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note
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All the samples were crushed with an aluminum oxide mortar under a laminar flow of high-efficiency particulate arresting (HEPA)-filtered air. Because of the very low W concentration in nonmetallic phases (mostly silicates and oxides), we treated all the nonmagnetic phases as a single fraction. Consequently, only three fractions-magnetic, bulk rock, and nonmagnetic-were analyzed, and the separation was performed with a hand magnet. Because abundant fine-grained silicates are intimately intergrown with the metal phases, mechanical separation is unable to provide a pure metallic fraction. Therefore, in addition to the bulk metal measurement some portions of the bulk metal separates from each sample were treated first with hot 6 M HCl to preferentially dissolve the metals. The solution was then decanted from the residue, and the residue was subsequently digested as another silicate/oxide-rich fraction with variable amounts of metal.
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0343846046
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Web fig. 1
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Web fig. 1 is available at www.sciencemag.org/ feature/data/1048497.shl.
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note
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We thank E, Hauri and K. Righter for their reviews; M. Johnson for technical assistance; R. Hewins, G. W. Lugmair, M. Prinz, B. Zanda, and G. J. Wasserburg for discussion; and M. Lindstrom, C. J. MacPherson, and M. Wadhwa for access to their meteorite collections at NASA, the Smithsonian Institution of Washington, and the Field Museum in Chicago. This work was supported by NSF and NASA.
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