Chem. Soc., Dalton Trans. 1989, 2281. V: (e) Choukroun, R.; Lorber, Ch.; Donnadieu, B.; Henner, B.; Frantz, R.; Guerin, Ch. J. Chem. Soc., Chem Commun. 1999, 1099.
    • (1989) J. Chem. Soc., Dalton Trans. , pp. 2281
    • Etches, S.J.1    Hart, I.J.2    Stone, F.G.A.3
  • 30
    • 0033591763 scopus 로고    scopus 로고
    • Selected examples for Co: (a) Rubin, Y.; Knobler, C. B.; Diederich, F. J. Am. Chem. Soc. 1990, 112, 4966. Os, Ru: (b) Low, P. J.; Udachin, K. A.; Enright, G. D.; Carthy, A. J. J. Organomet. Chem. 1999, 578, 103. Ru: (c) Adams, R. D.; Bunz, U. H. F.; Fu, W.; Roidl, G. J. Organomet. Chem. 1999, 578, 55. Rh, Fe: (d) Etches, S. J.; Hart, I. J.; Stone, F. G. A. J. Chem. Soc., Dalton Trans. 1989, 2281. V: (e) Choukroun, R.; Lorber, Ch.; Donnadieu, B.; Henner, B.; Frantz, R.; Guerin, Ch. J. Chem. Soc., Chem Commun. 1999, 1099.
    • (1999) J. Chem. Soc., Chem Commun. , pp. 1099
    • Choukroun, R.1    Lorber, Ch.2    Donnadieu, B.3    Henner, B.4    Frantz, R.5    Guerin, Ch.6
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    • 0342480127 scopus 로고    scopus 로고
    • note
    • 5), 114.4 (C2), 115.8 (C3), 118.7 (C6), 160.0 (C4), 193.8 (C1).
  • 32
    • 0343349559 scopus 로고    scopus 로고
    • note
    • -3, 6266 measured reflections, 3340 were independent of symmetry, 2499 were observed (I > 2σ(I)), 316 refined parameters, R1 = 0.037, wR2 (all data) = 0.086.
  • 34
    • 0002204594 scopus 로고
    • 6), three-pulse NOESY sequence (mixing time 2 s), proton decoupling was applied throughout
    • 6), three-pulse NOESY sequence (mixing time 2 s), proton decoupling was applied throughout.
    • (1981) J. Am. Chem. Soc. , vol.103 , pp. 5327
    • Huang, Y.1    Macura, S.2    Ernst, R.R.3
  • 35
    • 84943920736 scopus 로고
    • 2 (SHELXL-93); structure representation by XP (Siemens). Atoms of disordered groups (in 1) are refined isotropically. All other non-hydrogen atoms are refined anisotropically. Hydrogen atoms are included at calculated positions and refined riding with the corresponding atom
    • 2 (SHELXL-93); structure representation by XP (Siemens). Atoms of disordered groups (in 1) are refined isotropically. All other non-hydrogen atoms are refined anisotropically. Hydrogen atoms are included at calculated positions and refined riding with the corresponding atom.
    • (1990) Acta Crytallogr., Sect. A , vol.46 , pp. 467
    • Sheldrick, G.M.1
  • 37
    • 0343349557 scopus 로고    scopus 로고
    • note
    • -1.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.