Analysis of Multiple-Pulse Techniques under Fast MAS Conditions

Journal of Magnetic Resonance

Volumn 147, Issue 2, 2000, Pages 250-260

  Filip, C ^a   Hafner, S ^b  

^a NATIONAL INSTITUTE FOR RESEARCH AND DEVELOPMENT OF ISOTOPIC AND MOLECULAR TECHNOLOGIES   (Romania)

^b MAX PLANCK INSTITUTE FOR POLYMER RESEARCH   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

ALANINE;

ARTICLE; CHEMISTRY; MATHEMATICS; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

ALANINE; MAGNETIC RESONANCE SPECTROSCOPY; MATHEMATICS;

EID: 0034571978     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.2000.2189     Document Type: Article

References (27)

1. J. S. Waugh, L. Huber, and U. Haeberlen, Approach to high-resolution NMR in solids, Phys. Rev. Lett. 20, 180-182 (1968).
2. E. R. Andrew, A. Bradbury, and R. G. Eads, NMR from a crystal rotated at high speeds, Nature 182, 1959 (1958).
3. I. J. Lowe, Free induction decays in rotating solids, Phys. Rev. Lett. 2, 285 (1959).
4. A. E. Bennet, R. G. Griffin, and S. Vega, Recoupling of homo- and heteronuclear dipolar interactions in rotating solids, in "NMR, Basic Principles and Progress," Vol. 33, Springer-Verlag, Berlin, 1994.
5. S. Hafner and H. W. Spiess, Advanced solid-state NMR spectroscopy of strongly dipolar coupled spins under fast magic angle spinning, Concepts Magn. Reson. 10, 99-128 (1998).
6. M. Maricq and J. S. Waugh, NMR in rotating solids, J. Chem. Phys. 70, 3300-3316 (1979).
7. C. Filip, S. Hafner, I. Schnell, D. E. Demco, and H. W. Spiess, Solid-state NMR spectra of dipolar-coupled multi-spin systems under fast magic angle spinning, J. Chem. Phys. 110, 423-440 (1999).
8. C. Filip, X. Filip, D. E Demco, and S. Hafner, Spin dynamics under magic angle spinning by Floquet formalism, Mol. Phys. 92, 757-771 (1997).
9. W. K. Rhim, D. D. Elleman, and R. W. Vaughn, Analysis of multiple pulse NMR in solids, J. Chem. Phys. 59, 3740-3749 (1973).
10. P. Mansfield, M. J. Orchard, D. C. Stalker, and K. H. B. Richards, Symmetrized multipulse nuclear magnetic resonance experiments in solids: Measurement of the chemical-shift shielding tensor in some compounds, Phys. Rev. B 7, 90-105 (1973).
11. U. Haeberlen, High-resolution NMR of solids, in "Advances in Magnetic Resonance: Selective Averaging," Academic Press, New York, 1976.
12. 1H chemical shift tensors, J. Chem. Phys. 71, 4541-4545 (1979).
13. 1H NMR in solids with multiple-pulse sequences and magic-angle sample spinning at 270 MHz, J. Magn. Reson. 44, 134-144 (1981).
14. 1H NMR analysis of solids by the CRAMPS and MAS-only techniques, J. Magn. Reson. 82, 454-466 (1989).
15. S. Hafner and H. W. Spiess, Multiple-pulse line-narrowing under fast magic-angle spinning, J. Magn. Reson. A 121, 160-166 (1996).
16. S. Hafner and H. W. Spiess, Multiple-pulse assisted line-narrowing by fast magic-angle spinning, Solid State NMR 8, 17-24 (1997).
17. D. E. Demco, S. Hafner, and H. W. Spiess, Rotation-synchronized homonuclear dipolar decoupling, J. Magn. Reson. A 116, 36 (1995).
18. S. Vega, E. T. Olejniczak, and R. G. Griffin, Rotor frequency lines in the nuclear magnetic resonance spectra of rotating solids, J. Chem. Phys. 80, 4832 (1984).
19. O. Weintraub and S. Vega, Floquet density matrices and effective Hamiltonians in magic-angle-spinning NMR spectroscopy, J. Magn. Reson. A 105, 245-267 (1993).
20. T. Nakai and C. A. McDowell, Application of Floquet theory to the nuclear magnetic resonance spectra of homonuclear two-spin systems in rotating solids, J. Chem. Phys. 96, 3452-3466 (1992).
21. T. O. Levante, M. Baldus, B. H. Meier, and R. R. Ernst, Formalized Floquet theory and its applications to sample spinning in nuclear magnetic resonance, Mol. Phys. 86, 1195-1212 (1995).
22. M. Lee and W. I. Goldburg, Nuclear-magnetic-resonance line narrowing by a rotating rf field, Phys. Rev. 6140, A1261-A1271 (1965).
23. U. Haeberlen and J. S. Waugh, Coherent averaging effects in magnetic resonance, Phys. Rev. 175, 453-467 (1968).
24. M. Hohwy and N. C. Nielsen, Elimination of high order terms in multiple pulse nuclear magnetic resonance spectroscopy: Application to homonuclear decoupling in solids, J. Chem. Phys. 106, 7571-7586 (1997).
25. H. Cho, Off-resonance multiple-pulse dynamics in solid-state NMR spectroscopy: A revised coherence averaging theory analysis, J. Chem. Phys. 141, 164-179 (1999).
26. T. M. Barbara and L. Baltusis, Phase-cycled multiple-window-acquisition, multiple-pulse NMR, J. Magn. Reson. A 106, 182 (1994).
27. H. Cho, Tilted-axis precession and phase-sensitive detection of nuclear magnetization, J. Magn. Reson. A 121, 8-22 (1996).