Proton MAS NMR Spectra at High Magnetic Fields and High Spinning Frequencies: Spectral Simulations Using Floquet Theory

Journal of Magnetic Resonance

Volumn 135, Issue 2, 1998, Pages 418-426

  Ray, Siddharth ^a   Vinogradov, Elena ^a   Boender, Gert Jan ^a   Vega, Shimon ^a  

^a WEIZMANN INSTITUTE OF SCIENCE   (Israel)

Author keywords

[No Author keywords available]

Indexed keywords

ARTICLE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

MAGNETIC RESONANCE SPECTROSCOPY;

EID: 0032246292     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.1998.9998     Document Type: Article

References (37)

1. A. Mehta, B. Tounge, S. Burns, X. Wu, I. Wu, and K. W. Zilm, in 38th Rocky Mountain Conference on Analytical Chemistry, Denver, 1996.
2. L. M. Ryan, R. E. Taylor, A. J. Paff, and B. C. Gerstein, J. Chem. Phys. 72, 508-515 (1980); G. E. Maciel, C. E. Bronnimann, and B. L. Hawkins, Adv. Magn. Reson. 14, 125-150 (1990).
3. L. M. Ryan, R. E. Taylor, A. J. Paff, and B. C. Gerstein, J. Chem. Phys. 72, 508-515 (1980); G. E. Maciel, C. E. Bronnimann, and B. L. Hawkins, Adv. Magn. Reson. 14, 125-150 (1990).
4. D. E. Demco, S. Hafner, and H. W. Spiess, J. Magn. Reson. A 116, 36-45 (1995).
5. A. Bielecki, A. C. Kolbert, and M. H. Levitt, Chem. Phys. Lett. 155, 341-346 (1989).
6. B.-J. Van Rossum, H. Forster, and H. J. M. de Groot, J. Magn. Reson. 124, 516-519 (1997).
7. H. Geen, J. J. Titmann, J. Gottwald, and H. W. Spiess, J. Magn. Reson. A 114, 264-267 (1995).
8. O. Weintraub and S. Vega, J. Magn. Reson. A 105, 245-267 (1993).
9. T. Nakai and C. A. McDowell, Mol. Phys. 77, 569-584 (1992); T. Nakai and C. A. McDowell, J. Chem. Phys. 96, 3452-3466 (1992).
10. T. Nakai and C. A. McDowell, Mol. Phys. 77, 569-584 (1992); T. Nakai and C. A. McDowell, J. Chem. Phys. 96, 3452-3466 (1992).
11. D. Marks and S. Vega, J. Magn. Reson. A 118, 157-172 (1996).
12. M. M. Maricq and J. S. Waugh, J. Chem. Phys. 70, 3300-3316 (1979).
13. M. H. Levitt, D. P. Raleigh, F. Creuzet, and R. G. Griffin, J. Chem. Phys. 92, 6347-6364 (1990).
14. R. Wind, in "Modern NMR Techniques and Their Application in Chemistry" (A.I. Popov and K. Hallenda, Eds.), p. 125; R. Wind, private communication.
15. R. Wind, in "Modern NMR Techniques and Their Application in Chemistry" (A.I. Popov and K. Hallenda, Eds.), p. 125; R. Wind, private communication.
16. R. Challoner and C. A. McDowell, J. Magn. Reson. 98, 123-133 (1992).
17. E. Brunner, D. Freude, B. C. Gerstein, and H. Pfeifer, J. Magn. Reson. 90, 90-99 (1990).
18. A. Schmidt and A. Vega, J. Chem. Phys. 96, 2655-2680 (1992).
19. E. Bennet, R. G. Griffin, and S. Vega, in "NMR, Basic Principles and Progress" (P. Diehl, E. Fluck, H. Gunther, R. Kosfeld, and J. Seeling, Eds.), Vol. 33, p. 1, Springer-Verlag, Berlin (1994).
20. H. Conroy, J. Chem. Phys. 47, 5307-5318 (1967).
21. T. O. Levante, M. Baldus, B. H. Meier, and R. R. Ernst, Mol. Phys. 86, 1195-1211 (1995).
22. S. Zhang, J. Magn. Reson. A 110, 73-76 (1994); O. B. Peersen, X. Wu, and S. O. Smith, J. Magn. Reson. A106, 127-131 (1994); O. B. Peersen, X. Wu, I. Kustanovich, and S. O. Smith, J. Magn. Reson. A 104, 334-339 (1993).
23. S. Zhang, J. Magn. Reson. A 110, 73-76 (1994); O. B. Peersen, X. Wu, and S. O. Smith, J. Magn. Reson. A106, 127-131 (1994); O. B. Peersen, X. Wu, I. Kustanovich, and S. O. Smith, J. Magn. Reson. A 104, 334-339 (1993).
24. S. Zhang, J. Magn. Reson. A 110, 73-76 (1994); O. B. Peersen, X. Wu, and S. O. Smith, J. Magn. Reson. A106, 127-131 (1994); O. B. Peersen, X. Wu, I. Kustanovich, and S. O. Smith, J. Magn. Reson. A 104, 334-339 (1993).
25. S. Zhang, B. H. Meier, and R. R. Ernst, J. Magn. Reson. 108, 30-37 (1994); S. Hediger, B. H. Meier, N. D. Kurur, G. Bodenhausen, and R. R. Ernst, Chem. Phys. Lett. 223, 283-288 (1994); S. Hediger, B. H. Meier, and R. R. Ernst, Chem. Phys. Lett. 240, 449-456 (1995); A. Verhoeven, R. Verel, and B. H. Meier, Chem. Phys. Lett. 266, 465-472 (1997); M. Baldus, D. G. Geurts, S. Hediger, and B. H. Meier, J. Magn. Reson. 118, 140-144 (1996).
26. S. Zhang, B. H. Meier, and R. R. Ernst, J. Magn. Reson. 108, 30-37 (1994); S. Hediger, B. H. Meier, N. D. Kurur, G. Bodenhausen, and R. R. Ernst, Chem. Phys. Lett. 223, 283-288 (1994); S. Hediger, B. H. Meier, and R. R. Ernst, Chem. Phys. Lett. 240, 449-456 (1995); A. Verhoeven, R. Verel, and B. H. Meier, Chem. Phys. Lett. 266, 465-472 (1997); M. Baldus, D. G. Geurts, S. Hediger, and B. H. Meier, J. Magn. Reson. 118, 140-144 (1996).
27. S. Zhang, B. H. Meier, and R. R. Ernst, J. Magn. Reson. 108, 30-37 (1994); S. Hediger, B. H. Meier, N. D. Kurur, G. Bodenhausen, and R. R. Ernst, Chem. Phys. Lett. 223, 283-288 (1994); S. Hediger, B. H. Meier, and R. R. Ernst, Chem. Phys. Lett. 240, 449-456 (1995); A. Verhoeven, R. Verel, and B. H. Meier, Chem. Phys. Lett. 266, 465-472 (1997); M. Baldus, D. G. Geurts, S. Hediger, and B. H. Meier, J. Magn. Reson. 118, 140-144 (1996).
28. S. Zhang, B. H. Meier, and R. R. Ernst, J. Magn. Reson. 108, 30-37 (1994); S. Hediger, B. H. Meier, N. D. Kurur, G. Bodenhausen, and R. R. Ernst, Chem. Phys. Lett. 223, 283-288 (1994); S. Hediger, B. H. Meier, and R. R. Ernst, Chem. Phys. Lett. 240, 449-456 (1995); A. Verhoeven, R. Verel, and B. H. Meier, Chem. Phys. Lett. 266, 465-472 (1997); M. Baldus, D. G. Geurts, S. Hediger, and B. H. Meier, J. Magn. Reson. 118, 140-144 (1996).
29. S. Zhang, B. H. Meier, and R. R. Ernst, J. Magn. Reson. 108, 30-37 (1994); S. Hediger, B. H. Meier, N. D. Kurur, G. Bodenhausen, and R. R. Ernst, Chem. Phys. Lett. 223, 283-288 (1994); S. Hediger, B. H. Meier, and R. R. Ernst, Chem. Phys. Lett. 240, 449-456 (1995); A. Verhoeven, R. Verel, and B. H. Meier, Chem. Phys. Lett. 266, 465-472 (1997); M. Baldus, D. G. Geurts, S. Hediger, and B. H. Meier, J. Magn. Reson. 118, 140-144 (1996).
30. D. Suter and R. R. Ernst, Phys. Rev. B 32, 5608-5627 (1985).
31. D. E. Demco, J. Tegenfeldt, and J. S. Waugh, Phys. Rev. B 11, 4133-4151 (1975); D. Suter and R. R. Ernst, Phys. Rev. B 25, 6038-6041 (1982); S. R. Hartmann and E. L. Hahn, Phys. Rev. 128, 2042-2053 (1962); F. M. Lurie and C. P. Slichter, Phys. Rev. A 133, 1108-1122 (1964); A. Pines, M. G. Gibby, and J. S. Waugh, J. Chem. Phys. 59, 569-590 (1973); M. Mehring, "Principles of High Resolution NMR in Solids," 2nd ed., Springer-Verlag, Berlin/New York (1983); D. Michel and F. Engelke, in "NMR, Basic Principles and Progress" (P. Diehl, E. Fluck, H. Gunther, R. Kosfeld, and J. Seeling, Eds.), Vol. 32, p. 69, Springer-Verlag, Berlin (1994).
32. D. E. Demco, J. Tegenfeldt, and J. S. Waugh, Phys. Rev. B 11, 4133-4151 (1975); D. Suter and R. R. Ernst, Phys. Rev. B 25, 6038-6041 (1982); S. R. Hartmann and E. L. Hahn, Phys. Rev. 128, 2042-2053 (1962); F. M. Lurie and C. P. Slichter, Phys. Rev. A 133, 1108-1122 (1964); A. Pines, M. G. Gibby, and J. S. Waugh, J. Chem. Phys. 59, 569-590 (1973); M. Mehring, "Principles of High Resolution NMR in Solids," 2nd ed., Springer-Verlag, Berlin/New York (1983); D. Michel and F. Engelke, in "NMR, Basic Principles and Progress" (P. Diehl, E. Fluck, H. Gunther, R. Kosfeld, and J. Seeling, Eds.), Vol. 32, p. 69, Springer-Verlag, Berlin (1994).
33. D. E. Demco, J. Tegenfeldt, and J. S. Waugh, Phys. Rev. B 11, 4133-4151 (1975); D. Suter and R. R. Ernst, Phys. Rev. B 25, 6038-6041 (1982); S. R. Hartmann and E. L. Hahn, Phys. Rev. 128, 2042-2053 (1962); F. M. Lurie and C. P. Slichter, Phys. Rev. A 133, 1108-1122 (1964); A. Pines, M. G. Gibby, and J. S. Waugh, J. Chem. Phys. 59, 569-590 (1973); M. Mehring, "Principles of High Resolution NMR in Solids," 2nd ed., Springer-Verlag, Berlin/New York (1983); D. Michel and F. Engelke, in "NMR, Basic Principles and Progress" (P. Diehl, E. Fluck, H. Gunther, R. Kosfeld, and J. Seeling, Eds.), Vol. 32, p. 69, Springer-Verlag, Berlin (1994).
34. D. E. Demco, J. Tegenfeldt, and J. S. Waugh, Phys. Rev. B 11, 4133-4151 (1975); D. Suter and R. R. Ernst, Phys. Rev. B 25, 6038-6041 (1982); S. R. Hartmann and E. L. Hahn, Phys. Rev. 128, 2042-2053 (1962); F. M. Lurie and C. P. Slichter, Phys. Rev. A 133, 1108-1122 (1964); A. Pines, M. G. Gibby, and J. S. Waugh, J. Chem. Phys. 59, 569-590 (1973); M. Mehring, "Principles of High Resolution NMR in Solids," 2nd ed., Springer-Verlag, Berlin/New York (1983); D. Michel and F. Engelke, in "NMR, Basic Principles and Progress" (P. Diehl, E. Fluck, H. Gunther, R. Kosfeld, and J. Seeling, Eds.), Vol. 32, p. 69, Springer-Verlag, Berlin (1994).
35. D. E. Demco, J. Tegenfeldt, and J. S. Waugh, Phys. Rev. B 11, 4133-4151 (1975); D. Suter and R. R. Ernst, Phys. Rev. B 25, 6038-6041 (1982); S. R. Hartmann and E. L. Hahn, Phys. Rev. 128, 2042-2053 (1962); F. M. Lurie and C. P. Slichter, Phys. Rev. A 133, 1108-1122 (1964); A. Pines, M. G. Gibby, and J. S. Waugh, J. Chem. Phys. 59, 569-590 (1973); M. Mehring, "Principles of High Resolution NMR in Solids," 2nd ed., Springer-Verlag, Berlin/New York (1983); D. Michel and F. Engelke, in "NMR, Basic Principles and Progress" (P. Diehl, E. Fluck, H. Gunther, R. Kosfeld, and J. Seeling, Eds.), Vol. 32, p. 69, Springer-Verlag, Berlin (1994).
36. D. E. Demco, J. Tegenfeldt, and J. S. Waugh, Phys. Rev. B 11, 4133-4151 (1975); D. Suter and R. R. Ernst, Phys. Rev. B 25, 6038-6041 (1982); S. R. Hartmann and E. L. Hahn, Phys. Rev. 128, 2042-2053 (1962); F. M. Lurie and C. P. Slichter, Phys. Rev. A 133, 1108-1122 (1964); A. Pines, M. G. Gibby, and J. S. Waugh, J. Chem. Phys. 59, 569-590 (1973); M. Mehring, "Principles of High Resolution NMR in Solids," 2nd ed., Springer-Verlag, Berlin/New York (1983); D. Michel and F. Engelke, in "NMR, Basic Principles and Progress" (P. Diehl, E. Fluck, H. Gunther, R. Kosfeld, and J. Seeling, Eds.), Vol. 32, p. 69, Springer-Verlag, Berlin (1994).
37. D. E. Demco, J. Tegenfeldt, and J. S. Waugh, Phys. Rev. B 11, 4133-4151 (1975); D. Suter and R. R. Ernst, Phys. Rev. B 25, 6038-6041 (1982); S. R. Hartmann and E. L. Hahn, Phys. Rev. 128, 2042-2053 (1962); F. M. Lurie and C. P. Slichter, Phys. Rev. A 133, 1108-1122 (1964); A. Pines, M. G. Gibby, and J. S. Waugh, J. Chem. Phys. 59, 569-590 (1973); M. Mehring, "Principles of High Resolution NMR in Solids," 2nd ed., Springer-Verlag, Berlin/New York (1983); D. Michel and F. Engelke, in "NMR, Basic Principles and Progress" (P. Diehl, E. Fluck, H. Gunther, R. Kosfeld, and J. Seeling, Eds.), Vol. 32, p. 69, Springer-Verlag, Berlin (1994).