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note
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To exclude the possibility of catalysis by trace amounts of metals remaining in the autoclave from previous experiments, the reactor was washed extensively with acids, bases, and various organic solvents but no significant change in epoxidation rate was observed. Finally, we decided to manifacture a new autoclave from austenitic steel (material number 1.4571). Again almost quantitative epoxidation of cis-cyclo-octene occurred in the first run.
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85007646219
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This induction period shows some variation, see Table 1, entry 3.
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