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8 and expanded using Fourier techniques, and refined by full-matrix least-square calculations. The non-hydrogen atoms were refined anisotropically. Hydrogen atoms were included, but their positions were not refined. All calculations were performed using the teXsan crystallographic software package of Molecular Structure Corporation. The final R1 = 0.034, Rw = 0.055, goodness of fit = 0.64, max. Shift/e.s.d = 0.007.
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