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0032539236
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Syntheses of 1 and 2 followed established procedures; see: (a) Haaf, M. H.; Schmiedl, A.; Schmedake, T. A.; Powell, D. R.; Millevolte, A. J.; Denk, M.; West, R. J. Am. Chem. Soc. 1998, 120, 12714.
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33646273473
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note
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2). Due to the extreme reactivity of the complex, satisfactory elemental analyses could not be obtained.
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14
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33646301264
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note
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3, R(F) = 0.0418 for 4908 observed reflections. All non-hydrogen atoms were refined with anisotropic displacement parameters. Full crystallographic information is given in the Supporting Information.
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15
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